New developments in micro-X-ray diffraction and X-ray absorption spectroscopy for high-pressure research at 16-BM-D at the Advanced Photon Source
Abstract
We report the monochromator and focusing mirrors of the 16-BM-D beamline, which is dedicated to high-pressure research with micro-X-ray diffraction (micro-XRD) and X-ray absorption near edge structure (XANES) (6-45 keV) spectroscopy, have been recently upgraded. Monochromatic X-rays are selected by a Si (111) double-crystal monochromator operated in an artificial channel-cut mode and focused to 5 μm × 5 μm (FWHM) by table-top Kirkpatrick-Baez type mirrors located near the sample stage. The typical X-ray flux is ~5 × 108 photons/s at 30 keV. The instrumental resolution, Δq/qmax, reaches to 2 × 10–3 and is tunable through adjustments of the detector distance and X-ray energy. The setup is stable and reproducible, which allows versatile application to various types of experiments including resistive heating and cryogenic cooling as well as ambient temperature compression. Transmission XANES is readily combined with micro-XRD utilizing the fixed-exit feature of the monochromator, which allows combined XRD-XANES measurements at a given sample condition.
- Authors:
-
[1];
[1];
- Carnegie Inst. of Washington, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT)
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF)
- OSTI Identifier:
- 1203738
- Alternate Identifier(s):
- OSTI ID: 1228693
- Grant/Contract Number:
- NA0001974; FG02-99ER45775; EAR-1128799; FG02-94ER14466; AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Volume: 86; Journal Issue: 7; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- ENGLISH
- Subject:
- 47 OTHER INSTRUMENTATION; Raman spectroscopy; Detectors; Diffractometers; Mechanical instruments; Crystal monochromators; Thermodynamic states and processes; Ionization chambers; X-ray absorption spectroscopy; Diamond anvil cells; X-ray diffraction
Citation Formats
Park, Changyong, Popov, Dmitry, Ikuta, Daijo, Lin, Chuanlong, Kenney-Benson, Curtis, Rod, Eric, Bommannavar, Arunkumar, and Shen, Guoyin. New developments in micro-X-ray diffraction and X-ray absorption spectroscopy for high-pressure research at 16-BM-D at the Advanced Photon Source. United States: N. p., 2015.
Web. doi:10.1063/1.4926893.
Park, Changyong, Popov, Dmitry, Ikuta, Daijo, Lin, Chuanlong, Kenney-Benson, Curtis, Rod, Eric, Bommannavar, Arunkumar, & Shen, Guoyin. New developments in micro-X-ray diffraction and X-ray absorption spectroscopy for high-pressure research at 16-BM-D at the Advanced Photon Source. United States. https://doi.org/10.1063/1.4926893
Park, Changyong, Popov, Dmitry, Ikuta, Daijo, Lin, Chuanlong, Kenney-Benson, Curtis, Rod, Eric, Bommannavar, Arunkumar, and Shen, Guoyin. Tue .
"New developments in micro-X-ray diffraction and X-ray absorption spectroscopy for high-pressure research at 16-BM-D at the Advanced Photon Source". United States. https://doi.org/10.1063/1.4926893. https://www.osti.gov/servlets/purl/1203738.
@article{osti_1203738,
title = {New developments in micro-X-ray diffraction and X-ray absorption spectroscopy for high-pressure research at 16-BM-D at the Advanced Photon Source},
author = {Park, Changyong and Popov, Dmitry and Ikuta, Daijo and Lin, Chuanlong and Kenney-Benson, Curtis and Rod, Eric and Bommannavar, Arunkumar and Shen, Guoyin},
abstractNote = {We report the monochromator and focusing mirrors of the 16-BM-D beamline, which is dedicated to high-pressure research with micro-X-ray diffraction (micro-XRD) and X-ray absorption near edge structure (XANES) (6-45 keV) spectroscopy, have been recently upgraded. Monochromatic X-rays are selected by a Si (111) double-crystal monochromator operated in an artificial channel-cut mode and focused to 5 μm × 5 μm (FWHM) by table-top Kirkpatrick-Baez type mirrors located near the sample stage. The typical X-ray flux is ~5 × 108 photons/s at 30 keV. The instrumental resolution, Δq/qmax, reaches to 2 × 10–3 and is tunable through adjustments of the detector distance and X-ray energy. The setup is stable and reproducible, which allows versatile application to various types of experiments including resistive heating and cryogenic cooling as well as ambient temperature compression. Transmission XANES is readily combined with micro-XRD utilizing the fixed-exit feature of the monochromator, which allows combined XRD-XANES measurements at a given sample condition.},
doi = {10.1063/1.4926893},
journal = {Review of Scientific Instruments},
number = 7,
volume = 86,
place = {United States},
year = {Tue Jul 21 00:00:00 EDT 2015},
month = {Tue Jul 21 00:00:00 EDT 2015}
}
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