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The effect of post-deformation aging on superelastic properties of Ni{sub 50.9}Ti thin wires attaining micro and nano-substructure

Abstract

Highlights: ► Precipitation of Ni{sub 4}Ti{sub 3} during aging at 450 °C is hindered after severe cold work. ► Nanostructure formation improves the superelastic behavior of Ni-rich NiTi. ► Deformations less than 0.4 result in work hardening and reduce plateau strain. ► Deformations more than 0.4 yield in high stress and strain values of upper plateau. -- Abstract: Superelastic properties of Ni{sub 50.9}Ti shape memory wires were studied after cold drawing and post-deformation annealing at 450 °C. Characteristic transformation temperatures were determined using differential scanning calorimetry. Microstructural investigations were performed using optical and transmission electron microscopy. Results indicate that deformations more than 0.4 of true strain yield in high stress and high strain values of upper plateau. On the other hand, deformations less than 0.4 result in work hardening and reduce plateau strain. Post-deformation heat treatment at 450 °C leads to precipitation of Ni{sub 4}Ti{sub 3} particles and development of recovered microstructure in slightly cold drawn wires. Post-deformation annealing of wires with cold work value of 0.6 in true strain develop nanocrystalline microstructure and hindered the formation of Ni{sub 4}Ti{sub 3} precipitates. Precipitation of Ni{sub 4}Ti{sub 3} particles improves the superelastic properties of not cold drawn wires. However, in comparison  More>>
Publication Date:
Jun 25, 2013
Product Type:
Journal Article
Resource Relation:
Journal Name: Journal of Alloys and Compounds; Journal Volume: 563; Other Information: Copyright (c) 2013 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA)
Subject:
36 MATERIALS SCIENCE; 77 NANOSCIENCE AND NANOTECHNOLOGY; ALLOYS; ANNEALING; CALORIMETRY; CRYSTALS; DEFORMATION; MICROSTRUCTURE; NANOSTRUCTURES; PRECIPITATION; SHAPE MEMORY EFFECT; STRAIN HARDENING; STRAINS; STRESSES; TRANSMISSION ELECTRON MICROSCOPY
OSTI ID:
22223069
Country of Origin:
Netherlands
Language:
English
Other Identifying Numbers:
Journal ID: ISSN 0925-8388; CODEN: JALCEU; Other: PII: S0925-8388(13)00325-3; TRN: NL14R3458044024
Availability:
Available from http://dx.doi.org/10.1016/j.jallcom.2013.02.027
Submitting Site:
NLN
Size:
page(s) 44-50
Announcement Date:
May 01, 2014

Citation Formats

Abbasi-Chianeh, V., E-mail: vahid61abbasi@gmail.com [Faculty of Mechanics Engineering, Urmia University of Technology, Urmia (Iran, Islamic Republic of), Research Center for Advanced Materials and Mineral Processing, Faculty of Materials Engineering, Sahand University of Technology, Tabriz (Iran, Islamic Republic of)], Khalil-Allafi, J., and Kazemi-choobi, K. The effect of post-deformation aging on superelastic properties of Ni{sub 50.9}Ti thin wires attaining micro and nano-substructure. Netherlands: N. p., 2013. Web. doi:10.1016/J.JALLCOM.2013.02.027.
Abbasi-Chianeh, V., E-mail: vahid61abbasi@gmail.com [Faculty of Mechanics Engineering, Urmia University of Technology, Urmia (Iran, Islamic Republic of), Research Center for Advanced Materials and Mineral Processing, Faculty of Materials Engineering, Sahand University of Technology, Tabriz (Iran, Islamic Republic of)], Khalil-Allafi, J., & Kazemi-choobi, K. The effect of post-deformation aging on superelastic properties of Ni{sub 50.9}Ti thin wires attaining micro and nano-substructure. Netherlands. https://doi.org/10.1016/J.JALLCOM.2013.02.027
Abbasi-Chianeh, V., E-mail: vahid61abbasi@gmail.com [Faculty of Mechanics Engineering, Urmia University of Technology, Urmia (Iran, Islamic Republic of), Research Center for Advanced Materials and Mineral Processing, Faculty of Materials Engineering, Sahand University of Technology, Tabriz (Iran, Islamic Republic of)], Khalil-Allafi, J., and Kazemi-choobi, K. 2013. "The effect of post-deformation aging on superelastic properties of Ni{sub 50.9}Ti thin wires attaining micro and nano-substructure." Netherlands. https://doi.org/10.1016/J.JALLCOM.2013.02.027.
@misc{etde_22223069,
title = {The effect of post-deformation aging on superelastic properties of Ni{sub 50.9}Ti thin wires attaining micro and nano-substructure}
author = {Abbasi-Chianeh, V., E-mail: vahid61abbasi@gmail.com [Faculty of Mechanics Engineering, Urmia University of Technology, Urmia (Iran, Islamic Republic of), Research Center for Advanced Materials and Mineral Processing, Faculty of Materials Engineering, Sahand University of Technology, Tabriz (Iran, Islamic Republic of)], Khalil-Allafi, J., and Kazemi-choobi, K.}
abstractNote = {Highlights: ► Precipitation of Ni{sub 4}Ti{sub 3} during aging at 450 °C is hindered after severe cold work. ► Nanostructure formation improves the superelastic behavior of Ni-rich NiTi. ► Deformations less than 0.4 result in work hardening and reduce plateau strain. ► Deformations more than 0.4 yield in high stress and strain values of upper plateau. -- Abstract: Superelastic properties of Ni{sub 50.9}Ti shape memory wires were studied after cold drawing and post-deformation annealing at 450 °C. Characteristic transformation temperatures were determined using differential scanning calorimetry. Microstructural investigations were performed using optical and transmission electron microscopy. Results indicate that deformations more than 0.4 of true strain yield in high stress and high strain values of upper plateau. On the other hand, deformations less than 0.4 result in work hardening and reduce plateau strain. Post-deformation heat treatment at 450 °C leads to precipitation of Ni{sub 4}Ti{sub 3} particles and development of recovered microstructure in slightly cold drawn wires. Post-deformation annealing of wires with cold work value of 0.6 in true strain develop nanocrystalline microstructure and hindered the formation of Ni{sub 4}Ti{sub 3} precipitates. Precipitation of Ni{sub 4}Ti{sub 3} particles improves the superelastic properties of not cold drawn wires. However, in comparison with annealed and aged wires, severely deformed wires attain better superelastic properties after annealing at 450 °C without any Ni{sub 4}Ti{sub 3} precipitates.}
doi = {10.1016/J.JALLCOM.2013.02.027}
journal = []
volume = {563}
journal type = {AC}
place = {Netherlands}
year = {2013}
month = {Jun}
}