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Thermal decomposition of rhenium (5) complexes with 1,2,4-triazole. Termicheskoe razlozhenie kompleksov reniya (5) s 1,2,4-triazolom

Journal Article:

Abstract

Processes of thermal decomposition of rhenium (5) complexes with 1,2,4-triazole were studied. Thermolysis products were identified on the basis of data of the element analysis, IR spectra, conductometry and other methods. It is ascertained that at the first stage of thermolysis of hydroxyl-containing monomer complexes removal of water molecules occurs, and at the second one - dimerization process with formation of Re-O-Re group. It is shown that the nature of halide ion practically does not affect the temperature of the start of intensive thermal decomposition of the complexes.
Authors:
Amindzhanov, A A; Gagieva, S Ch; Kotegov, K V [1] 
  1. Tadzhikskij Gosudarstvennyj Univ., Dushanbe (Tajikistan)
Publication Date:
Jan 01, 1991
Product Type:
Journal Article
Reference Number:
AIX-23-046464; EDB-92-109660
Resource Relation:
Journal Name: Izvestiya Vysshikh Uchebnykh Zavedenij, Khimiya i Khimicheskaya Tekhnologiya; (USSR); Journal Volume: 34:10
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; RHENIUM COMPLEXES; PYROLYSIS; CHEMICAL COMPOSITION; CHEMICAL REACTION KINETICS; HYDRATES; INFRARED SPECTRA; OXYHALIDES; PYROLYSIS PRODUCTS; THERMAL GRAVIMETRIC ANALYSIS; TRIAZOLES; AZOLES; CHEMICAL ANALYSIS; CHEMICAL REACTIONS; COMPLEXES; DECOMPOSITION; GRAVIMETRIC ANALYSIS; HALOGEN COMPOUNDS; HETEROCYCLIC COMPOUNDS; KINETICS; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; OXYGEN COMPOUNDS; QUANTITATIVE CHEMICAL ANALYSIS; REACTION KINETICS; SPECTRA; THERMAL ANALYSIS; THERMOCHEMICAL PROCESSES; TRANSITION ELEMENT COMPLEXES; 400201* - Chemical & Physicochemical Properties
OSTI ID:
5185300
Country of Origin:
USSR
Language:
Russian
Other Identifying Numbers:
Journal ID: ISSN 0579-2991; CODEN: IVUKA
Submitting Site:
INIS
Size:
Pages: 21-25
Announcement Date:
Aug 01, 1992

Journal Article:

Citation Formats

Amindzhanov, A A, Gagieva, S Ch, and Kotegov, K V. Thermal decomposition of rhenium (5) complexes with 1,2,4-triazole. Termicheskoe razlozhenie kompleksov reniya (5) s 1,2,4-triazolom. USSR: N. p., 1991. Web.
Amindzhanov, A A, Gagieva, S Ch, & Kotegov, K V. Thermal decomposition of rhenium (5) complexes with 1,2,4-triazole. Termicheskoe razlozhenie kompleksov reniya (5) s 1,2,4-triazolom. USSR.
Amindzhanov, A A, Gagieva, S Ch, and Kotegov, K V. 1991. "Thermal decomposition of rhenium (5) complexes with 1,2,4-triazole. Termicheskoe razlozhenie kompleksov reniya (5) s 1,2,4-triazolom." USSR.
@misc{etde_5185300,
title = {Thermal decomposition of rhenium (5) complexes with 1,2,4-triazole. Termicheskoe razlozhenie kompleksov reniya (5) s 1,2,4-triazolom}
author = {Amindzhanov, A A, Gagieva, S Ch, and Kotegov, K V}
abstractNote = {Processes of thermal decomposition of rhenium (5) complexes with 1,2,4-triazole were studied. Thermolysis products were identified on the basis of data of the element analysis, IR spectra, conductometry and other methods. It is ascertained that at the first stage of thermolysis of hydroxyl-containing monomer complexes removal of water molecules occurs, and at the second one - dimerization process with formation of Re-O-Re group. It is shown that the nature of halide ion practically does not affect the temperature of the start of intensive thermal decomposition of the complexes.}
journal = {Izvestiya Vysshikh Uchebnykh Zavedenij, Khimiya i Khimicheskaya Tekhnologiya; (USSR)}
volume = {34:10}
journal type = {AC}
place = {USSR}
year = {1991}
month = {Jan}
}