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Improvement of the obtention process of phosphorus-32 of the ININ through the application of nuclear analytical techniques; Perfeccionamiento del proceso de obtencion de fosforo-32 del ININ, mediante la aplicacion de tecnicas analiticas nucleares

Abstract

The phosphorus-32, is radioisotope emitting pure {beta}{sup -}, of maximum energy 1.71 MeV with an average life of 14.28 days, and that has application in the industry, agriculture, medicine and biology. The {sup 32} P, produced by means of two nuclear reactions {sup 32} S(n,p){sup 32} P and {sup 31} P (n,{gamma}){sup 32} P; by the facility of handling of sulfur, his low cost and its fast acquisition in the market. I selected the reaction {sup 32} S(n,p){sup 32} P. To produce {sup 32} P it is necessary to prepare and to characterize the target (S-{alpha}) that is obtained from the purification of the raw material, make the mathematical calculations of irradiation, irradiation of the target in the nuclear reactor TRIGA Mark III, radiochemical separation of {sup 32} P of {sup 32} S by a dry distillation method and an hydrolysis of {sup 32} P with diluted HCl obtaining H{sub 3}{sup 32}PO{sub 4} and finally quality control. In the order to make the radiochemistry separation it was necessary to make previous modifications to the process guarantee the quality of product ({sup 32} P), and security of the operator. (Author)
Authors:
Zepeda R, C P [1] 
  1. UMSNH, Facultad de Ingenieria Quimica, Morelia, Michoacan (Mexico)
Publication Date:
Jul 01, 2007
Product Type:
Thesis/Dissertation
Report Number:
INIS-MX-2310
Resource Relation:
Other Information: TH: Thesis (Chemical Engineer)
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; ALPHA PARTICLES; BETA PARTICLES; CHEMICAL PREPARATION; DECAY; DIAGRAMS; ELECTROMAGNETIC RADIATION; EQUATIONS; EXPERIMENTAL DATA; GAMMA SPECTROSCOPY; IMAGES; IONIZING RADIATIONS; ISOTOPE PRODUCTION; MODIFICATIONS; NEUTRONS; NUCLEAR REACTIONS; OPTIMIZATION; PHOSPHORUS 32; PHOSPHORUS ISOTOPES; PROPOSALS; RADIATIONS; SCANNING ELECTRON MICROSCOPY; TRIGA-3-SALAZAR REACTOR; X-RAY DIFFRACTION
OSTI ID:
20935607
Research Organizations:
Instituto Nacional de Investigaciones Nucleares, Ocoyoacac, Estado de Mexico (Mexico)
Country of Origin:
Mexico
Language:
Spanish
Other Identifying Numbers:
TRN: MX0700375093100
Availability:
Available from INIS in electronic form
Submitting Site:
MXN
Size:
126 pages
Announcement Date:
Nov 26, 2007

Citation Formats

Zepeda R, C P. Improvement of the obtention process of phosphorus-32 of the ININ through the application of nuclear analytical techniques; Perfeccionamiento del proceso de obtencion de fosforo-32 del ININ, mediante la aplicacion de tecnicas analiticas nucleares. Mexico: N. p., 2007. Web.
Zepeda R, C P. Improvement of the obtention process of phosphorus-32 of the ININ through the application of nuclear analytical techniques; Perfeccionamiento del proceso de obtencion de fosforo-32 del ININ, mediante la aplicacion de tecnicas analiticas nucleares. Mexico.
Zepeda R, C P. 2007. "Improvement of the obtention process of phosphorus-32 of the ININ through the application of nuclear analytical techniques; Perfeccionamiento del proceso de obtencion de fosforo-32 del ININ, mediante la aplicacion de tecnicas analiticas nucleares." Mexico.
@misc{etde_20935607,
title = {Improvement of the obtention process of phosphorus-32 of the ININ through the application of nuclear analytical techniques; Perfeccionamiento del proceso de obtencion de fosforo-32 del ININ, mediante la aplicacion de tecnicas analiticas nucleares}
author = {Zepeda R, C P}
abstractNote = {The phosphorus-32, is radioisotope emitting pure {beta}{sup -}, of maximum energy 1.71 MeV with an average life of 14.28 days, and that has application in the industry, agriculture, medicine and biology. The {sup 32} P, produced by means of two nuclear reactions {sup 32} S(n,p){sup 32} P and {sup 31} P (n,{gamma}){sup 32} P; by the facility of handling of sulfur, his low cost and its fast acquisition in the market. I selected the reaction {sup 32} S(n,p){sup 32} P. To produce {sup 32} P it is necessary to prepare and to characterize the target (S-{alpha}) that is obtained from the purification of the raw material, make the mathematical calculations of irradiation, irradiation of the target in the nuclear reactor TRIGA Mark III, radiochemical separation of {sup 32} P of {sup 32} S by a dry distillation method and an hydrolysis of {sup 32} P with diluted HCl obtaining H{sub 3}{sup 32}PO{sub 4} and finally quality control. In the order to make the radiochemistry separation it was necessary to make previous modifications to the process guarantee the quality of product ({sup 32} P), and security of the operator. (Author)}
place = {Mexico}
year = {2007}
month = {Jul}
}