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Synthesis and characterization particles of Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtained by the citrate-EDTA technique; Sintese e caracterizacao de particulados de Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtidos pela tecnica dos citratos-EDTA

Abstract

The Ba{sub (1-x)}Sr{sub (x)}Co{sub (1-y)}Fe{sub (y)}O{sub (3)} (BSCF) has been studied as a cathode material for Intermediate Temperature Solid Oxide Fuel Cell, due to its better ion and electron conduction. This work aims to study the synthesis of the compound obtained from the citrate-EDTA technique. Thermogravimetric analysis indicated the formation of the compound above 800 deg C. The materials calcined at temperatures of 700, 800 and 900 deg C for 5 h showed cubic pseudo-perovskite structure, according to the literature. By analysis of X-ray fluorescence were obtained powders with nominal chemical composition in the temperature range studied. The micrographs obtained by SEM and particle size distribution analysis showed the formation of particle with diameters below 1 micron. (author)
Authors:
Bonturim, E; Vargas, R A; Andreoli, M; Seo, E S.M., [1] 
  1. Instituto de Pesquisas Energeticas e Nucleares (CCTM/IPEN/CNEN-SP), Sao Paulo, SP (Brazil). Centro de Ciencia e Tecnologia de Materiais
Publication Date:
Jul 01, 2010
Product Type:
Conference
Report Number:
INIS-BR-9021
Resource Relation:
Conference: 19. CBECIMAT: Brazilian congress on engineering and materials science, 19. CBECIMAT: Congresso brasileiro de engenharia e ciencia dos materiais, Campos do Jordao, SP (Brazil), 21-25 Nov 2010
Subject:
36 MATERIALS SCIENCE; CHEMICAL COMPOSITION; FLUORESCENCE; FLUORESCENCE SPECTROSCOPY; OXIDE MINERALS; PARTICLE SIZE; PEROVSKITES; POWDER METALLURGY; POWDERS; QUANTITATIVE CHEMICAL ANALYSIS; SINTERED MATERIALS; STOICHIOMETRY; X RADIATION; X-RAY FLUORESCENCE ANALYSIS; CHEMICAL ANALYSIS; ELECTROMAGNETIC RADIATION; EMISSION; EMISSION SPECTROSCOPY; IONIZING RADIATIONS; LUMINESCENCE; MATERIALS; METALLURGY; MINERALS; NONDESTRUCTIVE ANALYSIS; PHOTON EMISSION; RADIATIONS; SIZE; SPECTROSCOPY; X-RAY EMISSION ANALYSIS
OSTI ID:
21449240
Research Organizations:
Associacao Brasileira de Ceramica (ABC), Sao Paulo, SP (Brazil); Associacao Brasileira de Metalurgia, Materiais e Mineracao (ABM), Sao Paulo, SP (Brazil); Associacao Brasileira de Polimeros (ABPol), Sao Paulo, SP (Brazil)
Country of Origin:
Brazil
Language:
Portuguese
Other Identifying Numbers:
TRN: BR11V1526044067
Availability:
Available from INIS in electronic form
Submitting Site:
BRN
Size:
8 p. pages
Announcement Date:
Jul 07, 2011

Citation Formats

Bonturim, E, Vargas, R A, Andreoli, M, and Seo, E S.M.,. Synthesis and characterization particles of Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtained by the citrate-EDTA technique; Sintese e caracterizacao de particulados de Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtidos pela tecnica dos citratos-EDTA. Brazil: N. p., 2010. Web.
Bonturim, E, Vargas, R A, Andreoli, M, & Seo, E S.M.,. Synthesis and characterization particles of Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtained by the citrate-EDTA technique; Sintese e caracterizacao de particulados de Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtidos pela tecnica dos citratos-EDTA. Brazil.
Bonturim, E, Vargas, R A, Andreoli, M, and Seo, E S.M.,. 2010. "Synthesis and characterization particles of Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtained by the citrate-EDTA technique; Sintese e caracterizacao de particulados de Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtidos pela tecnica dos citratos-EDTA." Brazil.
@misc{etde_21449240,
title = {Synthesis and characterization particles of Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtained by the citrate-EDTA technique; Sintese e caracterizacao de particulados de Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtidos pela tecnica dos citratos-EDTA}
author = {Bonturim, E, Vargas, R A, Andreoli, M, and Seo, E S.M.,}
abstractNote = {The Ba{sub (1-x)}Sr{sub (x)}Co{sub (1-y)}Fe{sub (y)}O{sub (3)} (BSCF) has been studied as a cathode material for Intermediate Temperature Solid Oxide Fuel Cell, due to its better ion and electron conduction. This work aims to study the synthesis of the compound obtained from the citrate-EDTA technique. Thermogravimetric analysis indicated the formation of the compound above 800 deg C. The materials calcined at temperatures of 700, 800 and 900 deg C for 5 h showed cubic pseudo-perovskite structure, according to the literature. By analysis of X-ray fluorescence were obtained powders with nominal chemical composition in the temperature range studied. The micrographs obtained by SEM and particle size distribution analysis showed the formation of particle with diameters below 1 micron. (author)}
place = {Brazil}
year = {2010}
month = {Jul}
}