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Kinetic study and application of analytical techniques in the obtention of TeO{sub 2} for the production of {sup 131} I; Estudio cinetico y aplicacion de tecnicas analiticas en la obtencion de TeO{sub 2} para la produccion de {sup 131} I

Abstract

The objectives of this investigation work were: A) To synthesize TeO{sub 2} starting from the reaction among the Te and HNO{sub 3} with a superior yield to 90% b) To determine the good temperature of obtaining of the TeO{sub 2} at laboratory level, c) To determine those constant of reaction kinetics, for each one of the tests carried out to different temperatures, and the activation energy of the reaction, d) To characterize the produced TeO{sub 2}, e) To check the viability of using the obtained TeO{sub 2} as raw matter in the production of {sup 131} I in order to contribute to the technological development of our country inside the radioisotope production area. The production process of TeO{sub 2} consists primarily of seven phases: 1) Preparing and assembly of the production equipment of TeO{sub 2}, 2) Oxidation reaction of tellurium, 3) Drying and elimination of sludges of TeO{sub 2}, 4) Sintering of TeO{sub 2}, 5) Characterization of the TeO{sub 2} by means of analytical techniques, 6) Irradiation of the TeO{sub 2}, 7) Quality control. The present document has five chapters, which allow the reader to follow the development of this work to achieve the objectives and to contrast with the  More>>
Authors:
Publication Date:
Jul 01, 2006
Product Type:
Thesis/Dissertation
Report Number:
INIS-MX-2243
Resource Relation:
Other Information: TH: Thesis (Chemical Engineer)
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; ACTIVATION ENERGY; DIAGRAMS; EXPERIMENTAL DATA; IMAGES; IODINE 131; KINETICS; NEUTRON ACTIVATION ANALYSIS; NITRIC ACID; QUALITATIVE CHEMICAL ANALYSIS; QUANTITATIVE CHEMICAL ANALYSIS; RADIOCHEMICAL ANALYSIS; RADIOISOTOPES; RADIOPHARMACEUTICALS; REACTION KINETICS; SCANNING ELECTRON MICROSCOPY; SINTERING; SYNTHESIS; TELLURIUM; TELLURIUM OXIDES; TEMPERATURE DEPENDENCE; TIME DEPENDENCE; TITRATION; TRIGA-3-SALAZAR REACTOR; VOLUMETRIC ANALYSIS; X-RAY DIFFRACTION
OSTI ID:
20899201
Research Organizations:
UAEM, Facultad de Quimica, 50000 Toluca, Estado de Mexico (Mexico)
Country of Origin:
Mexico
Language:
Spanish
Other Identifying Numbers:
TRN: MX0700275061398
Availability:
Available from INIS in electronic form
Submitting Site:
MXN
Size:
137 pages
Announcement Date:
Aug 30, 2007

Citation Formats

Plata D, G. Kinetic study and application of analytical techniques in the obtention of TeO{sub 2} for the production of {sup 131} I; Estudio cinetico y aplicacion de tecnicas analiticas en la obtencion de TeO{sub 2} para la produccion de {sup 131} I. Mexico: N. p., 2006. Web.
Plata D, G. Kinetic study and application of analytical techniques in the obtention of TeO{sub 2} for the production of {sup 131} I; Estudio cinetico y aplicacion de tecnicas analiticas en la obtencion de TeO{sub 2} para la produccion de {sup 131} I. Mexico.
Plata D, G. 2006. "Kinetic study and application of analytical techniques in the obtention of TeO{sub 2} for the production of {sup 131} I; Estudio cinetico y aplicacion de tecnicas analiticas en la obtencion de TeO{sub 2} para la produccion de {sup 131} I." Mexico.
@misc{etde_20899201,
title = {Kinetic study and application of analytical techniques in the obtention of TeO{sub 2} for the production of {sup 131} I; Estudio cinetico y aplicacion de tecnicas analiticas en la obtencion de TeO{sub 2} para la produccion de {sup 131} I}
author = {Plata D, G}
abstractNote = {The objectives of this investigation work were: A) To synthesize TeO{sub 2} starting from the reaction among the Te and HNO{sub 3} with a superior yield to 90% b) To determine the good temperature of obtaining of the TeO{sub 2} at laboratory level, c) To determine those constant of reaction kinetics, for each one of the tests carried out to different temperatures, and the activation energy of the reaction, d) To characterize the produced TeO{sub 2}, e) To check the viability of using the obtained TeO{sub 2} as raw matter in the production of {sup 131} I in order to contribute to the technological development of our country inside the radioisotope production area. The production process of TeO{sub 2} consists primarily of seven phases: 1) Preparing and assembly of the production equipment of TeO{sub 2}, 2) Oxidation reaction of tellurium, 3) Drying and elimination of sludges of TeO{sub 2}, 4) Sintering of TeO{sub 2}, 5) Characterization of the TeO{sub 2} by means of analytical techniques, 6) Irradiation of the TeO{sub 2}, 7) Quality control. The present document has five chapters, which allow the reader to follow the development of this work to achieve the objectives and to contrast with the hypothesis of the work. (Author)}
place = {Mexico}
year = {2006}
month = {Jul}
}