Abstract
Methods for synthesizing oxohalide complexes of rhenium and molybdenum with +5 oxidation degree with 4',4[sup (5)]-divaleryldibenzo-18-crown-6 were developed. Content and composition of prepared compounds were investigated by the methods of element analysis, crystal optics, conductometry, IR spectroscopy in the near and far regions, thermogravimetry. Oxidation degree of the complex-forming metal was determined. It was established that composition of the compounds coressponded to the general formula MOLX [sub [center dot]] H[sub 2]O, where M - Re, Mo; L -4',4[sup (5)]-divaleryldibenzo-18-crown-6; X -Cl[sup -], Br[sup -].
Ashurova, N Kh;
Yakubov, K G;
Tashmukhamedova, A K;
Basitova, S M
[1]
- Tadzhikskij Gosudarstvennyj Univ., Dushanbe (Tajikistan)
Citation Formats
Ashurova, N Kh, Yakubov, K G, Tashmukhamedova, A K, and Basitova, S M.
Rhenium(5) and molybdenum(5) complexes with 4',4[sup (]5[sup )]-divaleryldibenzo-18-crown-6. Kompleksnye soedineniya reniya(5) i molibdena(5) s 4',4[sup (]5[sup )]-divalerildibenzo-18-kraun-6.
Russian Federation: N. p.,
1993.
Web.
Ashurova, N Kh, Yakubov, K G, Tashmukhamedova, A K, & Basitova, S M.
Rhenium(5) and molybdenum(5) complexes with 4',4[sup (]5[sup )]-divaleryldibenzo-18-crown-6. Kompleksnye soedineniya reniya(5) i molibdena(5) s 4',4[sup (]5[sup )]-divalerildibenzo-18-kraun-6.
Russian Federation.
Ashurova, N Kh, Yakubov, K G, Tashmukhamedova, A K, and Basitova, S M.
1993.
"Rhenium(5) and molybdenum(5) complexes with 4',4[sup (]5[sup )]-divaleryldibenzo-18-crown-6. Kompleksnye soedineniya reniya(5) i molibdena(5) s 4',4[sup (]5[sup )]-divalerildibenzo-18-kraun-6."
Russian Federation.
@misc{etde_5969948,
title = {Rhenium(5) and molybdenum(5) complexes with 4',4[sup (]5[sup )]-divaleryldibenzo-18-crown-6. Kompleksnye soedineniya reniya(5) i molibdena(5) s 4',4[sup (]5[sup )]-divalerildibenzo-18-kraun-6}
author = {Ashurova, N Kh, Yakubov, K G, Tashmukhamedova, A K, and Basitova, S M}
abstractNote = {Methods for synthesizing oxohalide complexes of rhenium and molybdenum with +5 oxidation degree with 4',4[sup (5)]-divaleryldibenzo-18-crown-6 were developed. Content and composition of prepared compounds were investigated by the methods of element analysis, crystal optics, conductometry, IR spectroscopy in the near and far regions, thermogravimetry. Oxidation degree of the complex-forming metal was determined. It was established that composition of the compounds coressponded to the general formula MOLX [sub [center dot]] H[sub 2]O, where M - Re, Mo; L -4',4[sup (5)]-divaleryldibenzo-18-crown-6; X -Cl[sup -], Br[sup -].}
journal = []
volume = {38:2}
journal type = {AC}
place = {Russian Federation}
year = {1993}
month = {Feb}
}
title = {Rhenium(5) and molybdenum(5) complexes with 4',4[sup (]5[sup )]-divaleryldibenzo-18-crown-6. Kompleksnye soedineniya reniya(5) i molibdena(5) s 4',4[sup (]5[sup )]-divalerildibenzo-18-kraun-6}
author = {Ashurova, N Kh, Yakubov, K G, Tashmukhamedova, A K, and Basitova, S M}
abstractNote = {Methods for synthesizing oxohalide complexes of rhenium and molybdenum with +5 oxidation degree with 4',4[sup (5)]-divaleryldibenzo-18-crown-6 were developed. Content and composition of prepared compounds were investigated by the methods of element analysis, crystal optics, conductometry, IR spectroscopy in the near and far regions, thermogravimetry. Oxidation degree of the complex-forming metal was determined. It was established that composition of the compounds coressponded to the general formula MOLX [sub [center dot]] H[sub 2]O, where M - Re, Mo; L -4',4[sup (5)]-divaleryldibenzo-18-crown-6; X -Cl[sup -], Br[sup -].}
journal = []
volume = {38:2}
journal type = {AC}
place = {Russian Federation}
year = {1993}
month = {Feb}
}