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Complexes of technetium(IV) and (III) with tertiary phosphines

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Abstract

The synthesis and characterization of the complexes trans-TcX/sub 4/L/sub 2/ and mer-TcX/sub 3/L/sub 3/(X = Cl and Br, and L = PMe/sub 2/Ph, PEt/sub 2/Ph and PPh/sub 3/) are reported. Configurations were deduced by far-IR and /sup 1/H NMR studies. Magnetic susceptibility and /sup 1/H NMR results for mer-TcCl/sub 3/(PMe/sub 2/Ph)/sub 3/ are compared with those for analogues d/sup 4/ complexes.
Authors:
Mazzi, U; De Paoli, G; Di Bernardo, P; Magon, L [1] 
  1. Consiglio Nazionale delle Ricerche, Padua (Italy). Lab. di Chimica e Tecnologia dei Radioelementi
Publication Date:
Jan 01, 1976
DOI:
https://doi.org/10.1016/0022-1902(76)80344-2
Product Type:
Journal Article
Reference Number:
AIX-07-243959; EDB-77-003238
Resource Relation:
Journal Name: J. Inorg. Nucl. Chem.; (United Kingdom); Journal Volume: 38:4
Subject:
38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEAR CHEMISTRY; TECHNETIUM COMPLEXES; CHEMICAL PREPARATION; FAR INFRARED RADIATION; INFRARED SPECTRA; MAGNETIC SUSCEPTIBILITY; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE; ORGANIC PHOSPHORUS COMPOUNDS; PHOSPHINES; STRUCTURAL CHEMICAL ANALYSIS; COMPLEXES; ELECTROMAGNETIC RADIATION; INFRARED RADIATION; MAGNETIC PROPERTIES; MAGNETIC RESONANCE; ORGANIC COMPOUNDS; PHOSPHORUS COMPOUNDS; PHYSICAL PROPERTIES; RADIATIONS; RESONANCE; SPECTRA; SYNTHESIS; TRANSITION ELEMENT COMPLEXES; 400702* - Radiochemistry & Nuclear Chemistry- Properties of Radioactive Materials
OSTI ID:
7259553
Country of Origin:
United Kingdom
Language:
English
Other Identifying Numbers:
Journal ID: CODEN: JINCA
Submitting Site:
INIS
Size:
Pages: 721-725
Announcement Date:
Aug 01, 1976

Journal Article:

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Citation Formats

Mazzi, U, De Paoli, G, Di Bernardo, P, and Magon, L. Complexes of technetium(IV) and (III) with tertiary phosphines. United Kingdom: N. p., 1976. Web. doi:10.1016/0022-1902(76)80344-2.
Mazzi, U, De Paoli, G, Di Bernardo, P, & Magon, L. Complexes of technetium(IV) and (III) with tertiary phosphines. United Kingdom. https://doi.org/10.1016/0022-1902(76)80344-2
Mazzi, U, De Paoli, G, Di Bernardo, P, and Magon, L. 1976. "Complexes of technetium(IV) and (III) with tertiary phosphines." United Kingdom. https://doi.org/10.1016/0022-1902(76)80344-2.
@misc{etde_7259553,
title = {Complexes of technetium(IV) and (III) with tertiary phosphines}
 author = {Mazzi, U, De Paoli, G, Di Bernardo, P, and Magon, L}
 abstractNote = {The synthesis and characterization of the complexes trans-TcX/sub 4/L/sub 2/ and mer-TcX/sub 3/L/sub 3/(X = Cl and Br, and L = PMe/sub 2/Ph, PEt/sub 2/Ph and PPh/sub 3/) are reported. Configurations were deduced by far-IR and /sup 1/H NMR studies. Magnetic susceptibility and /sup 1/H NMR results for mer-TcCl/sub 3/(PMe/sub 2/Ph)/sub 3/ are compared with those for analogues d/sup 4/ complexes.}
 doi = {10.1016/0022-1902(76)80344-2}
 journal = []
 volume = {38:4}
 journal type = {AC}
 place = {United Kingdom}
 year = {1976}
 month = {Jan}
 }