Superconductivity versus structural phase transition in the closely related Bi2Rh3.5S2 and Bi2Rh3S2

Kaluarachchi, Udhara S.; Xie, Weiwei; Lin, Qisheng; Taufour, Valentin; Bud'ko, Sergey L.; Miller, Gordon J.; Canfield, Paul C.

doi:10.1103/PhysRevB.91.174513

Title: Superconductivity versus structural phase transition in the closely related Bi₂Rh_3.5S₂ and Bi₂Rh₃S₂

Abstract

Single crystals of Bi₂Rh₃S₂ and Bi₂Rh_3.5S₂ were synthesized by solution growth, and the crystal structures and thermodynamic and transport properties of both compounds were studied. In the case of Bi₂Rh₃S₂, a structural first-order transition at around 165 K is identified by single-crystal diffraction experiments, with clear signatures visible in resistivity, magnetization, and specific heat data. No superconducting transition for Bi₂Rh₃S₂ was observed down to 0.5 K. In contrast, no structural phase transition at high temperature was observed for Bi₂Rh_3.5S₂; however, bulk superconductivity with a critical temperature, T_c ≈ 1.7 K, was observed. The Sommerfeld coefficient γ and the Debye temperature (Θ_D) were found to be 9.41 mJ mol^–1K^–2 and 209 K, respectively, for Bi₂Rh₃S₂, and 22 mJ mol^–1K^–2 and 196 K, respectively, for Bi₂Rh_3.5S₂. As a result, the study of the specific heat in the superconducting state of Bi₂Rh_3.5S₂ suggests that Bi₂Rh_3.5S₂ is a weakly coupled, BCS superconductor.

Authors:

Kaluarachchi, Udhara S. ^[1]; Xie, Weiwei ^[1]; Lin, Qisheng ^[1]; Taufour, Valentin ^[1]; Bud'ko, Sergey L. ^[1]; Miller, Gordon J. ^[1]; Canfield, Paul C. ^[1]

Iowa State Univ., Ames, IA (United States)

Publication Date:: Tue May 19 00:00:00 EDT 2015

Research Org.:: Ames Laboratory (AMES), Ames, IA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1227310

Alternate Identifier(s):: OSTI ID: 1182334

Report Number(s):: IS-J-8643
Journal ID: ISSN 1098-0121; PRBMDO

Grant/Contract Number:: FA9550-09-1-0603; AC02-07CH11358

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review. B, Condensed Matter and Materials Physics

Additional Journal Information:: Journal Volume: 91; Journal Issue: 17; Journal ID: ISSN 1098-0121

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Kaluarachchi, Udhara S., Xie, Weiwei, Lin, Qisheng, Taufour, Valentin, Bud'ko, Sergey L., Miller, Gordon J., and Canfield, Paul C. Superconductivity versus structural phase transition in the closely related Bi2Rh3.5S2 and Bi2Rh3S2.  United States: N. p., 2015. 
Web.  doi:10.1103/PhysRevB.91.174513.

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                    Kaluarachchi, Udhara S., Xie, Weiwei, Lin, Qisheng, Taufour, Valentin, Bud'ko, Sergey L., Miller, Gordon J., & Canfield, Paul C. Superconductivity versus structural phase transition in the closely related Bi2Rh3.5S2 and Bi2Rh3S2.  United States.  https://doi.org/10.1103/PhysRevB.91.174513

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                    Kaluarachchi, Udhara S., Xie, Weiwei, Lin, Qisheng, Taufour, Valentin, Bud'ko, Sergey L., Miller, Gordon J., and Canfield, Paul C. Tue .  
"Superconductivity versus structural phase transition in the closely related Bi2Rh3.5S2 and Bi2Rh3S2".  United States.  https://doi.org/10.1103/PhysRevB.91.174513.  https://www.osti.gov/servlets/purl/1227310.

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@article{osti_1227310,

  title        = {Superconductivity versus structural phase transition in the closely related Bi2Rh3.5S2 and Bi2Rh3S2},

  author       = {Kaluarachchi, Udhara S. and Xie, Weiwei and Lin, Qisheng and Taufour, Valentin and Bud'ko, Sergey L. and Miller, Gordon J. and Canfield, Paul C.},

  abstractNote = {Single crystals of Bi2Rh3S2 and Bi2Rh3.5S2 were synthesized by solution growth, and the crystal structures and thermodynamic and transport properties of both compounds were studied. In the case of Bi2Rh3S2, a structural first-order transition at around 165 K is identified by single-crystal diffraction experiments, with clear signatures visible in resistivity, magnetization, and specific heat data. No superconducting transition for Bi2Rh3S2 was observed down to 0.5 K. In contrast, no structural phase transition at high temperature was observed for Bi2Rh3.5S2; however, bulk superconductivity with a critical temperature, Tc ≈ 1.7 K, was observed. The Sommerfeld coefficient γ and the Debye temperature (ΘD) were found to be 9.41 mJ mol–1K–2 and 209 K, respectively, for Bi2Rh3S2, and 22 mJ mol–1K–2 and 196 K, respectively, for Bi2Rh3.5S2. As a result, the study of the specific heat in the superconducting state of Bi2Rh3.5S2 suggests that Bi2Rh3.5S2 is a weakly coupled, BCS superconductor.},

  doi          = {10.1103/PhysRevB.91.174513},

  journal      = {Physical Review. B, Condensed Matter and Materials Physics},

  number       = 17,

  volume       = 91,

  place        = {United States},

  year         = {Tue May 19 00:00:00 EDT 2015},

  month        = {Tue May 19 00:00:00 EDT 2015}

}

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Works referencing / citing this record:

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples
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Canfield, Paul C.; Kong, Tai; Kaluarachchi, Udhara S.
Philosophical Magazine, Vol. 96, Issue 1
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Superconducting and charge density wave transition in single crystalline LaPt ₂ Si ₂
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New materials physics
journal, November 2019

Canfield, Paul C.
Reports on Progress in Physics, Vol. 83, Issue 1
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Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples
text, January 2015

Canfield, Paul C.; Kong, Tai; Kaluarachchi, Udhara S.
arXiv
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Title: Superconductivity versus structural phase transition in the closely related Bi2Rh3.5S2 and Bi2Rh3S2

Abstract

Citation Formats

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On the theory of superconductivity: the one-dimensional case journal, May 1954

Theory of Superconductivity journal, December 1957

Superconductors with charge- and spin-density waves: theory and experiment (Review) journal, May 2000

Charge- and spin-density-wave superconductors journal, March 2001

Charge-Density Waves in Metallic, Layered, Transition-Metal Dichalcogenides journal, April 1974

Heat capacity of 2HNbSe2 at the charge density wave transition journal, August 1975

Electric Field Breakdown of Charge-Density-Wave—Induced Anomalies in Nb Se 3 journal, September 1976

Electronic properties and superlattice formation in the semimetal TiSe 2 journal, November 1976

Electronic phase transition and partially gapped Fermi surface in superconducting Lu 5 Ir 4 Si 10 journal, October 1986

Strongly coupled charge-density wave transition in single-crystal Lu 5 Ir 4 Si 10 journal, March 1999

Novel charge density wave transition in crystals of R5Ir4Si10 journal, May 2002

Phase transitions in Lu 2 Ir 3 Si 5 journal, January 2005

Superconductivity in CuxTiSe2 journal, July 2006

Synthesis and electrical properties of shandite-parkerite phases, A2M3Ch2 journal, March 1988

Superconductivity in ternary chalcogenides Bi 2 Ni 3 X 2 (X = S, Se) journal, April 2006

Transport properties in normal-metal Bi 2 Pd 3 S 2 and superconducting Bi 2 Pd 3 Se 2 journal, July 2008

Development of viable solutions for the synthesis of sulfur bearing single crystals journal, July 2012

Charge-density-wave superconductor Bi 2 Rh 3 Se 2 journal, February 2007

Pressure effect and electron diffraction on the anomalous transition in ternary superconductor Bi2Rh3Se2 journal, January 2014

Pressure effect on the charge-density-wave formation in 2 H − N b Se 2 and correlation between structural instabilities and superconductivity in unstable solids journal, February 1977

Charge density wave formation, superconductivity and Fermi surface determination in NbSe 3 : a pressure study journal, April 1980

Effect of pressure and chemical substitutions on the charge-density-wave in LaAgSb 2 journal, May 2006

Growth of single crystals from metallic fluxes journal, June 1992

High-temperature solution growth of intermetallic single crystals and quasicrystals journal, May 2001

Growing intermetallic single crystals using in situ decanting journal, July 2012

EXPGUI , a graphical user interface for GSAS journal, April 2001

An empirical correction for absorption anisotropy journal, January 1995

Half Antiperovskites: IV. Crystallographic and Electronic Structure Investigations on A 2 Rh 3 S 2 ( A = In, Sn, Tl, Pb, Bi) journal, September 2009

Diamagnetic Corrections and Pascal's Constants journal, April 2008

Upper Limit for the Critical Field in Hard Superconductors journal, September 1962

Pressure-induced superconductivity in CaFe 2 As 2 journal, July 2008

Evidence for filamentary superconductivity nucleated at antiphase domain walls in antiferromagnetic CaFe 2 As 2 journal, January 2012

Filamentary superconductivity across the phase diagram of Ba(Fe,Co) 2 As 2 journal, August 2012

Superconductivity of La 3 Co 4 Sn 13 and La 3 Rh 4 Sn 13 : A comparative study journal, March 2014

Upper Critical Field Peculiarities of Superconducting YNi 2 B 2 C and LuNi 2 B 2 C journal, February 1998

Anisotropy and Temperature Dependence of the Upper Critical Field of Type-II Superconductors journal, January 1967

Anisotropic Upper Critical Field of LuN i 2 B 2 C journal, September 1997

Transition Temperature of Strong-Coupled Superconductors journal, March 1968

Magnetic measurements of the upper critical field of YBa 2 Cu 3 O 7 − δ single crystals journal, April 1989

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples journal, December 2015

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New materials physics journal, November 2019

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Title: Superconductivity versus structural phase transition in the closely related Bi₂Rh_3.5S₂ and Bi₂Rh₃S₂

Zur Theorie der elektrischen und thermischen Leitfähigkeit von Metallen
journal, January 1930

On the theory of superconductivity: the one-dimensional case
journal, May 1954

Theory of Superconductivity
journal, December 1957

Superconductors with charge- and spin-density waves: theory and experiment (Review)
journal, May 2000

Charge- and spin-density-wave superconductors
journal, March 2001

Charge-Density Waves in Metallic, Layered, Transition-Metal Dichalcogenides
journal, April 1974

Heat capacity of 2HNbSe2 at the charge density wave transition
journal, August 1975

Electric Field Breakdown of Charge-Density-Wave—Induced Anomalies in Nb ${Se}_{3}$
journal, September 1976

Electronic properties and superlattice formation in the semimetal ${TiSe}_{2}$
journal, November 1976

Electronic phase transition and partially gapped Fermi surface in superconducting ${Lu}_{5}$ ${Ir}_{4}$ ${Si}_{10}$
journal, October 1986

Strongly coupled charge-density wave transition in single-crystal ${Lu}_{5} {Ir}_{4} {Si}_{10}$
journal, March 1999

Novel charge density wave transition in crystals of R5Ir4Si10
journal, May 2002

Phase transitions in ${Lu}_{2} {Ir}_{3} {Si}_{5}$
journal, January 2005

Superconductivity in CuxTiSe2
journal, July 2006

Synthesis and electrical properties of shandite-parkerite phases, A2M3Ch2
journal, March 1988

Superconductivity in ternary chalcogenides Bi ₂ Ni ₃ X ₂ (X = S, Se)
journal, April 2006

Transport properties in normal-metal ${Bi}_{2} {Pd}_{3} S_{2}$ and superconducting ${Bi}_{2} {Pd}_{3} {Se}_{2}$
journal, July 2008

Development of viable solutions for the synthesis of sulfur bearing single crystals
journal, July 2012

Charge-density-wave superconductor ${Bi}_{2} {Rh}_{3} {Se}_{2}$
journal, February 2007

Pressure effect and electron diffraction on the anomalous transition in ternary superconductor Bi2Rh3Se2
journal, January 2014

Pressure effect on the charge-density-wave formation in $2 H - N b {Se}_{2}$ and correlation between structural instabilities and superconductivity in unstable solids
journal, February 1977

Charge density wave formation, superconductivity and Fermi surface determination in NbSe ₃ : a pressure study
journal, April 1980

Effect of pressure and chemical substitutions on the charge-density-wave in ${LaAgSb}_{2}$
journal, May 2006

Growth of single crystals from metallic fluxes
journal, June 1992

High-temperature solution growth of intermetallic single crystals and quasicrystals
journal, May 2001

Growing intermetallic single crystals using in situ decanting
journal, July 2012

EXPGUI , a graphical user interface for GSAS
journal, April 2001

An empirical correction for absorption anisotropy
journal, January 1995

Half Antiperovskites: IV. Crystallographic and Electronic Structure Investigations on A ₂ Rh ₃ S ₂ ( A = In, Sn, Tl, Pb, Bi)
journal, September 2009

Diamagnetic Corrections and Pascal's Constants
journal, April 2008

Upper Limit for the Critical Field in Hard Superconductors
journal, September 1962

Pressure-induced superconductivity in CaFe ₂ As ₂
journal, July 2008

Evidence for filamentary superconductivity nucleated at antiphase domain walls in antiferromagnetic CaFe $_{2}$ As $_{2}$
journal, January 2012

Filamentary superconductivity across the phase diagram of Ba(Fe,Co) $_{2}$ As $_{2}$
journal, August 2012

Superconductivity of ${La}_{3} {Co}_{4} {Sn}_{13}$ and ${La}_{3} {Rh}_{4} {Sn}_{13}$ : A comparative study
journal, March 2014

Upper Critical Field Peculiarities of Superconducting ${YNi}_{2} B_{2} C$ and ${LuNi}_{2} B_{2} C$
journal, February 1998

Anisotropy and Temperature Dependence of the Upper Critical Field of Type-II Superconductors
journal, January 1967

Anisotropic Upper Critical Field of LuN $i_{2}$ $B_{2}$ C
journal, September 1997

Transition Temperature of Strong-Coupled Superconductors
journal, March 1968

Magnetic measurements of the upper critical field of ${YBa}_{2}$ ${Cu}_{3}$ $O_{7 - δ}$ single crystals
journal, April 1989

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples
journal, December 2015

Superconducting and charge density wave transition in single crystalline LaPt ₂ Si ₂
journal, May 2017

New materials physics
journal, November 2019

Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples
text, January 2015