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Title: Defects Engineered Monolayer MoS2 for Improved Hydrogen Evolution Reaction

Abstract

MoS2 is a promising, low-cost material for electrochemical hydrogen production due to its high activity and stability during the reaction. Our work represents an easy method to increase the hydrogen production in electrochemical reaction of MoS2 via defect engineering, and helps to understand the catalytic properties of MoS2.

Authors:
 [1];  [2];  [3];  [1];  [1];  [3];  [4];  [1];  [5]
  1. Rice Univ., Houston, TX (United States). Department of Materials Science and NanoEngineering
  2. Rice Univ., Houston, TX (United States). Department of Chemistry
  3. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science & Technology Division; Vanderbilt Univ., Nashville, TN (United States). Department of Physics and Astronomy
  4. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science & Technology Division
  5. Rice Univ., Houston, TX (United States). Department of Materials Science and NanoEngineering; Rice Univ., Houston, TX (United States). Department of Chemistry
Publication Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Center for Nanophase Materials Sciences (CNMS)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1240562
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Nano Letters
Additional Journal Information:
Journal Volume: 16; Journal Issue: 2; Journal ID: ISSN 1530-6984
Publisher:
American Chemical Society
Country of Publication:
United States
Language:
English
Subject:
77 NANOSCIENCE AND NANOTECHNOLOGY; Monolayer MoS2; hydrogen evolution reaction; defects; oxygen plasma; hydrogen treatment

Citation Formats

Ye, Gonglan, Gong, Yongji, Lin, Junhao, Li, Bo, He, Yongmin, Pantelides, Sokrates T., Zhou, Wu, Vajtai, Robert, and Ajayan, Pulickel M.. Defects Engineered Monolayer MoS2 for Improved Hydrogen Evolution Reaction. United States: N. p., 2016. Web. https://doi.org/10.1021/acs.nanolett.5b04331.
Ye, Gonglan, Gong, Yongji, Lin, Junhao, Li, Bo, He, Yongmin, Pantelides, Sokrates T., Zhou, Wu, Vajtai, Robert, & Ajayan, Pulickel M.. Defects Engineered Monolayer MoS2 for Improved Hydrogen Evolution Reaction. United States. https://doi.org/10.1021/acs.nanolett.5b04331
Ye, Gonglan, Gong, Yongji, Lin, Junhao, Li, Bo, He, Yongmin, Pantelides, Sokrates T., Zhou, Wu, Vajtai, Robert, and Ajayan, Pulickel M.. Wed . "Defects Engineered Monolayer MoS2 for Improved Hydrogen Evolution Reaction". United States. https://doi.org/10.1021/acs.nanolett.5b04331. https://www.osti.gov/servlets/purl/1240562.
@article{osti_1240562,
title = {Defects Engineered Monolayer MoS2 for Improved Hydrogen Evolution Reaction},
author = {Ye, Gonglan and Gong, Yongji and Lin, Junhao and Li, Bo and He, Yongmin and Pantelides, Sokrates T. and Zhou, Wu and Vajtai, Robert and Ajayan, Pulickel M.},
abstractNote = {MoS2 is a promising, low-cost material for electrochemical hydrogen production due to its high activity and stability during the reaction. Our work represents an easy method to increase the hydrogen production in electrochemical reaction of MoS2 via defect engineering, and helps to understand the catalytic properties of MoS2.},
doi = {10.1021/acs.nanolett.5b04331},
journal = {Nano Letters},
number = 2,
volume = 16,
place = {United States},
year = {2016},
month = {1}
}

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Cited by: 127 works
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    • DOI: 10.1038/s41699-019-0107-5

    Oxygen Vacancies in ZnO Nanosheets Enhance CO 2 Electrochemical Reduction to CO
    journal, April 2018

    • Geng, Zhigang; Kong, Xiangdong; Chen, Weiwei
    • Angewandte Chemie, Vol. 130, Issue 21
    • DOI: 10.1002/ange.201711255

    Theoretical investigation of various aspects of two dimensional holey boroxine, B 3 O 3
    journal, January 2019

    • Ullah, Saif; Denis, Pablo A.; Sato, Fernando
    • RSC Advances, Vol. 9, Issue 64
    • DOI: 10.1039/c9ra07338h

    Quick Optical Identification of the Defect Formation in Monolayer WSe2 for Growth Optimization
    journal, August 2019


    Regulating p-block metals in perovskite nanodots for efficient electrocatalytic water oxidation
    journal, October 2017


    Wafer-scale synthesis of ultrathin CoO nanosheets with enhanced electrochemical catalytic properties
    journal, January 2017

    • Wang, Fei; Yu, Yanhao; Yin, Xin
    • Journal of Materials Chemistry A, Vol. 5, Issue 19
    • DOI: 10.1039/c7ta01857f

    Colloidally synthesized defect-rich $$\hbox {MoSe}_{2}$$ MoSe 2 nanosheets for superior catalytic activity
    journal, March 2019

    • Hassan, Md Samim; Jana, Atanu; Gahlawat, Soniya
    • Bulletin of Materials Science, Vol. 42, Issue 2
    • DOI: 10.1007/s12034-019-1774-8

    An Efficient and Extremely Stable Photocatalytic PtSe 2 /FTO Thin Film for Water Splitting
    journal, September 2019


    Dual-Functional N Dopants in Edges and Basal Plane of MoS 2 Nanosheets Toward Efficient and Durable Hydrogen Evolution
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    • Xiao, Wen; Liu, Peitao; Zhang, Jingyan
    • Advanced Energy Materials, Vol. 7, Issue 7
    • DOI: 10.1002/aenm.201602086

    Hierarchical Nanoboxes Composed of Co 9 S 8 −MoS 2 Nanosheets as Efficient Electrocatalysts for the Hydrogen Evolution Reaction
    journal, January 2018

    • Ganesan, Vinoth; Lim, Sunghyun; Kim, Jinkwon
    • Chemistry - An Asian Journal, Vol. 13, Issue 4
    • DOI: 10.1002/asia.201701536

    Phase engineering of a multiphasic 1T/2H MoS 2 catalyst for highly efficient hydrogen evolution
    journal, January 2017

    • Wang, Dezhi; Zhang, Xiangyong; Bao, Siyuan
    • Journal of Materials Chemistry A, Vol. 5, Issue 6
    • DOI: 10.1039/c6ta09409k

    Enhancing potassium-ion battery performance by defect and interlayer engineering
    journal, January 2019

    • Xu, Yang; Bahmani, Farzaneh; Zhou, Min
    • Nanoscale Horizons, Vol. 4, Issue 1
    • DOI: 10.1039/c8nh00305j

    Confined Catalysis: Progress and Prospects in Energy Conversion
    journal, September 2019

    • Shifa, Tofik Ahmed; Vomiero, Alberto
    • Advanced Energy Materials, Vol. 9, Issue 40
    • DOI: 10.1002/aenm.201902307

    Activating MoS 2 basal planes for hydrogen evolution through direct CVD morphology control
    journal, January 2019

    • Dong, Lianqing; Guo, Shaoqiang; Wang, Yuyan
    • Journal of Materials Chemistry A, Vol. 7, Issue 48
    • DOI: 10.1039/c9ta08738a

    Promoting the electroreduction of CO 2 with oxygen vacancies on a plasma-activated SnO x /carbon foam monolithic electrode
    journal, January 2020

    • Li, Hongqiang; Xiao, Nan; Wang, Yuwei
    • Journal of Materials Chemistry A, Vol. 8, Issue 4
    • DOI: 10.1039/c9ta12401b

    Tuning the electronic and magnetic properties of MoS 2 nanotubes with vacancy defects
    journal, January 2019

    • Yang, Yanmei; Liu, Yang; Man, Baoyuan
    • RSC Advances, Vol. 9, Issue 30
    • DOI: 10.1039/c8ra08981g

    Vertically conductive MoS 2 pyramids with a high density of active edge sites for efficient hydrogen evolution
    journal, January 2020

    • Zhou, Qingwei; Su, Shaoqiang; Cheng, Pengfei
    • Journal of Materials Chemistry C, Vol. 8, Issue 9
    • DOI: 10.1039/c9tc05872a

    Recent Progress on Irradiation-Induced Defect Engineering of Two-Dimensional 2H-MoS2 Few Layers
    journal, February 2019

    • Zhao, Guang-Yi; Deng, Hua; Tyree, Nathaniel
    • Applied Sciences, Vol. 9, Issue 4
    • DOI: 10.3390/app9040678

    Engineering two-dimensional metal oxides via surface functionalization for biological applications
    journal, January 2020

    • Ren, Baiyu; Wang, Yichao; Ou, Jian Zhen
    • Journal of Materials Chemistry B, Vol. 8, Issue 6
    • DOI: 10.1039/c9tb02423a

    Alloy Foam‐Derived Ni 0.86 Fe 2.14 O 4 Hexagonal Plates as an Efficient Electrochemical Catalyst for the Oxygen Evolution Reaction
    journal, January 2020


    Probing the active sites of newly predicted stable Janus scandium dichalcogenides for photocatalytic water-splitting
    journal, January 2019

    • Yang, Xiaoyong; Banerjee, Amitava; Ahuja, Rajeev
    • Catalysis Science & Technology, Vol. 9, Issue 18
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    Substrate screening effects on the quasiparticle band gap and defect charge transition levels in MoS 2
    journal, August 2018


    Solution-phase phosphorus substitution for enhanced oxygen evolution reaction in Cu 2 WS 4
    journal, January 2019

    • Novak, Travis G.; Prakash, Om; Tiwari, Anand P.
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    Nanocatalysts for hydrogen evolution reactions
    journal, January 2018

    • Ojha, Kasinath; Saha, Soumen; Dagar, Preeti
    • Physical Chemistry Chemical Physics, Vol. 20, Issue 10
    • DOI: 10.1039/c7cp06316d

    Photoemission spectroscopy study of structural defects in molybdenum disulfide (MoS 2 ) grown by chemical vapor deposition (CVD)
    journal, January 2019

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    • Chemical Communications, Vol. 55, Issue 70
    • DOI: 10.1039/c9cc01577a

    Enhancing the electrocatalytic activity of 2H-WS 2 for hydrogen evolution via defect engineering
    journal, January 2019

    • Wu, Longfei; van Hoof, Arno J. F.; Dzade, Nelson Y.
    • Physical Chemistry Chemical Physics, Vol. 21, Issue 11
    • DOI: 10.1039/c9cp00722a

    WS 2 Nanosheets with Highly‐Enhanced Electrochemical Activity by Facile Control of Sulfur Vacancies
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    State-of-the-Art Advances and Perspectives for Electrocatalysis
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    Direct deposition of MoSe 2 nanocrystals onto conducting substrates: towards ultra-efficient electrocatalysts for hydrogen evolution
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    • Damien, Dijo; Anil, Athira; Chatterjee, Dipanwita
    • Journal of Materials Chemistry A, Vol. 5, Issue 26
    • DOI: 10.1039/c6ta09645j

    Structural Engineering of 2D Nanomaterials for Energy Storage and Catalysis
    journal, February 2018


    Synergetic Exfoliation and Lateral Size Engineering of MoS 2 for Enhanced Photocatalytic Hydrogen Generation
    journal, March 2018


    Structurally Deformed MoS 2 for Electrochemically Stable, Thermally Resistant, and Highly Efficient Hydrogen Evolution Reaction
    journal, October 2017


    Heterostructure engineering of Co-doped MoS 2 coupled with Mo 2 CT x MXene for enhanced hydrogen evolution in alkaline media
    journal, January 2019

    • Liang, Junmei; Ding, Chaoying; Liu, Jiapeng
    • Nanoscale, Vol. 11, Issue 22
    • DOI: 10.1039/c9nr02085c

    Direct Synthesis of Large-Area 2D Mo 2 C on In Situ Grown Graphene
    journal, July 2017

    • Geng, Dechao; Zhao, Xiaoxu; Chen, Zhongxin
    • Advanced Materials, Vol. 29, Issue 35
    • DOI: 10.1002/adma.201700072

    Composite electrocatalyst MoxW1-xS2 nanosheets on carbon fiber paper for highly efficient hydrogen evolution reaction
    journal, June 2018

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    • DOI: 10.1007/s10008-018-3991-2

    A bifunctional electrode engineered by sulfur vacancies for efficient electrocatalysis
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    Emerging two-dimensional nanomaterials for electrochemical hydrogen evolution
    journal, January 2017

    • Chen, Yunxu; Yang, Kena; Jiang, Bei
    • Journal of Materials Chemistry A, Vol. 5, Issue 18
    • DOI: 10.1039/c7ta00816c

    Highly Periodic Metal Dichalcogenide Nanostructures with Complex Shapes, High Resolution, and High Aspect Ratios
    journal, October 2017

    • Jang, Sungwoo; Kim, Seon Joon; Koh, Hyeong-Jun
    • Advanced Functional Materials, Vol. 27, Issue 46
    • DOI: 10.1002/adfm.201703842

    Graphene Nanoarchitectonics: Recent Advances in Graphene‐Based Electrocatalysts for Hydrogen Evolution Reaction
    journal, September 2019


    Design, synthesis, and energy-related applications of metal sulfides
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    • Liu, Yongchang; Li, Yang; Kang, Hongyan
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    • DOI: 10.1039/c6mh00075d

    Theoretical investigation on the hydrogen evolution reaction mechanism at MoS 2 heterostructures: the essential role of the 1T/2H phase interface
    journal, January 2020

    • Zhang, Tian; Zhu, Houyu; Guo, Chen
    • Catalysis Science & Technology, Vol. 10, Issue 2
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    Nanostructured Metal Chalcogenides for Energy Storage and Electrocatalysis
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    • Zhang, Yu; Zhou, Qian; Zhu, Jixin
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    Oxygen Evolution Reaction on 2D Ferromagnetic Fe 3 GeTe 2 : Boosting the Reactivity by the Self‐Reduction of Surface Hydroxyl
    journal, August 2019

    • Zhao, Yinghe; Gu, Jinxing; Chen, Zhongfang
    • Advanced Functional Materials, Vol. 29, Issue 44
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    Template‐Assisted Synthesis of Metallic 1T′‐Sn 0.3 W 0.7 S 2 Nanosheets for Hydrogen Evolution Reaction
    journal, November 2019

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    • Advanced Functional Materials, Vol. 30, Issue 5
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    Unveiling Active Sites for the Hydrogen Evolution Reaction on Monolayer MoS 2
    journal, September 2017


    Nanoarchitectonics for Transition‐Metal‐Sulfide‐Based Electrocatalysts for Water Splitting
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    Probing the Electronic Properties of Monolayer MoS 2 via Interaction with Molecular Hydrogen
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    Engineered MoSe 2 -Based Heterostructures for Efficient Electrochemical Hydrogen Evolution Reaction
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    • Advanced Energy Materials, Vol. 8, Issue 16
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    Metallic Twin Boundaries Boost the Hydrogen Evolution Reaction on the Basal Plane of Molybdenum Selenotellurides
    journal, April 2018

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    Doped-MoSe 2 Nanoflakes/3d Metal Oxide-Hydr(Oxy)Oxides Hybrid Catalysts for pH-Universal Electrochemical Hydrogen Evolution Reaction
    journal, August 2018

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    Benchmarking the Activity, Stability, and Inherent Electrochemistry of Amorphous Molybdenum Sulfide for Hydrogen Production
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    Single Atoms and Clusters Based Nanomaterials for Hydrogen Evolution, Oxygen Evolution Reactions, and Full Water Splitting
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    Activation of MoS 2 Basal Planes for Hydrogen Evolution by Zinc
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    Oxygen Vacancies in ZnO Nanosheets Enhance CO 2 Electrochemical Reduction to CO
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    Enhanced Raman and photoluminescence response in monolayer MoS 2 due to laser healing of defects: Enhanced Raman and photoluminescence response
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    Conductive Molybdenum Sulfide for Efficient Electrocatalytic Hydrogen Evolution
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    Extending the Colloidal Transition Metal Dichalcogenide Library to ReS 2 Nanosheets for Application in Gas Sensing and Electrocatalysis
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    Incorporation of active phase in porous MoS2 for enhanced hydrogen evolution reaction
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    Hydrogen adsorption engineering by intramolecular proton transfer on 2D nanosheets
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    Colloidal synthesis of VSe 2 single-layer nanosheets as novel electrocatalysts for the hydrogen evolution reaction
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    Electrocatalysis of layered Group 5 metallic transition metal dichalcogenides (MX 2 , M = V, Nb, and Ta; X = S, Se, and Te)
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    Magnetism in monolayer 1T-MoS 2 and 1T-MoS 2 H tuned by strain
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    Computational screening for high-activity MoS 2 monolayer-based catalysts for the oxygen reduction reaction via substitutional doping with transition metal
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    • Wang, Zhongxu; Zhao, Jingxiang; Cai, Qinghai
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    Engineering of transition metal dichalcogenide-based 2D nanomaterials through doping for environmental applications
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    Structural and electronic properties of hydrogenated GaBi and InBi honeycomb monolayers with point defects
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    Carbon nanotube-induced phase and stability engineering: a strained cobalt-doped WSe 2 /MWNT heterostructure for enhanced hydrogen evolution reaction
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    • Journal of Materials Chemistry A, Vol. 6, Issue 11
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    Engineering the nanostructure of molybdenum nitride nanodot embedded N-doped porous hollow carbon nanochains for rapid all pH hydrogen evolution
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    • Wang, Min-Qiang; Tang, Chun; Ye, Cui
    • Journal of Materials Chemistry A, Vol. 6, Issue 30
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    Microwave-assisted synthesis of group 5 transition metal dichalcogenide thin films
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    • Kwak, Junghyeok; Jung, Sunshin; Lee, Noho
    • Journal of Materials Chemistry C, Vol. 6, Issue 42
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    Porous aluminum electrodes with 3D channels and zig-zag edges for efficient hydrogen evolution
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    Applications of nano-porous graphene materials – critical review on performance and challenges
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    Recent advances in two-dimensional materials and their nanocomposites in sustainable energy conversion applications
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    1% defect enriches MoS 2 quantum dot: catalysis and blue luminescence
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    Revealing the nature of active sites in electrocatalysis
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    • Garlyyev, Batyr; Fichtner, Johannes; Piqué, Oriol
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    Interfacial aspect of ZnTe/In 2 Te 3 heterostructures as an efficient catalyst for the hydrogen evolution reaction
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    2D coordination polymers: Design guidelines and materials perspective
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    Revealing the microscopic CVD growth mechanism of MoSe 2 and the role of hydrogen gas during the growth procedure
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    Single-layer 1 T ′-MoS 2 under electron irradiation from ab initio molecular dynamics
    journal, March 2018


    Recent progress in plasma-assisted synthesis and modification of 2D materials
    journal, April 2018


    Novel Pd 2 Se 3 Two-Dimensional Phase Driven by Interlayer Fusion in Layered PdSe 2
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    Carbon-Based Photocathode Materials for Solar Hydrogen Production
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    Multiscale structural and electronic control of molybdenum disulfide foam for highly efficient hydrogen production
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    Electrochemical generation of sulfur vacancies in the basal plane of MoS2 for hydrogen evolution
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    Non-equilibrium fractal growth of MoS 2 for electrocatalytic hydrogen evolution
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    In situ synthesis of MoS 2 /graphene nanosheets as free-standing and flexible electrode paper for high-efficiency hydrogen evolution reaction
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    Superhydrophobic states of 2D nanomaterials controlled by atomic defects can modulate cell adhesion
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    MoC based Mott–Schottky electrocatalyst for boosting the hydrogen evolution reaction performance
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    Mo 2 C/graphene heterostructures: low temperature chemical vapor deposition on liquid bimetallic Sn–Cu and hydrogen evolution reaction electrocatalytic properties
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    Polypyrrole coated niobium disulfide nanowires as high performance electrocatalysts for hydrogen evolution reaction
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    Prevention of Hydrogen Damage Using MoS2 Coating on Iron Surface
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