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Characterization and analysis of epoxy/clay nanotubes composites; Cacaterizacao e analise de compositos de epoxi, argila e nanotubos de carbono

Abstract

An DGEBA epoxy matrix was used aiming to achieve a nanocomposite material, through the dispersion of (CNT) via mechanical stirring followed by sonication. In this work the following characterization were performed: mechanical characterization, differential scanning calorimetry (DSC), wide angle X-ray diffraction (WXRD) and scanning electron microscopy (SEM). The addition of CNT and modified clays promoted the increase of modulus of the epoxy matrix, and a synergistic effect between CNT and both clays could be presumed. SEM images of the fracture surface show the difference between the fracture surface area and the presence of clusters among the samples, allowing a correlation with the modulus of elasticity. X-ray diffractograms from 2{Theta} = 5 deg showed no peaks for modified clay samples, however it is possible to affirm that modified clay platelets are forming a less organized structure compared to the structure of the clay as natural in epoxy. (author)
Publication Date:
Jul 01, 2011
Product Type:
Conference
Report Number:
INIS-BR-11641
Resource Relation:
Conference: 11. Brazilian congress on polymers, 11. Congresso brasileira de polimeros, Campos do Jordao, SP (Brazil), 16-20 Oct 2011
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; CARBON; CLAYS; DIFFERENTIAL THERMAL ANALYSIS; EPOXIDES; NANOSTRUCTURES; RESINS; SCANNING ELECTRON MICROSCOPY; STRUCTURAL CHEMICAL ANALYSIS; X RADIATION; X-RAY DIFFRACTION; COHERENT SCATTERING; DIFFRACTION; ELECTROMAGNETIC RADIATION; ELECTRON MICROSCOPY; ELEMENTS; IONIZING RADIATIONS; MICROSCOPY; MINERALS; NONMETALS; ORGANIC COMPOUNDS; ORGANIC OXYGEN COMPOUNDS; ORGANIC POLYMERS; PETROCHEMICALS; PETROLEUM PRODUCTS; POLYMERS; RADIATIONS; SCATTERING; SILICATE MINERALS; THERMAL ANALYSIS
OSTI ID:
21592835
Research Organizations:
Associacao Brasileira de Polimeros (ABPol), Sao Carlos, SP (Brazil)
Country of Origin:
Brazil
Language:
Portuguese
Other Identifying Numbers:
TRN: BR12V2085070980
Availability:
Available from INIS in electronic form
Submitting Site:
BRN
Size:
6 pages
Announcement Date:
Sep 06, 2012

Citation Formats

None. Characterization and analysis of epoxy/clay nanotubes composites; Cacaterizacao e analise de compositos de epoxi, argila e nanotubos de carbono. Brazil: N. p., 2011. Web.
None. Characterization and analysis of epoxy/clay nanotubes composites; Cacaterizacao e analise de compositos de epoxi, argila e nanotubos de carbono. Brazil.
None. 2011. "Characterization and analysis of epoxy/clay nanotubes composites; Cacaterizacao e analise de compositos de epoxi, argila e nanotubos de carbono." Brazil.
@misc{etde_21592835,
title = {Characterization and analysis of epoxy/clay nanotubes composites; Cacaterizacao e analise de compositos de epoxi, argila e nanotubos de carbono}
author = {None}
abstractNote = {An DGEBA epoxy matrix was used aiming to achieve a nanocomposite material, through the dispersion of (CNT) via mechanical stirring followed by sonication. In this work the following characterization were performed: mechanical characterization, differential scanning calorimetry (DSC), wide angle X-ray diffraction (WXRD) and scanning electron microscopy (SEM). The addition of CNT and modified clays promoted the increase of modulus of the epoxy matrix, and a synergistic effect between CNT and both clays could be presumed. SEM images of the fracture surface show the difference between the fracture surface area and the presence of clusters among the samples, allowing a correlation with the modulus of elasticity. X-ray diffractograms from 2{Theta} = 5 deg showed no peaks for modified clay samples, however it is possible to affirm that modified clay platelets are forming a less organized structure compared to the structure of the clay as natural in epoxy. (author)}
place = {Brazil}
year = {2011}
month = {Jul}
}