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Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria

Abstract

LC-MS/MS was used for determination of selected tetracyclines, sulfonamides, trimethoprim, and fluoroquinolones in manure samples of pig, chicken and turkey, as well as arable soils fertilized with manure. Recoveries from spiked samples ranged from 61 to 105%. Method quantification limits were set to 100 {mu}g/kg for all substances. Analysis of 30 pig manure, 20 chicken and turkey dung, and 30 lyophilized soil samples taken in Austria revealed that in pig manure up to 46 mg/kg chlortetracycline, 29 mg/kg oxytetracycline and 23 mg/kg tetracycline could be detected. As representatives of the group of sulfonamides, sulfadimidine in pig manure and sulfadiazine in chicken and turkey dung were detected in significant amounts (maximum concentration, 20 and 91 mg/kg, respectively). Enrofloxacin was particularly observed in chicken and turkey samples. Positive detection of chlortetracycline, enrofloxacin, and ciprofloxacin, in soil samples should be outlined as most important results of this study. - Specific exposure data of selected veterinarian antibiotics in manure and samples of agriculturally used soils are reported for the first time in Austria.
Authors:
Martinez-Carballo, Elena; [1]  Gonzalez-Barreiro, Carmen; [1]  Scharf, Sigrid; [1]  Gans, Oliver [1] 
  1. Department of Hazardous Substances and Metabolites, Umweltbundesamt GmbH - Austrian Federal Environment Agency, Spittelauer Laende 5, A-1090 Vienna (Austria)
Publication Date:
Jul 15, 2007
Product Type:
Journal Article
Resource Relation:
Journal Name: Environmental Pollution (1987); Journal Volume: 148; Journal Issue: 2; Other Information: DOI: 10.1016/j.envpol.2006.11.035; PII: S0269-7491(06)00681-6; Copyright (c) 2006 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA)
Subject:
60 APPLIED LIFE SCIENCES; CHICKENS; LIQUID COLUMN CHROMATOGRAPHY; MANURES; MASS SPECTROSCOPY; OXYTETRACYCLINE; PYRIMIDINES; SOILS; SULFONAMIDES; SWINE
OSTI ID:
20973326
Country of Origin:
United Kingdom
Language:
English
Other Identifying Numbers:
Journal ID: ISSN 0269-7491; ENPOEK; TRN: GB07R5893002764
Submitting Site:
GBN
Size:
page(s) 570-579
Announcement Date:
Feb 06, 2008

Citation Formats

Martinez-Carballo, Elena, Gonzalez-Barreiro, Carmen, Scharf, Sigrid, and Gans, Oliver. Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria. United Kingdom: N. p., 2007. Web. doi:10.1016/j.envpol.2006.11.035.
Martinez-Carballo, Elena, Gonzalez-Barreiro, Carmen, Scharf, Sigrid, & Gans, Oliver. Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria. United Kingdom. doi:10.1016/j.envpol.2006.11.035.
Martinez-Carballo, Elena, Gonzalez-Barreiro, Carmen, Scharf, Sigrid, and Gans, Oliver. 2007. "Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria." United Kingdom. doi:10.1016/j.envpol.2006.11.035. https://www.osti.gov/servlets/purl/10.1016/j.envpol.2006.11.035.
@misc{etde_20973326,
title = {Environmental monitoring study of selected veterinary antibiotics in animal manure and soils in Austria}
author = {Martinez-Carballo, Elena, Gonzalez-Barreiro, Carmen, Scharf, Sigrid, and Gans, Oliver}
abstractNote = {LC-MS/MS was used for determination of selected tetracyclines, sulfonamides, trimethoprim, and fluoroquinolones in manure samples of pig, chicken and turkey, as well as arable soils fertilized with manure. Recoveries from spiked samples ranged from 61 to 105%. Method quantification limits were set to 100 {mu}g/kg for all substances. Analysis of 30 pig manure, 20 chicken and turkey dung, and 30 lyophilized soil samples taken in Austria revealed that in pig manure up to 46 mg/kg chlortetracycline, 29 mg/kg oxytetracycline and 23 mg/kg tetracycline could be detected. As representatives of the group of sulfonamides, sulfadimidine in pig manure and sulfadiazine in chicken and turkey dung were detected in significant amounts (maximum concentration, 20 and 91 mg/kg, respectively). Enrofloxacin was particularly observed in chicken and turkey samples. Positive detection of chlortetracycline, enrofloxacin, and ciprofloxacin, in soil samples should be outlined as most important results of this study. - Specific exposure data of selected veterinarian antibiotics in manure and samples of agriculturally used soils are reported for the first time in Austria.}
doi = {10.1016/j.envpol.2006.11.035}
journal = {Environmental Pollution (1987)}
issue = {2}
volume = {148}
place = {United Kingdom}
year = {2007}
month = {Jul}
}