Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials
Abstract
Within a high-pressure environment, crystal deformation is controlled by complex processes such as dislocation motion, twinning, and phase transitions, which change materials’ microscopic morphology and alter their properties. Understanding a crystal’s response to external stress provides a unique opportunity for rational tailoring of its functionalities. It is very challenging to track the strain evolution and physical deformation from a single nanoscale crystal under high-pressure stress. Here, we report an in situ three-dimensional mapping of morphology and strain evolutions in a single-crystal silver nanocube within a high-pressure environment using the Bragg Coherent Diffractive Imaging (CDI) method. We observed a continuous lattice distortion, followed by a deformation twining process at a constant pressure. As a result, the ability to visualize stress-introduced deformation of nanocrystals with high spatial resolution and prominent strain sensitivity provides an important route for interpreting and engineering novel properties of nanomaterials.
- Authors:
-
- Brookhaven National Lab. (BNL), Upton, NY (United States); Argonne National Lab. (ANL), Argonne, IL (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States); Center for High Pressure Science and Technology Advanced Research, Shanghai (China)
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Univ. College London, Bloomsbury (United Kingdom); Research Complex at Harwell, Didcot (United Kingdom)
- Center for High Pressure Science and Technology Advanced Research, Shanghai (China)
- Publication Date:
- Research Org.:
- Brookhaven National Laboratory (BNL), Upton, NY (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1237176
- Alternate Identifier(s):
- OSTI ID: 1237177; OSTI ID: 1340331
- Report Number(s):
- BNL-108436-2015-JA; BNL-108437-2015-JA; BNL-111705-2016-JA
Journal ID: ISSN 1530-6984; R&D Project: LS001
- Grant/Contract Number:
- SC00112704
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Nano Letters
- Additional Journal Information:
- Journal Volume: 15; Journal Issue: 11; Journal ID: ISSN 1530-6984
- Publisher:
- American Chemical Society
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; nanocrystal; deformation twinning; coherent diffraction imaging; X-ray imaging; coherent diffractive imaging; 77 NANOSCIENCE AND NANOTECHNOLOGY
Citation Formats
Huang, X. J., Yang, W. G., Harder, R., Sun, Y., Lu, M., Chu, Y. S., Robinson, I. K., and Mao, H. K. Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials. United States: N. p., 2015.
Web. doi:10.1021/acs.nanolett.5b03568.
Huang, X. J., Yang, W. G., Harder, R., Sun, Y., Lu, M., Chu, Y. S., Robinson, I. K., & Mao, H. K. Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials. United States. https://doi.org/10.1021/acs.nanolett.5b03568
Huang, X. J., Yang, W. G., Harder, R., Sun, Y., Lu, M., Chu, Y. S., Robinson, I. K., and Mao, H. K. Tue .
"Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials". United States. https://doi.org/10.1021/acs.nanolett.5b03568. https://www.osti.gov/servlets/purl/1237176.
@article{osti_1237176,
title = {Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials},
author = {Huang, X. J. and Yang, W. G. and Harder, R. and Sun, Y. and Lu, M. and Chu, Y. S. and Robinson, I. K. and Mao, H. K.},
abstractNote = {Within a high-pressure environment, crystal deformation is controlled by complex processes such as dislocation motion, twinning, and phase transitions, which change materials’ microscopic morphology and alter their properties. Understanding a crystal’s response to external stress provides a unique opportunity for rational tailoring of its functionalities. It is very challenging to track the strain evolution and physical deformation from a single nanoscale crystal under high-pressure stress. Here, we report an in situ three-dimensional mapping of morphology and strain evolutions in a single-crystal silver nanocube within a high-pressure environment using the Bragg Coherent Diffractive Imaging (CDI) method. We observed a continuous lattice distortion, followed by a deformation twining process at a constant pressure. As a result, the ability to visualize stress-introduced deformation of nanocrystals with high spatial resolution and prominent strain sensitivity provides an important route for interpreting and engineering novel properties of nanomaterials.},
doi = {10.1021/acs.nanolett.5b03568},
journal = {Nano Letters},
number = 11,
volume = 15,
place = {United States},
year = {Tue Oct 20 00:00:00 EDT 2015},
month = {Tue Oct 20 00:00:00 EDT 2015}
}
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