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Device for sampling sodium from a circuit with a view to dosing its impurities (1963); Dispositif de prelevement de sodium sur un cuicuit en vue du dosage des impuretes (1063)

Abstract

The device described was developed with the two following essential conditions in mind: - absence of any pollution during the sampling operation and the transfer to the analysis apparatus; - simultaneous extraction of several samples, each one remaining representative of the sodium in the circuit. The sampling is therefore carried out completely in a vacuum in a Pyrex-glass apparatus, this limiting the sodium temperature to a maximum of 240 deg. C. The samples are in the form of bulbs sealed in vacuo containing 2 to 3 grams of sodium each. The analysis of the oxygen by the amalgamation technique, carried out on samples obtained by this method show a very satisfactory reproducibility for concentrations of under 20 ppm. (authors) [French] Le dispositif decrit a ete mis au point compte tenu des deux imperatifs essentiels suivants: - absence de toute pollution pendant les operations de prelevement et de transport vers l'appareil d'analyse; - obtention simultanee de plusieurs echantillons, chacun restant representatif du sodium du circuit. A cet effet, le prelevement est effectue entierement sous vide dans un appareillage en verre Pyrex, ce qui limite la temperature du sodium a 240 deg. C. Les echantillons se presentent sous la forme d'ampoules scellees  More>>
Authors:
Sannier, J; Vingot, P [1] 
  1. Commissariat a l'Energie Atomique, Saclay (France). Centre d'Etudes Nucleaires
Publication Date:
Jul 01, 1963
Product Type:
Technical Report
Report Number:
CEA-R-2369
Resource Relation:
Other Information: 6 refs
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; COOLANTS; IMPURITIES; LIQUID METALS; MERCURY ALLOYS; OXYGEN; QUANTITATIVE CHEMICAL ANALYSIS; RELIABILITY; SAMPLERS; SAMPLING; SODIUM
OSTI ID:
20818051
Research Organizations:
CEA Saclay, 91 - Gif-sur-Yvette (France)
Country of Origin:
France
Language:
French
Other Identifying Numbers:
TRN: FR06R2369118180
Availability:
Available from INIS in electronic form
Submitting Site:
FRN
Size:
6 pages
Announcement Date:
Jan 04, 2007

Citation Formats

Sannier, J, and Vingot, P. Device for sampling sodium from a circuit with a view to dosing its impurities (1963); Dispositif de prelevement de sodium sur un cuicuit en vue du dosage des impuretes (1063). France: N. p., 1963. Web.
Sannier, J, & Vingot, P. Device for sampling sodium from a circuit with a view to dosing its impurities (1963); Dispositif de prelevement de sodium sur un cuicuit en vue du dosage des impuretes (1063). France.
Sannier, J, and Vingot, P. 1963. "Device for sampling sodium from a circuit with a view to dosing its impurities (1963); Dispositif de prelevement de sodium sur un cuicuit en vue du dosage des impuretes (1063)." France.
@misc{etde_20818051,
title = {Device for sampling sodium from a circuit with a view to dosing its impurities (1963); Dispositif de prelevement de sodium sur un cuicuit en vue du dosage des impuretes (1063)}
author = {Sannier, J, and Vingot, P}
abstractNote = {The device described was developed with the two following essential conditions in mind: - absence of any pollution during the sampling operation and the transfer to the analysis apparatus; - simultaneous extraction of several samples, each one remaining representative of the sodium in the circuit. The sampling is therefore carried out completely in a vacuum in a Pyrex-glass apparatus, this limiting the sodium temperature to a maximum of 240 deg. C. The samples are in the form of bulbs sealed in vacuo containing 2 to 3 grams of sodium each. The analysis of the oxygen by the amalgamation technique, carried out on samples obtained by this method show a very satisfactory reproducibility for concentrations of under 20 ppm. (authors) [French] Le dispositif decrit a ete mis au point compte tenu des deux imperatifs essentiels suivants: - absence de toute pollution pendant les operations de prelevement et de transport vers l'appareil d'analyse; - obtention simultanee de plusieurs echantillons, chacun restant representatif du sodium du circuit. A cet effet, le prelevement est effectue entierement sous vide dans un appareillage en verre Pyrex, ce qui limite la temperature du sodium a 240 deg. C. Les echantillons se presentent sous la forme d'ampoules scellees sous vide et contenant chacune 2 a 3 grammes de sodium. L'analyse de l'oxygene par la technique d'amalgamation, effectuee sur des echantillons preleves par cette methode, revele une reproductibilite tres satisfaisante, dans le domaine des teneurs inferieures a 20 ppm. (auteurs)}
place = {France}
year = {1963}
month = {Jul}
}