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Synthesis and stability of new nitrophenol complexes of {sup 99m}Tc as possible hypoxia imaging radiopharmaceuticals; Poluchenie i ustojchivost' novykh nitrofenol'nykh kompleksov {sup 99m}Ts - potentsial'nykh radiofarmpreparatov dlya vizualizatsii gipoksii

Abstract

Seven new nitrophenol derivatives were synthesized; their {sup 99m}Tc complexes (N{sub 2}OS chelates), which are possible hypoxia tumor imaging agents, were prepared by the reaction with [{sup 99m}Tc]NaTcO{sub 4} in the presence of SnCl{sub 2} at pH 10. The in vitro biostabilty of the complexes was evaluated. The purity and stability (in human and rat serum) of the complexes were evaluated by chromatographic methods (TLC, HPLC). The most stable (for more than 6 h) is the complex of {sup 99m}Tc with 3-[3'-N-(2''-hydroxy-5''-nitrobenzylamino)- 2'-hydroxypropyl]-1-methylthiourea.
Authors:
Dzhalilian, A R; Bineshmarvasti, M; [1]  Kumar, P; Vibe, L I [2] 
  1. Departament Tsiklotronnoj I Yadernoj Meditsiny Tsentra Yadernykh Issledovanij dlya Sel'skogo Khozyajstva I Meditsiny, Karadzh (Iran, Islamic Republic of)
  2. Fakul'tet Farmatsevtiki i Farmatsevticheskikh Nauk Universiteta Al'berty, Ehdmonton (Canada)
Publication Date:
Mar 01, 2005
Product Type:
Journal Article
Resource Relation:
Journal Name: Radiokhimiya; Journal Volume: 47; Journal Issue: 2; Other Information: 12 refs., 1 fig., 2 tabs; PBD: Mar 2005
Subject:
38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEAR CHEMISTRY; CHELATES; CHEMICAL COMPOSITION; CHEMICAL PREPARATION; NITRO COMPOUNDS; PHENOLS; RADIOPHARMACEUTICALS; STABILITY; TECHNETIUM 99; TECHNETIUM COMPLEXES
OSTI ID:
20617427
Country of Origin:
Russian Federation
Language:
Russian
Other Identifying Numbers:
Journal ID: ISSN 0033-8311; RADKAU; TRN: RU0501741060656
Submitting Site:
INIS
Size:
page(s) 185-188
Announcement Date:
Aug 21, 2005

Citation Formats

Dzhalilian, A R, Bineshmarvasti, M, Kumar, P, and Vibe, L I. Synthesis and stability of new nitrophenol complexes of {sup 99m}Tc as possible hypoxia imaging radiopharmaceuticals; Poluchenie i ustojchivost' novykh nitrofenol'nykh kompleksov {sup 99m}Ts - potentsial'nykh radiofarmpreparatov dlya vizualizatsii gipoksii. Russian Federation: N. p., 2005. Web.
Dzhalilian, A R, Bineshmarvasti, M, Kumar, P, & Vibe, L I. Synthesis and stability of new nitrophenol complexes of {sup 99m}Tc as possible hypoxia imaging radiopharmaceuticals; Poluchenie i ustojchivost' novykh nitrofenol'nykh kompleksov {sup 99m}Ts - potentsial'nykh radiofarmpreparatov dlya vizualizatsii gipoksii. Russian Federation.
Dzhalilian, A R, Bineshmarvasti, M, Kumar, P, and Vibe, L I. 2005. "Synthesis and stability of new nitrophenol complexes of {sup 99m}Tc as possible hypoxia imaging radiopharmaceuticals; Poluchenie i ustojchivost' novykh nitrofenol'nykh kompleksov {sup 99m}Ts - potentsial'nykh radiofarmpreparatov dlya vizualizatsii gipoksii." Russian Federation.
@misc{etde_20617427,
title = {Synthesis and stability of new nitrophenol complexes of {sup 99m}Tc as possible hypoxia imaging radiopharmaceuticals; Poluchenie i ustojchivost' novykh nitrofenol'nykh kompleksov {sup 99m}Ts - potentsial'nykh radiofarmpreparatov dlya vizualizatsii gipoksii}
author = {Dzhalilian, A R, Bineshmarvasti, M, Kumar, P, and Vibe, L I}
abstractNote = {Seven new nitrophenol derivatives were synthesized; their {sup 99m}Tc complexes (N{sub 2}OS chelates), which are possible hypoxia tumor imaging agents, were prepared by the reaction with [{sup 99m}Tc]NaTcO{sub 4} in the presence of SnCl{sub 2} at pH 10. The in vitro biostabilty of the complexes was evaluated. The purity and stability (in human and rat serum) of the complexes were evaluated by chromatographic methods (TLC, HPLC). The most stable (for more than 6 h) is the complex of {sup 99m}Tc with 3-[3'-N-(2''-hydroxy-5''-nitrobenzylamino)- 2'-hydroxypropyl]-1-methylthiourea.}
journal = []
issue = {2}
volume = {47}
journal type = {AC}
place = {Russian Federation}
year = {2005}
month = {Mar}
}