The use of photographic plates, and especially of the new Ilford and Kodak plates, in nuclear physics is briefly described. In particular, the application of these methods to the study of the radioactivity of rocks is discussed. In a series of studies made by the authors, the photographic plates were placed in close contact with a thin, highly polished sheet of the rock sample and then developed under specified conditions. This method was used to determine the concentration of U and Th in two radioactive rock samples and the results are given. The samples were then reduced to powder form and the concentrations were again determined. Work on dissolved samples has not yet been completed. In conclusion, the relative merits of these different techniques are indicated.