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Title: Data preparation and evaluation techniques for x-ray diffraction microscopy

Abstract

The post-experiment processing of X-ray Diffraction Microscopy data is often time-consuming and difficult. This is mostly due to the fact that even if a preliminary result has been reconstructed, there is no definitive answer as to whether or not a better result with more consistently retrieved phases can still be obtained. In addition, we show here that the first step in data analysis, the assembly of two-dimensional diffraction patterns from a large set of raw diffraction data, is crucial to obtaining reconstructions of highest possible consistency. We have developed software that automates this process and results in consistently accurate diffraction patterns. We have furthermore derived some criteria of validity for a tool commonly used to assess the consistency of reconstructions, the phase retrieval transfer function, and suggest a modified version that has improved utility for judging reconstruction quality.

Authors:
 [1];  [1];  [1];  [2];  [2];  [1];  [3]
  1. Stony Brook Univ., Stony Brook, NY (United States)
  2. Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
  3. Stony Brook Univ., Stony Brook, NY (United States); Northwestern Univ., Evanston, IL (United States); Argonne National Lab. (ANL), Argonne, IL (United States)
Publication Date:
Research Org.:
Stony Brook Univ., Stony Brook, NY (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1165054
Report Number(s):
DOE-RFSUNY-46128
Journal ID: ISSN 1094-4087; OPEXFF
Grant/Contract Number:  
FG02-04ER46128
Resource Type:
Accepted Manuscript
Journal Name:
Optics Express
Additional Journal Information:
Journal Volume: 18; Journal Issue: 18; Journal ID: ISSN 1094-4087
Publisher:
Optical Society of America (OSA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 77 NANOSCIENCE AND NANOTECHNOLOGY; 97 MATHEMATICS AND COMPUTING

Citation Formats

Steinbrener, Jan, Nelson, Johanna, Huang, Xiaojing, Marchesini, Stefano, Shapiro, David, Turner, Joshua J., and Jacobsen, Chris. Data preparation and evaluation techniques for x-ray diffraction microscopy. United States: N. p., 2010. Web. doi:10.1364/OE.18.018598.
Steinbrener, Jan, Nelson, Johanna, Huang, Xiaojing, Marchesini, Stefano, Shapiro, David, Turner, Joshua J., & Jacobsen, Chris. Data preparation and evaluation techniques for x-ray diffraction microscopy. United States. doi:10.1364/OE.18.018598.
Steinbrener, Jan, Nelson, Johanna, Huang, Xiaojing, Marchesini, Stefano, Shapiro, David, Turner, Joshua J., and Jacobsen, Chris. Fri . "Data preparation and evaluation techniques for x-ray diffraction microscopy". United States. doi:10.1364/OE.18.018598. https://www.osti.gov/servlets/purl/1165054.
@article{osti_1165054,
title = {Data preparation and evaluation techniques for x-ray diffraction microscopy},
author = {Steinbrener, Jan and Nelson, Johanna and Huang, Xiaojing and Marchesini, Stefano and Shapiro, David and Turner, Joshua J. and Jacobsen, Chris},
abstractNote = {The post-experiment processing of X-ray Diffraction Microscopy data is often time-consuming and difficult. This is mostly due to the fact that even if a preliminary result has been reconstructed, there is no definitive answer as to whether or not a better result with more consistently retrieved phases can still be obtained. In addition, we show here that the first step in data analysis, the assembly of two-dimensional diffraction patterns from a large set of raw diffraction data, is crucial to obtaining reconstructions of highest possible consistency. We have developed software that automates this process and results in consistently accurate diffraction patterns. We have furthermore derived some criteria of validity for a tool commonly used to assess the consistency of reconstructions, the phase retrieval transfer function, and suggest a modified version that has improved utility for judging reconstruction quality.},
doi = {10.1364/OE.18.018598},
journal = {Optics Express},
number = 18,
volume = 18,
place = {United States},
year = {2010},
month = {1}
}

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Cited by: 16 works
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    Works referencing / citing this record:

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