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Spectrographic determination of metallic impurities in organic coolants for nuclear reactors; Determinacion espectrografica de impurezas metalicas en refrigerantes organicos para reactores nucleares

Abstract

A spectrochemical method for determining metallic impurities in organic coolants for nuclear reactors is given. The organic matter in solid samples is eliminated by controlled distillation and dry ashing in the presence of magnesium oxide as carrier. Liquid, samples are vacuum distillated. The residue is analyzed by carrier distillation and by total burning techniques. The analytical results are discussed and compared with those obtained destroying the organic matter without carrier and using the copper spark technique. (Author) 12 refs.
Publication Date:
Jul 01, 1969
Product Type:
Technical Report
Report Number:
JEN-211
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; METALLIC GLASSES; IMPURITIES; MAGNESIUM; REACTORS; ORGANIC MATTER; VACUUM WELDING
OSTI ID:
21125878
Research Organizations:
Junta de Energia Nuclear (JEN), Madrid (Spain)
Country of Origin:
Spain
Language:
Spanish
Other Identifying Numbers:
TRN: ES09B0025
Availability:
Commercial reproduction prohibited; OSTI as DE21125878
Submitting Site:
SPN
Size:
9 pages
Announcement Date:
Feb 25, 2009

Citation Formats

Martin Munoz, M, and Alvarez Gonzalez, F. Spectrographic determination of metallic impurities in organic coolants for nuclear reactors; Determinacion espectrografica de impurezas metalicas en refrigerantes organicos para reactores nucleares. Spain: N. p., 1969. Web.
Martin Munoz, M, & Alvarez Gonzalez, F. Spectrographic determination of metallic impurities in organic coolants for nuclear reactors; Determinacion espectrografica de impurezas metalicas en refrigerantes organicos para reactores nucleares. Spain.
Martin Munoz, M, and Alvarez Gonzalez, F. 1969. "Spectrographic determination of metallic impurities in organic coolants for nuclear reactors; Determinacion espectrografica de impurezas metalicas en refrigerantes organicos para reactores nucleares." Spain.
@misc{etde_21125878,
title = {Spectrographic determination of metallic impurities in organic coolants for nuclear reactors; Determinacion espectrografica de impurezas metalicas en refrigerantes organicos para reactores nucleares}
author = {Martin Munoz, M, and Alvarez Gonzalez, F}
abstractNote = {A spectrochemical method for determining metallic impurities in organic coolants for nuclear reactors is given. The organic matter in solid samples is eliminated by controlled distillation and dry ashing in the presence of magnesium oxide as carrier. Liquid, samples are vacuum distillated. The residue is analyzed by carrier distillation and by total burning techniques. The analytical results are discussed and compared with those obtained destroying the organic matter without carrier and using the copper spark technique. (Author) 12 refs.}
place = {Spain}
year = {1969}
month = {Jul}
}