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Mono terpenes characterization by {sup 1} H and {sup 13} C-1 NMR; Caracterizacao de monoterpenos por RMN - {sup 1} H e de {sup 13} C-1

Miscellaneous:

Abstract

Artemisinine, a new lactone sesquiterpene containing one peroxide binding, is the main anti malarial agent obtained from the Artemisia annua L. Viewing to obtain a simple synthetic route for artemisinic acid preparation, which is the key intermediary for total synthesis of this type of anti malarial agent, R-carvone has been chosen as starting material. The S-carvone was used as model for reaction optimization and preparation of derivatives to be used for NMR studies. The main objective of this work is the signalling of the {sup 13} C and {sup 1} H NMR spectra, using the 2 D-COSY and 2 D-Hector spectra 4 refs., 3 figs., 1 tab
Authors:
Araujo, Martha T. de; [1]  Silveira, Carmen L.P.; [2]  Mcchesney, James D [3] 
  1. Universidade Federal Fluminense, Niteroi, RJ (Brazil). Dept. de Fisico-Quimica
  2. Universidade Federal Fluminense, Niteroi, RJ (Brazil). Dept. de Quimica Organica
  3. Mississippi Univ., University, MS (United States). Research Inst. of Pharmaceutical Sciences
Publication Date:
Dec 31, 1991
Product Type:
Miscellaneous
Report Number:
CONF-9105459-
Reference Number:
SCA: 665100; 664200; 400101; PA: AIX-29:045902; EDB-98:091435; SN: 98001998980
Resource Relation:
Conference: 3. meeting of nuclear magnetic resonance users, 3. Encontro de usuarios de ressonancia magnetica nuclear, Buzios (Brazil), 14-18 May 1991; Other Information: DN: 4 refs., 3 figs., 1 tab; PBD: 1991; Related Information: Is Part Of Proceedings of the 3. Meeting of nuclear magnetic resonance users; PB: 425 p.; Anais do 3. encontro de usuarios de ressonancia magnetica nuclear
Subject:
66 PHYSICS; 40 CHEMISTRY; ANTI-INFECTIVE AGENTS; DRUGS; LACTONES; MALARIA; NUCLEAR MAGNETIC RESONANCE; SPECTRA; TERPENES
OSTI ID:
636796
Research Organizations:
Associacao de Usuarios de Ressonancia Magnetica Nuclear, Rio de Janeiro, RJ (Brazil)
Country of Origin:
Brazil
Language:
Portuguese
Other Identifying Numbers:
TRN: BR98E1457045902
Availability:
Available from the Library of the Brazilian Nuclear Energy Commission, Rio de Janeiro
Submitting Site:
BRN
Size:
pp. 331-336
Announcement Date:
Jan 24, 2004

Miscellaneous:

Citation Formats

Araujo, Martha T. de, Silveira, Carmen L.P., and Mcchesney, James D. Mono terpenes characterization by {sup 1} H and {sup 13} C-1 NMR; Caracterizacao de monoterpenos por RMN - {sup 1} H e de {sup 13} C-1. Brazil: N. p., 1991. Web.
Araujo, Martha T. de, Silveira, Carmen L.P., & Mcchesney, James D. Mono terpenes characterization by {sup 1} H and {sup 13} C-1 NMR; Caracterizacao de monoterpenos por RMN - {sup 1} H e de {sup 13} C-1. Brazil.
Araujo, Martha T. de, Silveira, Carmen L.P., and Mcchesney, James D. 1991. "Mono terpenes characterization by {sup 1} H and {sup 13} C-1 NMR; Caracterizacao de monoterpenos por RMN - {sup 1} H e de {sup 13} C-1." Brazil.
@misc{etde_636796,
title = {Mono terpenes characterization by {sup 1} H and {sup 13} C-1 NMR; Caracterizacao de monoterpenos por RMN - {sup 1} H e de {sup 13} C-1}
author = {Araujo, Martha T. de, Silveira, Carmen L.P., and Mcchesney, James D}
abstractNote = {Artemisinine, a new lactone sesquiterpene containing one peroxide binding, is the main anti malarial agent obtained from the Artemisia annua L. Viewing to obtain a simple synthetic route for artemisinic acid preparation, which is the key intermediary for total synthesis of this type of anti malarial agent, R-carvone has been chosen as starting material. The S-carvone was used as model for reaction optimization and preparation of derivatives to be used for NMR studies. The main objective of this work is the signalling of the {sup 13} C and {sup 1} H NMR spectra, using the 2 D-COSY and 2 D-Hector spectra 4 refs., 3 figs., 1 tab}
place = {Brazil}
year = {1991}
month = {Dec}
}