Abstract
Cottonseed hulls (8.3 tons per digester) and H/sub 2/SO/sub 4/ solution at temperature of 100/sup 0/ were added to the digester simultaneously. The final H/sub 2/SO/sub 4/ concentration of the charge was approximately 0.7%. The pentosans were hydrolyzed at 133/sup 0/ and 2 atmosphere for 6 hours and 15 minutes, then the temperature was raised to 179/sup 0/ at the top and to 150/sup 0/ at the bottom of the digester for 5 hours and 30 minutes. The hydrolytic products of pentosan were separated, neutralized, and transferred to a dehydration tank. The hexosans were then hydrolyzed at 179 to 187/sup 0/. Dry hulls gave 19.4% of pentose reducing sugars, of which 81.4% were fermented. One ton of dry hulls gave 74 to 79 l. of ethanol. The optimum condition for dehydration was at 165 to 175/sup 0/ for no longer than 4 to 4.5 hours. 2-Furaldehyde was produced in the following steps: the pentosan hydrolyzate was dehydrated with steam, the vapor-furaldehyde mixture was then reheated and finally distilled in a continuous column. The yield of furaldehyde was 36 to 37% of incoming pentoses (7% of dry hulls).
Citation Formats
Bobovnikov, B M, Tsirlin, Yu A, Chepigo, S V, and Shpuntova, M E.
Production of furfural and ethyl alcohol from cottonseed hulls.
USSR: N. p.,
1957.
Web.
Bobovnikov, B M, Tsirlin, Yu A, Chepigo, S V, & Shpuntova, M E.
Production of furfural and ethyl alcohol from cottonseed hulls.
USSR.
Bobovnikov, B M, Tsirlin, Yu A, Chepigo, S V, and Shpuntova, M E.
1957.
"Production of furfural and ethyl alcohol from cottonseed hulls."
USSR.
@misc{etde_5074705,
title = {Production of furfural and ethyl alcohol from cottonseed hulls}
author = {Bobovnikov, B M, Tsirlin, Yu A, Chepigo, S V, and Shpuntova, M E}
abstractNote = {Cottonseed hulls (8.3 tons per digester) and H/sub 2/SO/sub 4/ solution at temperature of 100/sup 0/ were added to the digester simultaneously. The final H/sub 2/SO/sub 4/ concentration of the charge was approximately 0.7%. The pentosans were hydrolyzed at 133/sup 0/ and 2 atmosphere for 6 hours and 15 minutes, then the temperature was raised to 179/sup 0/ at the top and to 150/sup 0/ at the bottom of the digester for 5 hours and 30 minutes. The hydrolytic products of pentosan were separated, neutralized, and transferred to a dehydration tank. The hexosans were then hydrolyzed at 179 to 187/sup 0/. Dry hulls gave 19.4% of pentose reducing sugars, of which 81.4% were fermented. One ton of dry hulls gave 74 to 79 l. of ethanol. The optimum condition for dehydration was at 165 to 175/sup 0/ for no longer than 4 to 4.5 hours. 2-Furaldehyde was produced in the following steps: the pentosan hydrolyzate was dehydrated with steam, the vapor-furaldehyde mixture was then reheated and finally distilled in a continuous column. The yield of furaldehyde was 36 to 37% of incoming pentoses (7% of dry hulls).}
journal = []
volume = {10:2}
journal type = {AC}
place = {USSR}
year = {1957}
month = {Jan}
}
title = {Production of furfural and ethyl alcohol from cottonseed hulls}
author = {Bobovnikov, B M, Tsirlin, Yu A, Chepigo, S V, and Shpuntova, M E}
abstractNote = {Cottonseed hulls (8.3 tons per digester) and H/sub 2/SO/sub 4/ solution at temperature of 100/sup 0/ were added to the digester simultaneously. The final H/sub 2/SO/sub 4/ concentration of the charge was approximately 0.7%. The pentosans were hydrolyzed at 133/sup 0/ and 2 atmosphere for 6 hours and 15 minutes, then the temperature was raised to 179/sup 0/ at the top and to 150/sup 0/ at the bottom of the digester for 5 hours and 30 minutes. The hydrolytic products of pentosan were separated, neutralized, and transferred to a dehydration tank. The hexosans were then hydrolyzed at 179 to 187/sup 0/. Dry hulls gave 19.4% of pentose reducing sugars, of which 81.4% were fermented. One ton of dry hulls gave 74 to 79 l. of ethanol. The optimum condition for dehydration was at 165 to 175/sup 0/ for no longer than 4 to 4.5 hours. 2-Furaldehyde was produced in the following steps: the pentosan hydrolyzate was dehydrated with steam, the vapor-furaldehyde mixture was then reheated and finally distilled in a continuous column. The yield of furaldehyde was 36 to 37% of incoming pentoses (7% of dry hulls).}
journal = []
volume = {10:2}
journal type = {AC}
place = {USSR}
year = {1957}
month = {Jan}
}