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Hydriding properties of the intermetallic compounds Zr(Mn{sub 1-y}Nb{sub y}){sub x} (x=0.97-2.91, y=0-0.208)

Abstract

Pressure-composition (P-C) isotherm and X-ray diffraction measurements on Zr(Mn{sub 1-y}Nb{sub y}){sub x} (x=0.97-2.91, y=0-0.208; 26 charges) have been carried out. The equilibrium pressure decreases and the lattice parameter increases with increasing Nb addition. The hydrogen capacity of non-stoichiometric Zr(Mn{sub 1-y}Nb{sub y}){sub x} (hypo-Zr) is nearly proportional to the total number of Zr2Mn2, ZrNbMn2, Zr2MnNb and ZrMn2Nb interstices. Both vertical stroke {Delta}H{sub A} vertical stroke and vertical stroke {Delta}H{sub D} vertical stroke increase with increasing lattice parameter, with the former showing a clearer dependence than the latter. {Delta}S{sub A} shows a weak dependence on the lattice parameter, but {Delta}S{sub D} shows no dependence at all. Both {Delta}H{sub A}/{Delta}S{sub A} and {Delta}H{sub D}/{Delta}S{sub D} display a strong dependence on the lattice parameters. The degree of slope of the plateau in the P-C isotherm is nearly proportional to vertical stroke {Delta}H vertical stroke {Delta}{sub c}(2{theta}), where {Delta}{sub c}(2{theta}) is the corrected halfwidth of the X-ray diffraction profile. (orig.)
Authors:
Kodama, T; [1]  Kaminaka, H [1] 
  1. Sumitomo Metal Industries Ltd., Hyogo (Japan). Res. and Development Center
Publication Date:
Feb 01, 1996
Product Type:
Journal Article
Reference Number:
SCA: 080201; 360102; PA: CHF-96:0G5910; EDB-96:058408; SN: 96001567307
Resource Relation:
Journal Name: Journal of Alloys and Compounds; Journal Volume: 234; Journal Issue: 1; Other Information: PBD: 1 Feb 1996
Subject:
08 HYDROGEN FUEL; 36 MATERIALS SCIENCE; ZIRCONIUM ALLOYS; HYDRIDATION; MANGANESE ALLOYS; NIOBIUM ALLOYS; STOICHIOMETRY; INTERSTITIALS; DESORPTION; THERMODYNAMIC PROPERTIES; X-RAY DIFFRACTION; HYDROGEN STORAGE; LATTICE PARAMETERS
OSTI ID:
206178
Country of Origin:
Switzerland
Language:
English
Other Identifying Numbers:
Journal ID: JALCEU; ISSN 0925-8388; TRN: CH96G5910
Submitting Site:
CHF
Size:
pp. 93-100
Announcement Date:
Apr 15, 1996

Citation Formats

Kodama, T, and Kaminaka, H. Hydriding properties of the intermetallic compounds Zr(Mn{sub 1-y}Nb{sub y}){sub x} (x=0.97-2.91, y=0-0.208). Switzerland: N. p., 1996. Web. doi:10.1016/0925-8388(95)01935-9.
Kodama, T, & Kaminaka, H. Hydriding properties of the intermetallic compounds Zr(Mn{sub 1-y}Nb{sub y}){sub x} (x=0.97-2.91, y=0-0.208). Switzerland. https://doi.org/10.1016/0925-8388(95)01935-9
Kodama, T, and Kaminaka, H. 1996. "Hydriding properties of the intermetallic compounds Zr(Mn{sub 1-y}Nb{sub y}){sub x} (x=0.97-2.91, y=0-0.208)." Switzerland. https://doi.org/10.1016/0925-8388(95)01935-9.
@misc{etde_206178,
title = {Hydriding properties of the intermetallic compounds Zr(Mn{sub 1-y}Nb{sub y}){sub x} (x=0.97-2.91, y=0-0.208)}
author = {Kodama, T, and Kaminaka, H}
abstractNote = {Pressure-composition (P-C) isotherm and X-ray diffraction measurements on Zr(Mn{sub 1-y}Nb{sub y}){sub x} (x=0.97-2.91, y=0-0.208; 26 charges) have been carried out. The equilibrium pressure decreases and the lattice parameter increases with increasing Nb addition. The hydrogen capacity of non-stoichiometric Zr(Mn{sub 1-y}Nb{sub y}){sub x} (hypo-Zr) is nearly proportional to the total number of Zr2Mn2, ZrNbMn2, Zr2MnNb and ZrMn2Nb interstices. Both vertical stroke {Delta}H{sub A} vertical stroke and vertical stroke {Delta}H{sub D} vertical stroke increase with increasing lattice parameter, with the former showing a clearer dependence than the latter. {Delta}S{sub A} shows a weak dependence on the lattice parameter, but {Delta}S{sub D} shows no dependence at all. Both {Delta}H{sub A}/{Delta}S{sub A} and {Delta}H{sub D}/{Delta}S{sub D} display a strong dependence on the lattice parameters. The degree of slope of the plateau in the P-C isotherm is nearly proportional to vertical stroke {Delta}H vertical stroke {Delta}{sub c}(2{theta}), where {Delta}{sub c}(2{theta}) is the corrected halfwidth of the X-ray diffraction profile. (orig.)}
doi = {10.1016/0925-8388(95)01935-9}
journal = []
issue = {1}
volume = {234}
journal type = {AC}
place = {Switzerland}
year = {1996}
month = {Feb}
}