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Determination of Fe, Mn and Pb by GFAAS in red wine

Abstract

A method for determination of Fe, Mn and Pb in red wine samples was developed by the graphite furnace atomic absorption spectrometric. Several different matrix modifiers were necessary because of evident analyte losses that occurred immediately in sample incineration. Red wine samples were analyzed after microwave digestion using HNO{sub 3}. Standard addition method was used, the calibration concentration was 1 ng · ml{sup -1}, 3 ng · ml{sup -1}, 5 ng · ml{sup -1} which containing 580 μg/ml KNO{sub 3} as matrix and 0.2% HNO{sub 3}. The correlation coefficient of the calibration line was very good within the measurement area. The recovery with red wine sample was very good at the range from 95%-107.5%. (authors)
Authors:
Zhecong, Ying; Hua, Jin; Yulan, Su [1] 
  1. Department of Radiochemistry, China Institute of Atomic Energy, Beijing (China)
Publication Date:
Aug 15, 2008
Product Type:
Conference
Resource Relation:
Conference: 26. annual academic conference of China Chemical Society--modern nuclear chemistry and radiochemistry, Tianjin (China), 13-16 Jul 2008; Other Information: 2 refs.; Related Information: In: Proceedings of 26. annual academic conference of China Chemical Society--modern nuclear chemistry and radiochemistry| 126 p.
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; ABSORPTION; ABSORPTION SPECTROSCOPY; BEVERAGES; CALIBRATION; CONCENTRATION RATIO; CORRELATIONS; IRON; LEAD; MANGANESE; MEASURING METHODS; MICROWAVE HEATING; NITRIC ACID; POTASSIUM NITRATES
OSTI ID:
22529528
Research Organizations:
China Chemical Society, Beijing (China)
Country of Origin:
China
Language:
Chinese
Other Identifying Numbers:
TRN: CN1602876100469
Availability:
Available from China Nuclear Information Centre (China Institute of Nuclear Information & Economics), inisservice_cn@163.com
Submitting Site:
INIS
Size:
page(s) 82
Announcement Date:
Nov 16, 2016

Citation Formats

Zhecong, Ying, Hua, Jin, and Yulan, Su. Determination of Fe, Mn and Pb by GFAAS in red wine. China: N. p., 2008. Web.
Zhecong, Ying, Hua, Jin, & Yulan, Su. Determination of Fe, Mn and Pb by GFAAS in red wine. China.
Zhecong, Ying, Hua, Jin, and Yulan, Su. 2008. "Determination of Fe, Mn and Pb by GFAAS in red wine." China.
@misc{etde_22529528,
title = {Determination of Fe, Mn and Pb by GFAAS in red wine}
author = {Zhecong, Ying, Hua, Jin, and Yulan, Su}
abstractNote = {A method for determination of Fe, Mn and Pb in red wine samples was developed by the graphite furnace atomic absorption spectrometric. Several different matrix modifiers were necessary because of evident analyte losses that occurred immediately in sample incineration. Red wine samples were analyzed after microwave digestion using HNO{sub 3}. Standard addition method was used, the calibration concentration was 1 ng · ml{sup -1}, 3 ng · ml{sup -1}, 5 ng · ml{sup -1} which containing 580 μg/ml KNO{sub 3} as matrix and 0.2% HNO{sub 3}. The correlation coefficient of the calibration line was very good within the measurement area. The recovery with red wine sample was very good at the range from 95%-107.5%. (authors)}
place = {China}
year = {2008}
month = {Aug}
}