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Destructive distillation

Abstract

The broken-up shale is placed in cast-iron retorts, heated externally, having exit tubes placed at a low level. Each retort is provided with a steam-pipe with a regulating-cock outside, the pipe being carried around the walls of the retort in a spiral or zig-zag way to ensure superheating of the steam, perforations being made in the pipe to allow exit for the steam into the retort. The steam, which may if desired be superheated before entrance, is passed into the retort when the latter has attained a temperature of from 210 to 250/sup 0/C and the passage is continued while the temperature rises, as long as distillation goes on. The exit pipe to the retort leads to a condenser of much condensing-surface, provided with a drag obtained by an exhausting steam jet or otherwise. The distilled products consist of tar, oils, wax, ammoniacal water (stated to be in greater proportion through the use of the process), and lighting and heating gas. The latter gas goes through a scrubber to a gasholder. The carbonaceous residue in the retort is discharged when cooled below a red heat, into sheet-iron cylinders, with tightly fitting lids, to avoid as far as possible contact with  More>>
Authors:
Publication Date:
Aug 09, 1882
Product Type:
Patent
Report Number:
GB 3792
Reference Number:
EDB-78-100616
Subject:
04 OIL SHALES AND TAR SANDS; OIL SHALES; DESTRUCTIVE DISTILLATION; SHALE OIL; PRODUCTION; TAR; WAXES; AMMONIA; CAST IRON; COMMINUTION; GASES; HEATING; HIGH TEMPERATURE; PIPES; REMOVAL; RESIDUES; RETORTS; SCRUBBING; STEAM; SUPERHEATING; VAPOR CONDENSERS; ALLOYS; BITUMINOUS MATERIALS; CARBIDES; CARBON COMPOUNDS; CARBONACEOUS MATERIALS; CHEMICAL REACTIONS; CHEMICAL REACTORS; CONDENSERS; DECOMPOSITION; DISTILLATION; ENERGY SOURCES; FLUIDS; FOSSIL FUELS; FUELS; HYDRIDES; HYDROGEN COMPOUNDS; IRON ALLOYS; IRON BASE ALLOYS; IRON CARBIDES; IRON COMPOUNDS; MINERAL OILS; NITROGEN COMPOUNDS; NITROGEN HYDRIDES; OILS; ORGANIC COMPOUNDS; OTHER ORGANIC COMPOUNDS; SEPARATION PROCESSES; SYNTHETIC FUELS; SYNTHETIC PETROLEUM; TRANSITION ELEMENT COMPOUNDS; 040402* - Oil Shales & Tar Sands- Surface Methods
OSTI ID:
7205072
Country of Origin:
United Kingdom
Language:
English
Submitting Site:
TIC
Size:
Pages: v
Announcement Date:
May 13, 2001

Citation Formats

Mitting, E K. Destructive distillation. United Kingdom: N. p., 1882. Web.
Mitting, E K. Destructive distillation. United Kingdom.
Mitting, E K. 1882. "Destructive distillation." United Kingdom.
@misc{etde_7205072,
title = {Destructive distillation}
author = {Mitting, E K}
abstractNote = {The broken-up shale is placed in cast-iron retorts, heated externally, having exit tubes placed at a low level. Each retort is provided with a steam-pipe with a regulating-cock outside, the pipe being carried around the walls of the retort in a spiral or zig-zag way to ensure superheating of the steam, perforations being made in the pipe to allow exit for the steam into the retort. The steam, which may if desired be superheated before entrance, is passed into the retort when the latter has attained a temperature of from 210 to 250/sup 0/C and the passage is continued while the temperature rises, as long as distillation goes on. The exit pipe to the retort leads to a condenser of much condensing-surface, provided with a drag obtained by an exhausting steam jet or otherwise. The distilled products consist of tar, oils, wax, ammoniacal water (stated to be in greater proportion through the use of the process), and lighting and heating gas. The latter gas goes through a scrubber to a gasholder. The carbonaceous residue in the retort is discharged when cooled below a red heat, into sheet-iron cylinders, with tightly fitting lids, to avoid as far as possible contact with the atmosphere.}
place = {United Kingdom}
year = {1882}
month = {Aug}
}