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Quantitative analysis of water heavy by NMR spectroscopy; aplicacion de la resonancia magnetica nuclear al analisis cuantitativo de agua pesada

Abstract

Nuclear Magnetic Resonance has been applied to a wide variety of quantitative problems. A typical example has been the determination of isotopic composition. In this paper two different analytical methods for the determination of water in deuterium oxide are described. The first one, employs acetonitril as an internal standard compound and in the second one calibration curve of signal integral curve versus amount of D{sub 2}O is constructed. Both methods give results comparable to those of mass spectrometry of IR spectroscopy. (Author) 5 refs.
Authors:
Publication Date:
Jul 01, 1975
Product Type:
Technical Report
Report Number:
JEN-302
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; QUANTITATIVE CHEMICAL ANALYSIS; HEAVY WATER; NUCLEAR MAGNETIC RESONANCE; ISOTOPE RATIO; SPECTROSCOPY; ORGANIC OXYGEN COMPOUNDS; CALIBRATION STANDARDS; NITRILES
OSTI ID:
21040061
Research Organizations:
Junta de Energia Nuclear (JEN), Madrid (Spain)
Country of Origin:
Spain
Language:
Spanish
Other Identifying Numbers:
TRN: ES08B0305
Availability:
Commercial reproduction prohibited; OSTI as DE21040061
Submitting Site:
SPN
Size:
11 pages
Announcement Date:
Jun 23, 2008

Citation Formats

Gomez Gil, V. Quantitative analysis of water heavy by NMR spectroscopy; aplicacion de la resonancia magnetica nuclear al analisis cuantitativo de agua pesada. Spain: N. p., 1975. Web.
Gomez Gil, V. Quantitative analysis of water heavy by NMR spectroscopy; aplicacion de la resonancia magnetica nuclear al analisis cuantitativo de agua pesada. Spain.
Gomez Gil, V. 1975. "Quantitative analysis of water heavy by NMR spectroscopy; aplicacion de la resonancia magnetica nuclear al analisis cuantitativo de agua pesada." Spain.
@misc{etde_21040061,
title = {Quantitative analysis of water heavy by NMR spectroscopy; aplicacion de la resonancia magnetica nuclear al analisis cuantitativo de agua pesada}
author = {Gomez Gil, V}
abstractNote = {Nuclear Magnetic Resonance has been applied to a wide variety of quantitative problems. A typical example has been the determination of isotopic composition. In this paper two different analytical methods for the determination of water in deuterium oxide are described. The first one, employs acetonitril as an internal standard compound and in the second one calibration curve of signal integral curve versus amount of D{sub 2}O is constructed. Both methods give results comparable to those of mass spectrometry of IR spectroscopy. (Author) 5 refs.}
place = {Spain}
year = {1975}
month = {Jul}
}