Abstract
Electrolyte composition is devised, which permits to increase by an order (as compared with the known compositions) current efficiency in the process of niobium coating electrodeposition. The following ratio of the electrolyte components, g/l, is recommended: dicyclopentadienylniobiumdichloride 5-10, sodium perchlorate - 10-50, dimethylformamide or its mixture with methanol (4:1-20:1) - to 1 l. The process of electrodeposition is realized at the temperature 20-40 deg C and cathode current density 0.05 A/dmS for 0.25-2 h. The cathode potential has the value 0.9-1.5 V (as to relatively saturated mercurous chloride electrode). Copper, platinum, graphite were used as the cathode materials, graphite - as the anode one. The results obtained are substantiated. 1 table.
Citation Formats
Mikshis, Yu I, Kentra, P P, Knizhnikov, B A, and Ol'dekop, Yu A.
Electrolyte for niobium coating deposition. Ehlektrolit dlya osazhdeniya niobievykh pokrytij.
USSR: N. p.,
1982.
Web.
Mikshis, Yu I, Kentra, P P, Knizhnikov, B A, & Ol'dekop, Yu A.
Electrolyte for niobium coating deposition. Ehlektrolit dlya osazhdeniya niobievykh pokrytij.
USSR.
Mikshis, Yu I, Kentra, P P, Knizhnikov, B A, and Ol'dekop, Yu A.
1982.
"Electrolyte for niobium coating deposition. Ehlektrolit dlya osazhdeniya niobievykh pokrytij."
USSR.
@misc{etde_6292976,
title = {Electrolyte for niobium coating deposition. Ehlektrolit dlya osazhdeniya niobievykh pokrytij}
author = {Mikshis, Yu I, Kentra, P P, Knizhnikov, B A, and Ol'dekop, Yu A}
abstractNote = {Electrolyte composition is devised, which permits to increase by an order (as compared with the known compositions) current efficiency in the process of niobium coating electrodeposition. The following ratio of the electrolyte components, g/l, is recommended: dicyclopentadienylniobiumdichloride 5-10, sodium perchlorate - 10-50, dimethylformamide or its mixture with methanol (4:1-20:1) - to 1 l. The process of electrodeposition is realized at the temperature 20-40 deg C and cathode current density 0.05 A/dmS for 0.25-2 h. The cathode potential has the value 0.9-1.5 V (as to relatively saturated mercurous chloride electrode). Copper, platinum, graphite were used as the cathode materials, graphite - as the anode one. The results obtained are substantiated. 1 table.}
place = {USSR}
year = {1982}
month = {Jul}
}
title = {Electrolyte for niobium coating deposition. Ehlektrolit dlya osazhdeniya niobievykh pokrytij}
author = {Mikshis, Yu I, Kentra, P P, Knizhnikov, B A, and Ol'dekop, Yu A}
abstractNote = {Electrolyte composition is devised, which permits to increase by an order (as compared with the known compositions) current efficiency in the process of niobium coating electrodeposition. The following ratio of the electrolyte components, g/l, is recommended: dicyclopentadienylniobiumdichloride 5-10, sodium perchlorate - 10-50, dimethylformamide or its mixture with methanol (4:1-20:1) - to 1 l. The process of electrodeposition is realized at the temperature 20-40 deg C and cathode current density 0.05 A/dmS for 0.25-2 h. The cathode potential has the value 0.9-1.5 V (as to relatively saturated mercurous chloride electrode). Copper, platinum, graphite were used as the cathode materials, graphite - as the anode one. The results obtained are substantiated. 1 table.}
place = {USSR}
year = {1982}
month = {Jul}
}