Various diagnostic tools were employed to study and optimize the extent of space charge neutralization in the pulsed intense proton beam facility PROFA, comprising Langmuir probes, capacitive probes, and a novel type of the three electrode collector. The latter does not only allow us to measure ion and electron beam current densities in a high magnetic field environment, but also to deduce the density spectrum of the beam electrons. Appropriate operating conditions were identified to attain a complete space charge neutralisation. (author). 5 figs., 4 refs.