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Temperature dependence of composition ratio of Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} film by PLD method

Abstract

We have prepared Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} (Bi-2212) thin films by a pulse laser deposition (PLD) method followed by post-annealing. The thin films were grown on MgO substrates at 400-630 deg. C and 100 mTorr oxygen. They were about 200 nm thick. The crystalline structure of thin films deposited at lower temperature ({approx}470 deg. C) was amorphous. The films deposited at higher temperature ({approx}550 deg. C) began to crystallize (c-axis oriented) but it turned out that Bi decreased with an increase temperature. After deposition, post-annealing were performed at 860-880 deg. C in a tubular furnace with mixed gas (Ar:O{sub 2} = 93:7, 1 atm, 0.2 l/min flow) for 3 h. Bi did not decrease with the increase of post-annealing temperature up to 870 deg. C. The critical temperature of film was 78 K, and the root-mean-square (RMS) roughness in 10 {mu}m square was less than 10 nm.
Publication Date:
Oct 01, 2004
Product Type:
Journal Article
Resource Relation:
Journal Name: Physica. C, Superconductivity; Journal Volume: 412-414; Journal Issue: 1-2; Conference: ISS 2003: 16. International symposium on superconductivity: Advances in superconductivity XVI. Part I, Tsukuba (Japan), 27-29 Oct 2003; Other Information: DOI: 10.1016/j.physc.2004.02.223; PII: S092145340400944X; Copyright (c) 2004 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA); PBD: Oct 2004
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; ANNEALING; BISMUTH COMPOUNDS; CALCIUM COMPOUNDS; CRYSTAL STRUCTURE; CUPRATES; ENERGY BEAM DEPOSITION; LASER RADIATION; MAGNESIUM OXIDES; OXYGEN; PULSED IRRADIATION; ROUGHNESS; STRONTIUM COMPOUNDS; SUBSTRATES; TEMPERATURE DEPENDENCE; THIN FILMS; TRANSITION TEMPERATURE
OSTI ID:
20618562
Country of Origin:
Netherlands
Language:
English
Other Identifying Numbers:
Journal ID: ISSN 0921-4534; PHYCE6; TRN: NL05S0759062060
Submitting Site:
NLN
Size:
page(s) 1354-1357
Announcement Date:
Aug 21, 2005

Citation Formats

Kume, E, Fujino, H, Zhao, X, and Sakai, S. Temperature dependence of composition ratio of Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} film by PLD method. Netherlands: N. p., 2004. Web. doi:10.1016/j.physc.2004.02.223.
Kume, E, Fujino, H, Zhao, X, & Sakai, S. Temperature dependence of composition ratio of Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} film by PLD method. Netherlands. https://doi.org/10.1016/j.physc.2004.02.223
Kume, E, Fujino, H, Zhao, X, and Sakai, S. 2004. "Temperature dependence of composition ratio of Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} film by PLD method." Netherlands. https://doi.org/10.1016/j.physc.2004.02.223.
@misc{etde_20618562,
title = {Temperature dependence of composition ratio of Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} film by PLD method}
author = {Kume, E, Fujino, H, Zhao, X, and Sakai, S}
abstractNote = {We have prepared Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} (Bi-2212) thin films by a pulse laser deposition (PLD) method followed by post-annealing. The thin films were grown on MgO substrates at 400-630 deg. C and 100 mTorr oxygen. They were about 200 nm thick. The crystalline structure of thin films deposited at lower temperature ({approx}470 deg. C) was amorphous. The films deposited at higher temperature ({approx}550 deg. C) began to crystallize (c-axis oriented) but it turned out that Bi decreased with an increase temperature. After deposition, post-annealing were performed at 860-880 deg. C in a tubular furnace with mixed gas (Ar:O{sub 2} = 93:7, 1 atm, 0.2 l/min flow) for 3 h. Bi did not decrease with the increase of post-annealing temperature up to 870 deg. C. The critical temperature of film was 78 K, and the root-mean-square (RMS) roughness in 10 {mu}m square was less than 10 nm.}
doi = {10.1016/j.physc.2004.02.223}
journal = []
issue = {1-2}
volume = {412-414}
journal type = {AC}
place = {Netherlands}
year = {2004}
month = {Oct}
}