Superconducting properties of Rh9In4S4 single crystals

Kaluarachchi, Udhara S.; Lin, Qisheng; Xie, Weiwei; Taufour, Valentin; Bud'ko, Sergey L.; Miller, Gordon J.; Canfield, Paul C.

doi:10.1103/PhysRevB.93.094524

Title: Superconducting properties of ${Rh}_{9} {In}_{4} S_{4}$ single crystals

Abstract

The synthesis and crystallographic, thermodynamic, and transport properties of single crystalline Rh₉In₄S₄ were studied. The resistivity, magnetization, and specific heat measurements all clearly indicate bulk superconductivity with a critical temperature, T_c~2.25 K. The Sommerfeld coefficient γ and the Debye temperature (ΘD) were found to be 34 mJ mol^–1 K^–2 and 217 K, respectively. The observed specific heat jump, ΔC/γT_c=1.66, is larger than the expected BCS weak coupling value of 1.43. Ginzburg-Landau (GL) ratio of the low-temperature GL-penetration depth, λ_GL≈5750 Å, to the GL-coherence length, ξ_GL≈94 Å, is large: κ ~60. However, we observed a peak effect in the resistivity measurement as a function of both temperature and magnetic field.

Authors:

Kaluarachchi, Udhara S. ^[1]; Lin, Qisheng ^[1]; Xie, Weiwei ^[1]; Taufour, Valentin ^[1]; Bud'ko, Sergey L. ^[1]; Miller, Gordon J. ^[1]; Canfield, Paul C. ^[1]

Ames Lab. and Iowa State Univ., Ames, IA (United States)

Publication Date:: Mon Mar 28 00:00:00 EDT 2016

Research Org.:: Ames Laboratory (AMES), Ames, IA (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1253760

Alternate Identifier(s):: OSTI ID: 1244165

Report Number(s):: IS-J-8963
Journal ID: ISSN 2469-9950; PRBMDO

Grant/Contract Number:: AC02-07CH11358

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review B

Additional Journal Information:: Journal Volume: 93; Journal Issue: 9; Journal ID: ISSN 2469-9950

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats


                    Kaluarachchi, Udhara S., Lin, Qisheng, Xie, Weiwei, Taufour, Valentin, Bud'ko, Sergey L., Miller, Gordon J., and Canfield, Paul C. Superconducting properties of Rh9In4S4 single crystals.  United States: N. p., 2016. 
Web.  doi:10.1103/PhysRevB.93.094524.

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                    Kaluarachchi, Udhara S., Lin, Qisheng, Xie, Weiwei, Taufour, Valentin, Bud'ko, Sergey L., Miller, Gordon J., & Canfield, Paul C. Superconducting properties of Rh9In4S4 single crystals.  United States.  https://doi.org/10.1103/PhysRevB.93.094524

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                    Kaluarachchi, Udhara S., Lin, Qisheng, Xie, Weiwei, Taufour, Valentin, Bud'ko, Sergey L., Miller, Gordon J., and Canfield, Paul C. Mon .  
"Superconducting properties of Rh9In4S4 single crystals".  United States.  https://doi.org/10.1103/PhysRevB.93.094524.  https://www.osti.gov/servlets/purl/1253760.

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@article{osti_1253760,

  title        = {Superconducting properties of Rh9In4S4 single crystals},

  author       = {Kaluarachchi, Udhara S. and Lin, Qisheng and Xie, Weiwei and Taufour, Valentin and Bud'ko, Sergey L. and Miller, Gordon J. and Canfield, Paul C.},

  abstractNote = {The synthesis and crystallographic, thermodynamic, and transport properties of single crystalline Rh9In4S4 were studied. The resistivity, magnetization, and specific heat measurements all clearly indicate bulk superconductivity with a critical temperature, Tc~2.25 K. The Sommerfeld coefficient γ and the Debye temperature (ΘD) were found to be 34 mJ mol–1 K–2 and 217 K, respectively. The observed specific heat jump, ΔC/γTc=1.66, is larger than the expected BCS weak coupling value of 1.43. Ginzburg-Landau (GL) ratio of the low-temperature GL-penetration depth, λGL≈5750 Å, to the GL-coherence length, ξGL≈94 Å, is large: κ ~60. However, we observed a peak effect in the resistivity measurement as a function of both temperature and magnetic field.},

  doi          = {10.1103/PhysRevB.93.094524},

  journal      = {Physical Review B},

  number       = 9,

  volume       = 93,

  place        = {United States},

  year         = {Mon Mar 28 00:00:00 EDT 2016},

  month        = {Mon Mar 28 00:00:00 EDT 2016}

}

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New materials physics
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Title: Superconducting properties of Rh 9 In 4 S 4 single crystals

Abstract

Citation Formats

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples journal, December 2015

Superconductivity at High Magnetic Fields journal, July 1963

The electrical properties and the magnitude of the indirect gap in the semiconducting transition metal dichalcogenide layer crystals journal, January 1975

Flux vortices and transport currents in type II superconductors journal, March 1972

Peak effect in hydrogenated ReCr amorphous alloys journal, June 1997

Development of viable solutions for the synthesis of sulfur bearing single crystals journal, July 2012

The Peak Effect in Substitutional and Interstitial Solid Solutions of High-Field Superconductors journal, January 1964

High-Field Superconductivity in Niobium journal, December 1962

Growth of single crystals from metallic fluxes journal, June 1992

Anomalous electrical resistivity in the superconducting state of CeRu2 journal, July 1996

Flux Pinning by Superconducting Precipitates journal, June 1966

Varieties of dynamics in a disordered flux-line lattice journal, February 1996

Superconducting transition and phase diagram of single-crystal MgB 2 journal, January 2003

Peak effect in the vortex state of V3Si: a study of history dependence journal, May 2001

Electric-field-induced superconductivity at 9.4 K in a layered transition metal disulphide MoS 2 journal, July 2012

Critical currents and pinning effect in superconducting alloy films spatially modulated in concentration journal, December 1972

A note on the Maximum Critical Field of High‐Field Superconductors journal, September 1962

Superconductivity in ternary chalcogenides Bi 2 Ni 3 X 2 (X = S, Se) journal, April 2006

Observation of the peak effect in the superconductor Ca 3 Rh 4 Sn 13 journal, October 1997

Peak Effect in CeRu 2 : Role of Crystalline Defects journal, October 1998

Superconductivity in the PbO-type structure -FeSe journal, September 2008

Synthesis, Structure, and Bonding of Sc 4 Mg x Cu 15 - x Ga ∼ 7.5 ( x = 0, 0.5). Two Incommensurately Modulated Scandium Substitution Derivatives of Cubic Mg 2 Cu 6 Ga 5 journal, February 2008

Synthesis and electrical properties of shandite-parkerite phases, A2M3Ch2 journal, March 1988

Hall Effect, Resistivity, and Magnetoresistivity of Th, U, Zr, Ti, and Nb journal, May 1959

Regions of enhanced pinning in the mixed state of the superconductor Yb3Rh4Sn13 journal, June 1997

Growing intermetallic single crystals using in situ decanting journal, July 2012

Superconductivity at High Magnetic Fields and Current Densities in Some Nb-Zr Alloys journal, June 1961

Heat capacity of 2HNbSe2 at the charge density wave transition journal, August 1975

Scaling laws for flux pinning in hard superconductors journal, March 1973

Relationship between surface superconductivity, bulk superconductivity and the peak effect in MgB 2 single crystals journal, June 2008

Optical studies of metal-semiconductor transmutations produced by intercalation journal, January 1971

Superconductivity in CuxTiSe2 journal, July 2006

Superconductivity in the layered compound 2H-TaS2 journal, October 1992

Superconductivity at 27K in tetragonal FeSe under high pressure journal, October 2008

A possible mechanism for the peak effect in type II superconductors journal, February 1969

Flux Flow Transport Properties and Peak Effect in a CeRu 2 Single Crystal journal, June 1996

Charge-Density Waves in Metallic, Layered, Transition-Metal Dichalcogenides journal, April 1974

Electric Field Breakdown of Charge-Density-Wave—Induced Anomalies in Nb Se 3 journal, September 1976

Electronic properties and superlattice formation in the semimetal TiSe 2 journal, November 1976

Strongly Correlated Superconductivity in Rh 17 S 15 journal, January 2008

Magnetic structure of the new layered ferromagnetic chromium hexatellurosilicate Cr2Si2Te6 journal, March 1991

Magnetic properties of the itinerant metamagnetic system Co ( S 1 − x Se x ) 2 under high magnetic fields and high pressure journal, December 1997

Pressure effect on competition between charge density wave and superconductivity in ZrTe 3 : Appearance of pressure-induced reentrant superconductivity journal, April 2005

Transport properties in normal-metal Bi 2 Pd 3 S 2 and superconducting Bi 2 Pd 3 Se 2 journal, July 2008

Charge-density-wave superconductor Bi 2 Rh 3 Se 2 journal, February 2007

Superconductivity versus structural phase transition in the closely related Bi 2 Rh 3.5 S 2 and Bi 2 Rh 3 S 2 journal, May 2015

High-temperature solution growth of intermetallic single crystals and quasicrystals journal, May 2001

An empirical correction for absorption anisotropy journal, January 1995

EXPGUI , a graphical user interface for GSAS journal, April 2001

Theory of Superconductivity journal, December 1957

Transition Temperature of Strong-Coupled Superconductors journal, March 1968

Pinning in type II superconductors journal, February 1979

Anisotropy of the upper critical field and critical current in single crystal MgB 2 journal, November 2002

Temperature and Purity Dependence of the Superconducting Critical Field, H c 2 . II journal, July 1966

Upper Limit for the Critical Field in Hard Superconductors journal, September 1962

Note on supraconductivity journal, May 1934

Magnetic measurements of the upper critical field of YBa 2 Cu 3 O 7 − δ single crystals journal, April 1989

Flux vortices and transport currents in type II superconductors journal, December 2001

Strongly correlated superconductivity in Rh 17 S 15 journal, March 2009

Theory of Superconductivity journal, May 1965

High-Field Superconductivity in Niobium journal, February 1963

Superconductivity at 27 K in tetragonal FeSe under high pressure text, January 2008

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples text, January 2015

Superconducting Transition and Phase Diagram of Single Crystal MgB2 text, January 2002

Superconductivity in Cu_xTiSe_2 text, January 2006

New materials physics journal, November 2019

Title: Superconducting properties of ${Rh}_{9} {In}_{4} S_{4}$ single crystals

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples
journal, December 2015

Superconductivity at High Magnetic Fields
journal, July 1963

The electrical properties and the magnitude of the indirect gap in the semiconducting transition metal dichalcogenide layer crystals
journal, January 1975

Flux vortices and transport currents in type II superconductors
journal, March 1972

Peak effect in hydrogenated ReCr amorphous alloys
journal, June 1997

Development of viable solutions for the synthesis of sulfur bearing single crystals
journal, July 2012

The Peak Effect in Substitutional and Interstitial Solid Solutions of High-Field Superconductors
journal, January 1964

High-Field Superconductivity in Niobium
journal, December 1962

Growth of single crystals from metallic fluxes
journal, June 1992

Anomalous electrical resistivity in the superconducting state of CeRu2
journal, July 1996

Flux Pinning by Superconducting Precipitates
journal, June 1966

Varieties of dynamics in a disordered flux-line lattice
journal, February 1996

Superconducting transition and phase diagram of single-crystal ${MgB}_{2}$
journal, January 2003

Peak effect in the vortex state of V3Si: a study of history dependence
journal, May 2001

Electric-field-induced superconductivity at 9.4 K in a layered transition metal disulphide MoS ₂
journal, July 2012

Critical currents and pinning effect in superconducting alloy films spatially modulated in concentration
journal, December 1972

A note on the Maximum Critical Field of High‐Field Superconductors
journal, September 1962

Superconductivity in ternary chalcogenides Bi ₂ Ni ₃ X ₂ (X = S, Se)
journal, April 2006

Observation of the peak effect in the superconductor ${Ca}_{3} {Rh}_{4} {Sn}_{13}$
journal, October 1997

Peak Effect in CeRu ₂ : Role of Crystalline Defects
journal, October 1998

Superconductivity in the PbO-type structure -FeSe
journal, September 2008

Synthesis, Structure, and Bonding of Sc ₄ Mg _x Cu ₁₅ _- _x Ga _∼ _7.5 ( x = 0, 0.5). Two Incommensurately Modulated Scandium Substitution Derivatives of Cubic Mg ₂ Cu ₆ Ga ₅
journal, February 2008

Synthesis and electrical properties of shandite-parkerite phases, A2M3Ch2
journal, March 1988

Hall Effect, Resistivity, and Magnetoresistivity of Th, U, Zr, Ti, and Nb
journal, May 1959

Regions of enhanced pinning in the mixed state of the superconductor Yb3Rh4Sn13
journal, June 1997

Growing intermetallic single crystals using in situ decanting
journal, July 2012

Superconductivity at High Magnetic Fields and Current Densities in Some Nb-Zr Alloys
journal, June 1961

Heat capacity of 2HNbSe2 at the charge density wave transition
journal, August 1975

Scaling laws for flux pinning in hard superconductors
journal, March 1973

Relationship between surface superconductivity, bulk superconductivity and the peak effect in MgB ₂ single crystals
journal, June 2008

Optical studies of metal-semiconductor transmutations produced by intercalation
journal, January 1971

Superconductivity in CuxTiSe2
journal, July 2006

Superconductivity in the layered compound 2H-TaS2
journal, October 1992

Superconductivity at 27K in tetragonal FeSe under high pressure
journal, October 2008

A possible mechanism for the peak effect in type II superconductors
journal, February 1969

Flux Flow Transport Properties and Peak Effect in a CeRu ₂ Single Crystal
journal, June 1996

Charge-Density Waves in Metallic, Layered, Transition-Metal Dichalcogenides
journal, April 1974

Electric Field Breakdown of Charge-Density-Wave—Induced Anomalies in Nb ${Se}_{3}$
journal, September 1976

Electronic properties and superlattice formation in the semimetal ${TiSe}_{2}$
journal, November 1976

Strongly Correlated Superconductivity in ${Rh}_{17} S_{15}$
journal, January 2008

Magnetic structure of the new layered ferromagnetic chromium hexatellurosilicate Cr2Si2Te6
journal, March 1991

Magnetic properties of the itinerant metamagnetic system $Co (S_{1 - x} {Se}_{x})_{2}$ under high magnetic fields and high pressure
journal, December 1997

Pressure effect on competition between charge density wave and superconductivity in ${ZrTe}_{3}$ : Appearance of pressure-induced reentrant superconductivity
journal, April 2005

Transport properties in normal-metal ${Bi}_{2} {Pd}_{3} S_{2}$ and superconducting ${Bi}_{2} {Pd}_{3} {Se}_{2}$
journal, July 2008

Charge-density-wave superconductor ${Bi}_{2} {Rh}_{3} {Se}_{2}$
journal, February 2007

Superconductivity versus structural phase transition in the closely related ${Bi}_{2} {Rh}_{3.5} S_{2}$ and ${Bi}_{2} {Rh}_{3} S_{2}$
journal, May 2015

High-temperature solution growth of intermetallic single crystals and quasicrystals
journal, May 2001

An empirical correction for absorption anisotropy
journal, January 1995

EXPGUI , a graphical user interface for GSAS
journal, April 2001

Theory of Superconductivity
journal, December 1957

Transition Temperature of Strong-Coupled Superconductors
journal, March 1968

Pinning in type II superconductors
journal, February 1979

Anisotropy of the upper critical field and critical current in single crystal ${MgB}_{2}$
journal, November 2002

Temperature and Purity Dependence of the Superconducting Critical Field, $H_{c 2}$ . II
journal, July 1966

Upper Limit for the Critical Field in Hard Superconductors
journal, September 1962

Note on supraconductivity
journal, May 1934

Magnetic measurements of the upper critical field of ${YBa}_{2}$ ${Cu}_{3}$ $O_{7 - δ}$ single crystals
journal, April 1989

Flux vortices and transport currents in type II superconductors
journal, December 2001

Strongly correlated superconductivity in Rh ₁₇ S ₁₅
journal, March 2009

Theory of Superconductivity
journal, May 1965

High-Field Superconductivity in Niobium
journal, February 1963

Superconductivity at 27 K in tetragonal FeSe under high pressure
text, January 2008

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples
text, January 2015

Superconducting Transition and Phase Diagram of Single Crystal MgB2
text, January 2002

Superconductivity in Cu_xTiSe_2
text, January 2006

New materials physics
journal, November 2019