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Accuracy of determination of trace metals in soil and sewage sludge

Abstract

Errors in the analysis of liquid samples are often large enough to be important. For solid materials, additional potential complications arise in separating the determinand from the sample matrix and in controlling possible interferences from co-extracted species. These considerations have led to the development of a stepwise, co-ordinated approach by which a group of laboratories have achieved predefined standards of accuracy. Sample digestion has been examined. The analysis of digests has then been addressed; the control of analytical precision has been emphasised. Finally, a demonstration of overall comparability has been undertaken. The results are presented. (orig.). With 1 fig., 2 tabs.
Authors:
Ackers, C J; [1]  Gardner, M J; [2]  Ravenscroft, J E [2] 
  1. Central Regional Council, St. Ninians Road, Stirling FK8 2 HB (United Kingdom)
  2. WRc, Henley Road, Medmenham, Marlow SL7 2HD (United Kingdom)
Publication Date:
Mar 01, 1996
Product Type:
Journal Article
Report Number:
CONF-9505351-
Reference Number:
SCA: 400100; PA: DE-96:0GA255; EDB-96:094203; SN: 96001606100
Resource Relation:
Journal Name: Fresenius` Journal of Analytical Chemistry; Journal Volume: 354; Journal Issue: 5/6; Conference: 6. international Hans Wolfgang Nuernberg memorial symposium on metal compounds in environment and life, Juelich (Germany), 9-12 May 1995; Other Information: PBD: Mar 1996
Subject:
40 CHEMISTRY; SEWAGE SLUDGE; METALS; SOILS; QUANTITATIVE CHEMICAL ANALYSIS; INTERLABORATORY COMPARISONS; QUALITY CONTROL; ACCURACY; SAMPLE PREPARATION
OSTI ID:
241917
Country of Origin:
Germany
Language:
English
Other Identifying Numbers:
Journal ID: FJACES; ISSN 0937-0633; TRN: DE96GA255
Submitting Site:
DE
Size:
pp. 596-601
Announcement Date:
Jun 27, 1996

Citation Formats

Ackers, C J, Gardner, M J, and Ravenscroft, J E. Accuracy of determination of trace metals in soil and sewage sludge. Germany: N. p., 1996. Web.
Ackers, C J, Gardner, M J, & Ravenscroft, J E. Accuracy of determination of trace metals in soil and sewage sludge. Germany.
Ackers, C J, Gardner, M J, and Ravenscroft, J E. 1996. "Accuracy of determination of trace metals in soil and sewage sludge." Germany.
@misc{etde_241917,
title = {Accuracy of determination of trace metals in soil and sewage sludge}
author = {Ackers, C J, Gardner, M J, and Ravenscroft, J E}
abstractNote = {Errors in the analysis of liquid samples are often large enough to be important. For solid materials, additional potential complications arise in separating the determinand from the sample matrix and in controlling possible interferences from co-extracted species. These considerations have led to the development of a stepwise, co-ordinated approach by which a group of laboratories have achieved predefined standards of accuracy. Sample digestion has been examined. The analysis of digests has then been addressed; the control of analytical precision has been emphasised. Finally, a demonstration of overall comparability has been undertaken. The results are presented. (orig.). With 1 fig., 2 tabs.}
journal = []
issue = {5/6}
volume = {354}
journal type = {AC}
place = {Germany}
year = {1996}
month = {Mar}
}