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Radiotracers in Swedish Steel Industry

Abstract

Recent tracer investigations in Swedish steel plants have mainly dealt with problems concerning uon-metallic inclusions, slag weight determination and - labelling of special steel qualities for identification. Suspected inclusion sources, such as furnace slag, ladle-bottom mortar and some brick materials as stopper, nozzle.and channel bricks have been labelled radioactively in different ways. The labelling technique has been studied for the different systems and a new method was developed for brick materials. This includes vacuum impregnation with an aqueous solution of the inactive tracer, reheating to 1300 Degree-Sign C and neutron-irradiation in a reactor. A sufficiently homogeneous labelling of the material was obtained in this way. The tracer used was terbium, which was added as the nitrate and then decomposed to oxide during the heating process. The oxide is strongly bound to the ceramic material. The number of radioactive inclusions was determined by.autoradiography, and related to the total number pf inclusions, obtained by visual slag-counting, to give the percentage of inclusions originating from the labelled object. Some investigations have been made using simultaneous labelling of two or more sources. It seems to be difficult, however, to measure separately more than two tracers: one short-lived (e.g. 140La) and one long-lived (e.g. {sup  More>>
Authors:
Eriksson, I.; Erwall, L. G.; [1]  Nyquist, O. [2] 
  1. Isotope Techniques Laboratory, Stockholm (Sweden)
  2. Surahammars Bruks AB, Surahammar (Sweden)
Publication Date:
Jun 15, 1967
Product Type:
Conference
Report Number:
IAEA-SM-84/35
Resource Relation:
Conference: Symposium on Radioisotope Tracers in Industry and Geophysics, Prague (Czech Republic), 21-25 Nov 1966; Other Information: 4 refs., 7 figs., 1 tab.; Related Information: In: Radioisotope Tracers in Industry and Geophysics. Proceedings of the Symposium on Radioisotope Tracers in Industry and Geophysics| 728 p.
Subject:
36 MATERIALS SCIENCE; 07 ISOTOPES AND RADIATION SOURCES; AQUEOUS SOLUTIONS; BARIUM 131; BLAST FURNACES; BRICKS; CERAMICS; DILUTION; GRAPHITE; INCLUSIONS; IRRADIATION; LABELLING; LANTHANUM 140; NEUTRONS; OXIDES; SLAGS; STEELS; TERBIUM; TERBIUM 160; TRACER TECHNIQUES
OSTI ID:
22116251
Research Organizations:
International Atomic Energy Agency, Vienna (Austria)
Country of Origin:
IAEA
Language:
English
Other Identifying Numbers:
Other: ISSN 0074-1884; TRN: XA13M1501072906
Submitting Site:
INIS
Size:
page(s) 513-525
Announcement Date:
Jul 29, 2013

Citation Formats

Eriksson, I., Erwall, L. G., and Nyquist, O. Radiotracers in Swedish Steel Industry. IAEA: N. p., 1967. Web.
Eriksson, I., Erwall, L. G., & Nyquist, O. Radiotracers in Swedish Steel Industry. IAEA.
Eriksson, I., Erwall, L. G., and Nyquist, O. 1967. "Radiotracers in Swedish Steel Industry." IAEA.
@misc{etde_22116251,
title = {Radiotracers in Swedish Steel Industry}
author = {Eriksson, I., Erwall, L. G., and Nyquist, O.}
abstractNote = {Recent tracer investigations in Swedish steel plants have mainly dealt with problems concerning uon-metallic inclusions, slag weight determination and - labelling of special steel qualities for identification. Suspected inclusion sources, such as furnace slag, ladle-bottom mortar and some brick materials as stopper, nozzle.and channel bricks have been labelled radioactively in different ways. The labelling technique has been studied for the different systems and a new method was developed for brick materials. This includes vacuum impregnation with an aqueous solution of the inactive tracer, reheating to 1300 Degree-Sign C and neutron-irradiation in a reactor. A sufficiently homogeneous labelling of the material was obtained in this way. The tracer used was terbium, which was added as the nitrate and then decomposed to oxide during the heating process. The oxide is strongly bound to the ceramic material. The number of radioactive inclusions was determined by.autoradiography, and related to the total number pf inclusions, obtained by visual slag-counting, to give the percentage of inclusions originating from the labelled object. Some investigations have been made using simultaneous labelling of two or more sources. It seems to be difficult, however, to measure separately more than two tracers: one short-lived (e.g. 140La) and one long-lived (e.g. {sup 160}Tb). The slag weight determinations were made using the isotope dilution technique with {sup 131}Ba and {sup 140}La as tracers. A difference in slag weight is sometimes obtained. An attempt is made to explain these deviations. The material transport through a blast furnace has been followed by using a piece of graphite, labelled with {sup 140}La{sub 2}O{sub 3}, and measuring the radiation intensity outside the furnace walls and in the tuyere. Studies have been made to determine suitable radiotracers for labelling of steel for subsequent identification. Up to three different isotopes can be used simultaneously without making the identification too complicated for practical use. (author)}
place = {IAEA}
year = {1967}
month = {Jun}
}