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Title: Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability

Abstract

We discuss techniques for performing continuous measurements across a wide range of pressure-field-temperature phase space, combining the milli-Kelvin temperatures of a helium dilution refrigerator with that of the giga-Pascal pressures of a diamond anvil cell and the Tesla magnetic fields of a superconducting magnet. With a view towards minimizing remnant magnetic fields and background magnetic susceptibility, we then characterize high-strength superalloy materials for the pressure cell assembly, which allows high fidelity measurements of low-field phenomena such as superconductivity below 100 mK at pressures above 10 GPa. In situ tunability and measurement of the pressure permit experiments over a wide range of pressure, while at the same time making possible precise steps across abrupt phase transitions such as that from insulator to metal.

Authors:
 [1];  [1];  [2];  [1];  [3];  [4];  [5];  [6]
+ Show Author Affiliations
  1. Univ. of Chicago, IL (United States)
  2. Univ. of Chicago, IL (United States); Argonne National Lab. (ANL), Argonne, IL (United States)
  3. Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States)
  4. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  5. Argonne National Lab. (ANL), Argonne, IL (United States)
  6. Univ. of Chicago, IL (United States); California Inst. of Technology (CalTech), Pasadena, CA (United States)
Publication Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE Office of Science (SC)
OSTI Identifier:
1224169
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 86; Journal Issue: 9; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION; 36 MATERIALS SCIENCE; High Pressure; Diamond Anvil Cell; Low temperature

Citation Formats

Palmer, Alexander, Silevitch, Daniel, Feng, Yejun, Wang, Yishu, Jaramillo, R., Banerjee, Arnab, Ren, Yang, and Rosenbaum, Thomas F. Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability. United States: N. p., 2015. Web. doi:10.1063/1.4929861.
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Palmer, Alexander, Silevitch, Daniel, Feng, Yejun, Wang, Yishu, Jaramillo, R., Banerjee, Arnab, Ren, Yang, & Rosenbaum, Thomas F. Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability. United States. doi:10.1063/1.4929861.
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Palmer, Alexander, Silevitch, Daniel, Feng, Yejun, Wang, Yishu, Jaramillo, R., Banerjee, Arnab, Ren, Yang, and Rosenbaum, Thomas F. Fri . "Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability". United States. doi:10.1063/1.4929861. https://www.osti.gov/servlets/purl/1224169.
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@article{osti_1224169,
title = {Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability},
author = {Palmer, Alexander and Silevitch, Daniel and Feng, Yejun and Wang, Yishu and Jaramillo, R. and Banerjee, Arnab and Ren, Yang and Rosenbaum, Thomas F.},
abstractNote = {We discuss techniques for performing continuous measurements across a wide range of pressure-field-temperature phase space, combining the milli-Kelvin temperatures of a helium dilution refrigerator with that of the giga-Pascal pressures of a diamond anvil cell and the Tesla magnetic fields of a superconducting magnet. With a view towards minimizing remnant magnetic fields and background magnetic susceptibility, we then characterize high-strength superalloy materials for the pressure cell assembly, which allows high fidelity measurements of low-field phenomena such as superconductivity below 100 mK at pressures above 10 GPa. In situ tunability and measurement of the pressure permit experiments over a wide range of pressure, while at the same time making possible precise steps across abrupt phase transitions such as that from insulator to metal.},
doi = {10.1063/1.4929861},
journal = {Review of Scientific Instruments},
number = 9,
volume = 86,
place = {United States},
year = {2015},
month = {9}
}
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DOI:  10.1063/1.4929861
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