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Validation of a method to determine methylmercury in fish tissues using gas chromatography; Validacion de un metodo para determinar metilmercurio en tejido de pescado por cromatografia de gases

Journal Article:

Abstract

We validated a method to determine methylmercury in fish tissues using gas chromatography with an electron capture detector as described by the Association of Official Analytical Chemist (AOAC) International. The linear curve range was 0.02 to 1 g/ml and linear correlation coefficient was 0.9979. A 1 mg/kg methylmercury-contaminated fish sample was analyzed 20 times to determine repeatability of the method. The quantification limit was 0.16 mg/kg and detection limit was 0.06 ppm. Fish samples contaminated with 0.2 to 10 mg/kg methylmercury showed recovery indexes from 94.66 to 108.8%.
Authors:
Vega Bolannos, Luisa O; Arias Verdes, Jose A; Beltran Llerandi, Gilberto; Castro Diaz, Odalys; Moreno Tellez, Olga L [1] 
  1. Instituto de Nutricion e Higiene de los Alimentos, La Habana (Cuba)
Publication Date:
Jul 01, 2000
Product Type:
Journal Article
Resource Relation:
Journal Name: Revista Cubana de Alimentacion y Nutricion (Online); Journal Volume: 14; Journal Issue: 2
Subject:
60 APPLIED LIFE SCIENCES; CHEMICAL ANALYSIS; FISHES; GAS CHROMATOGRAPHY; METHYLMERCURY; TISSUE EXTRACTS
OSTI ID:
20642804
Country of Origin:
Cuba
Language:
Spanish
Other Identifying Numbers:
Journal ID: ISSN 1561-2929; TRN: CU0500198083725
Availability:
Also available on line at the Web site INFOMED http://bvs.sld.cu/revistas/ali/vol14_2_00/ali05200.htm;INIS
Submitting Site:
INIS
Size:
page(s) 104-108
Announcement Date:
Nov 17, 2005

Journal Article:

Citation Formats

Vega Bolannos, Luisa O, Arias Verdes, Jose A, Beltran Llerandi, Gilberto, Castro Diaz, Odalys, and Moreno Tellez, Olga L. Validation of a method to determine methylmercury in fish tissues using gas chromatography; Validacion de un metodo para determinar metilmercurio en tejido de pescado por cromatografia de gases. Cuba: N. p., 2000. Web.
Vega Bolannos, Luisa O, Arias Verdes, Jose A, Beltran Llerandi, Gilberto, Castro Diaz, Odalys, & Moreno Tellez, Olga L. Validation of a method to determine methylmercury in fish tissues using gas chromatography; Validacion de un metodo para determinar metilmercurio en tejido de pescado por cromatografia de gases. Cuba.
Vega Bolannos, Luisa O, Arias Verdes, Jose A, Beltran Llerandi, Gilberto, Castro Diaz, Odalys, and Moreno Tellez, Olga L. 2000. "Validation of a method to determine methylmercury in fish tissues using gas chromatography; Validacion de un metodo para determinar metilmercurio en tejido de pescado por cromatografia de gases." Cuba.
@misc{etde_20642804,
title = {Validation of a method to determine methylmercury in fish tissues using gas chromatography; Validacion de un metodo para determinar metilmercurio en tejido de pescado por cromatografia de gases}
author = {Vega Bolannos, Luisa O, Arias Verdes, Jose A, Beltran Llerandi, Gilberto, Castro Diaz, Odalys, and Moreno Tellez, Olga L}
abstractNote = {We validated a method to determine methylmercury in fish tissues using gas chromatography with an electron capture detector as described by the Association of Official Analytical Chemist (AOAC) International. The linear curve range was 0.02 to 1 g/ml and linear correlation coefficient was 0.9979. A 1 mg/kg methylmercury-contaminated fish sample was analyzed 20 times to determine repeatability of the method. The quantification limit was 0.16 mg/kg and detection limit was 0.06 ppm. Fish samples contaminated with 0.2 to 10 mg/kg methylmercury showed recovery indexes from 94.66 to 108.8%.}
journal = {Revista Cubana de Alimentacion y Nutricion (Online)}
issue = {2}
volume = {14}
place = {Cuba}
year = {2000}
month = {Jul}
}