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Title: The influence of hold time on the onset of plastic deformation in silicon

Abstract

Here, the formation of silicon (Si) in its -Sn form is known to be nucleation limited, with an undetermined period of time between when critical pressure for the trans- formation is reached and when the transformation actually occurs. In this letter, we use nanoindentation to apply critical pressure to diamond cubic Si and hold the sample under pressure to promote deformation via phase transformation and crystalline defects. We report that the number of indents in which phase transformation is observed increases with increasing hold time. Interestingly, the number of indents in which crystalline defects are observed also increase with increasing hold time, suggesting crystalline defects are also nucleation limited. Raman spectroscopy and cross-sectional transmission electron microscopy is used to show that these two deformation mechanisms are mutually exclusive under the indentation conditions used within this letter.

Authors:
 [1];  [2];  [3];  [3]
  1. Australian National Univ., Canberra (Australia)
  2. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  3. Australian National Univ. Canberra (Australia)
Publication Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE Office of Science (SC)
OSTI Identifier:
1237634
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Applied Physics
Additional Journal Information:
Journal Volume: 118; Journal Issue: 24; Journal ID: ISSN 0021-8979
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; hydrostatics; nucleation; dislocations; Raman spectra; nanotechnology

Citation Formats

Wong, Sherman, Haberl, Bianca, Bradby, Jodie E., and Williams, James S. The influence of hold time on the onset of plastic deformation in silicon. United States: N. p., 2015. Web. doi:10.1063/1.4938480.
Wong, Sherman, Haberl, Bianca, Bradby, Jodie E., & Williams, James S. The influence of hold time on the onset of plastic deformation in silicon. United States. https://doi.org/10.1063/1.4938480
Wong, Sherman, Haberl, Bianca, Bradby, Jodie E., and Williams, James S. Thu . "The influence of hold time on the onset of plastic deformation in silicon". United States. https://doi.org/10.1063/1.4938480. https://www.osti.gov/servlets/purl/1237634.
@article{osti_1237634,
title = {The influence of hold time on the onset of plastic deformation in silicon},
author = {Wong, Sherman and Haberl, Bianca and Bradby, Jodie E. and Williams, James S.},
abstractNote = {Here, the formation of silicon (Si) in its -Sn form is known to be nucleation limited, with an undetermined period of time between when critical pressure for the trans- formation is reached and when the transformation actually occurs. In this letter, we use nanoindentation to apply critical pressure to diamond cubic Si and hold the sample under pressure to promote deformation via phase transformation and crystalline defects. We report that the number of indents in which phase transformation is observed increases with increasing hold time. Interestingly, the number of indents in which crystalline defects are observed also increase with increasing hold time, suggesting crystalline defects are also nucleation limited. Raman spectroscopy and cross-sectional transmission electron microscopy is used to show that these two deformation mechanisms are mutually exclusive under the indentation conditions used within this letter.},
doi = {10.1063/1.4938480},
journal = {Journal of Applied Physics},
number = 24,
volume = 118,
place = {United States},
year = {Thu Dec 24 00:00:00 EST 2015},
month = {Thu Dec 24 00:00:00 EST 2015}
}

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Works referencing / citing this record:

Origin of a Nanoindentation Pop-in Event in Silicon Crystal
journal, March 2017


Nanoindentation Induced Deformation and Pop-in Events in a Silicon Crystal: Molecular Dynamics Simulation and Experiment
journal, August 2017