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Nanohardness and Young's modulus of YBCO samples textured by the Bridgman technique

Abstract

Mechanical properties of the orthorhombic phase of YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} (Y123) at room temperature have been investigated at different applied loads: 5, 10, 30 and 100 mN using a nanoindentation technique. This study was carried out for different monodomains on the (001) plane for textured Bridgman samples with dispersed particles of Y211 as pinning centres. Hardness and Young's modulus values were calculated using the Oliver-Pharr approach. Nanohardness and Young's modulus for the Y123, Y{sub 2}BaCuO{sub 5} (Y211) and Y 123/Y 211{sub composite} (YBCO) were determined using an applied load of 5 and 10 mN. For higher loads, it is not possible to differentiate the matrix (Y123) from the precipitates (Y211). In this case, only hardness and Young's modulus of the YBCO composite can be determined. Finally, the ultra-low load imprints obtained by nanoindentation have been correlated with parameters obtained by atomic force microscopy (AFM) and field emission scanning electron microscopy (FE-SEM)
Authors:
Roa, J J; Capdevila, X G; MartInez, M; Espiell, F; Segarra, M [1] 
  1. Centro DIOPMA, Departamento de Ciencia de los Materiales e Ingenieria Metalurgica, Instituto de Nanociencia y NanotecnologIa de la Universidad de Barcelona (IN2UB), Facultat de Quimica, Universidad de Barcelona, MartIi Franques 1, Barcelona E-08028 (Spain)
Publication Date:
Sep 26, 2007
Product Type:
Journal Article
Resource Relation:
Journal Name: Nanotechnology (Print); Journal Volume: 18; Journal Issue: 38; Other Information: PII: S0957-4484(07)49164-4; DOI: 10.1088/0957-4484/18/38/385701; Country of input: International Atomic Energy Agency (IAEA)
Subject:
36 MATERIALS SCIENCE; ATOMIC FORCE MICROSCOPY; BARIUM OXIDES; COPPER OXIDES; FIELD EMISSION; HARDNESS; HIGH-TC SUPERCONDUCTORS; NANOSTRUCTURES; ORTHORHOMBIC LATTICES; PARTICLES; PRECIPITATION; SCANNING ELECTRON MICROSCOPY; TEMPERATURE RANGE 0273-0400 K; YOUNG MODULUS; YTTRIUM OXIDES
OSTI ID:
21018793
Country of Origin:
United Kingdom
Language:
English
Other Identifying Numbers:
Journal ID: ISSN 0957-4484; TRN: GB08P4915040591
Submitting Site:
GBN
Size:
page(s) 385701
Announcement Date:
May 29, 2008

Citation Formats

Roa, J J, Capdevila, X G, MartInez, M, Espiell, F, and Segarra, M. Nanohardness and Young's modulus of YBCO samples textured by the Bridgman technique. United Kingdom: N. p., 2007. Web. doi:10.1088/0957-4484/18/38/385701; COUNTRY OF INPUT: INTERNATIONAL ATOMIC ENERGY AGENCY (IAEA).
Roa, J J, Capdevila, X G, MartInez, M, Espiell, F, & Segarra, M. Nanohardness and Young's modulus of YBCO samples textured by the Bridgman technique. United Kingdom. https://doi.org/10.1088/0957-4484/18/38/385701; COUNTRY OF INPUT: INTERNATIONAL ATOMIC ENERGY AGENCY (IAEA)
Roa, J J, Capdevila, X G, MartInez, M, Espiell, F, and Segarra, M. 2007. "Nanohardness and Young's modulus of YBCO samples textured by the Bridgman technique." United Kingdom. https://doi.org/10.1088/0957-4484/18/38/385701; COUNTRY OF INPUT: INTERNATIONAL ATOMIC ENERGY AGENCY (IAEA).
@misc{etde_21018793,
title = {Nanohardness and Young's modulus of YBCO samples textured by the Bridgman technique}
author = {Roa, J J, Capdevila, X G, MartInez, M, Espiell, F, and Segarra, M}
abstractNote = {Mechanical properties of the orthorhombic phase of YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} (Y123) at room temperature have been investigated at different applied loads: 5, 10, 30 and 100 mN using a nanoindentation technique. This study was carried out for different monodomains on the (001) plane for textured Bridgman samples with dispersed particles of Y211 as pinning centres. Hardness and Young's modulus values were calculated using the Oliver-Pharr approach. Nanohardness and Young's modulus for the Y123, Y{sub 2}BaCuO{sub 5} (Y211) and Y 123/Y 211{sub composite} (YBCO) were determined using an applied load of 5 and 10 mN. For higher loads, it is not possible to differentiate the matrix (Y123) from the precipitates (Y211). In this case, only hardness and Young's modulus of the YBCO composite can be determined. Finally, the ultra-low load imprints obtained by nanoindentation have been correlated with parameters obtained by atomic force microscopy (AFM) and field emission scanning electron microscopy (FE-SEM)}
doi = {10.1088/0957-4484/18/38/385701; COUNTRY OF INPUT: INTERNATIONAL ATOMIC ENERGY AGENCY (IAEA)}
journal = []
issue = {38}
volume = {18}
place = {United Kingdom}
year = {2007}
month = {Sep}
}