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A new pnCCD-based color X-ray camera for fast spatial and energy-resolved measurements

Abstract

We present a new high resolution X-ray imager based on a pnCCD detector and a polycapillary optics. The properties of the pnCCD like high quantum efficiency, high energy resolution and radiation hardness are maintained, while color corrected polycapillary lenses are used to direct the fluorescence photons from every spot on a sample to a corresponding pixel on the detector. The camera is sensitive to photons from 3 to 40 keV with still 30% quantum efficiency at 20 keV. The pnCCD is operated in split frame mode allowing a high frame rate of 400 Hz with an energy resolution of 152 eV for Mn K{alpha} (5.9 keV) at 450 kcps. In single-photon counting mode (SPC), the time, energy and position of every fluorescence photon is recorded for every frame. A dedicated software enables the visualization of the elements distribution in real time without the need of post-processing the data. A description of the key components including detector, X-ray optics and camera is given. First experiments show the capability of the camera to perform fast full-field X-Ray Fluorescence (FF-XRF) for element analysis. The imaging performance with a magnifying optics (3x) has also been successfully tested.
Authors:
Ordavo, I; [1]  PNDetector GmbH, Emil-Nolde-Strasse 10, 81735 Muenchen (Germany)]; Ihle, S; [1]  Arkadiev, V; [2]  Scharf, O; [3]  Soltau, H; [1]  Bjeoumikhov, A; Bjeoumikhova, S; [4]  Buzanich, G; [3]  Gubzhokov, R; Guenther, A; [4]  Hartmann, R; Holl, P; [1]  Kimmel, N; [5]  Max-Planck-Institut Halbleiterlabor, Otto-Hahn-Ring 6, 81739 Muenchen (Germany)]; Kuehbacher, M; [6]  Lang, M; [1]  Langhoff, N; [4]  Liebel, A; [7]  Radtke, M; Reinholz, U; Riesemeier, H; [3]  others, and
  1. PNSensor GmbH, Roemerstrasse 28, 80803 Muenchen (Germany)
  2. Institut fuer angewandte Photonik e.V., Rudower Chaussee 29/31, 12489 Berlin (Germany)
  3. BAM Federal Institute for Materials Research and Testing, Richard-Willstaetter-Strasse 11, 12489 Berlin (Germany)
  4. IFG - Institute for Scientific Instruments GmbH, Rudower Chaussee 29/31, 12489 Berlin (Germany)
  5. Max-Planck-Institut fuer extraterrestrische Physik, Giessenbachstrasse, 85748 Garching (Germany)
  6. Helmholtz Centre Berlin for Materials and Energy, Hahn-Meitner-Platz 1, 14109 Berlin (Germany)
  7. PNDetector GmbH, Emil-Nolde-Strasse 10, 81735 Muenchen (Germany)
Publication Date:
Oct 21, 2011
Product Type:
Journal Article
Resource Relation:
Journal Name: Nuclear Instruments and Methods in Physics Research. Section A, Accelerators, Spectrometers, Detectors and Associated Equipment; Journal Volume: 654; Journal Issue: 1; Other Information: Copyright (c) 2011 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA)
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; CHARGE-COUPLED DEVICES; COLOR MODEL; DISTRIBUTION; ENERGY RESOLUTION; FLUORESCENCE; HARDNESS; KEV RANGE; PERFORMANCE; QUANTUM EFFICIENCY; X RADIATION; X-RAY FLUORESCENCE ANALYSIS
OSTI ID:
22042601
Country of Origin:
Netherlands
Language:
English
Other Identifying Numbers:
Journal ID: ISSN 0168-9002; CODEN: NIMAER; Other: PII: S0168-9002(11)01171-5; TRN: NL12R5800002054
Availability:
Available from http://dx.doi.org/10.1016/j.nima.2011.05.080
Submitting Site:
NLN
Size:
page(s) 250-257
Announcement Date:
Feb 11, 2013

Citation Formats

Ordavo, I, PNDetector GmbH, Emil-Nolde-Strasse 10, 81735 Muenchen (Germany)], Ihle, S, Arkadiev, V, Scharf, O, Soltau, H, Bjeoumikhov, A, Bjeoumikhova, S, Buzanich, G, Gubzhokov, R, Guenther, A, Hartmann, R, Holl, P, Kimmel, N, Max-Planck-Institut Halbleiterlabor, Otto-Hahn-Ring 6, 81739 Muenchen (Germany)], Kuehbacher, M, Lang, M, Langhoff, N, Liebel, A, Radtke, M, Reinholz, U, Riesemeier, H, and others, and. A new pnCCD-based color X-ray camera for fast spatial and energy-resolved measurements. Netherlands: N. p., 2011. Web. doi:10.1016/J.NIMA.2011.05.080.
Ordavo, I, PNDetector GmbH, Emil-Nolde-Strasse 10, 81735 Muenchen (Germany)], Ihle, S, Arkadiev, V, Scharf, O, Soltau, H, Bjeoumikhov, A, Bjeoumikhova, S, Buzanich, G, Gubzhokov, R, Guenther, A, Hartmann, R, Holl, P, Kimmel, N, Max-Planck-Institut Halbleiterlabor, Otto-Hahn-Ring 6, 81739 Muenchen (Germany)], Kuehbacher, M, Lang, M, Langhoff, N, Liebel, A, Radtke, M, Reinholz, U, Riesemeier, H, & others, and. A new pnCCD-based color X-ray camera for fast spatial and energy-resolved measurements. Netherlands. https://doi.org/10.1016/J.NIMA.2011.05.080
Ordavo, I, PNDetector GmbH, Emil-Nolde-Strasse 10, 81735 Muenchen (Germany)], Ihle, S, Arkadiev, V, Scharf, O, Soltau, H, Bjeoumikhov, A, Bjeoumikhova, S, Buzanich, G, Gubzhokov, R, Guenther, A, Hartmann, R, Holl, P, Kimmel, N, Max-Planck-Institut Halbleiterlabor, Otto-Hahn-Ring 6, 81739 Muenchen (Germany)], Kuehbacher, M, Lang, M, Langhoff, N, Liebel, A, Radtke, M, Reinholz, U, Riesemeier, H, and others, and. 2011. "A new pnCCD-based color X-ray camera for fast spatial and energy-resolved measurements." Netherlands. https://doi.org/10.1016/J.NIMA.2011.05.080.
@misc{etde_22042601,
title = {A new pnCCD-based color X-ray camera for fast spatial and energy-resolved measurements}
author = {Ordavo, I, PNDetector GmbH, Emil-Nolde-Strasse 10, 81735 Muenchen (Germany)], Ihle, S, Arkadiev, V, Scharf, O, Soltau, H, Bjeoumikhov, A, Bjeoumikhova, S, Buzanich, G, Gubzhokov, R, Guenther, A, Hartmann, R, Holl, P, Kimmel, N, Max-Planck-Institut Halbleiterlabor, Otto-Hahn-Ring 6, 81739 Muenchen (Germany)], Kuehbacher, M, Lang, M, Langhoff, N, Liebel, A, Radtke, M, Reinholz, U, Riesemeier, H, and others, and}
abstractNote = {We present a new high resolution X-ray imager based on a pnCCD detector and a polycapillary optics. The properties of the pnCCD like high quantum efficiency, high energy resolution and radiation hardness are maintained, while color corrected polycapillary lenses are used to direct the fluorescence photons from every spot on a sample to a corresponding pixel on the detector. The camera is sensitive to photons from 3 to 40 keV with still 30% quantum efficiency at 20 keV. The pnCCD is operated in split frame mode allowing a high frame rate of 400 Hz with an energy resolution of 152 eV for Mn K{alpha} (5.9 keV) at 450 kcps. In single-photon counting mode (SPC), the time, energy and position of every fluorescence photon is recorded for every frame. A dedicated software enables the visualization of the elements distribution in real time without the need of post-processing the data. A description of the key components including detector, X-ray optics and camera is given. First experiments show the capability of the camera to perform fast full-field X-Ray Fluorescence (FF-XRF) for element analysis. The imaging performance with a magnifying optics (3x) has also been successfully tested.}
doi = {10.1016/J.NIMA.2011.05.080}
journal = []
issue = {1}
volume = {654}
journal type = {AC}
place = {Netherlands}
year = {2011}
month = {Oct}
}