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Report on the intercomparison of determination of selected radionuclides and trace elements in water (W-1, W-2 and W-3, 1975-76)

Abstract

Water is one of the most common materials which are analyzed for the purpose of monitoring of environmental pollution. While being an apparently 'easy' matrix it can in fact pose serious problems even for an experienced analyst. Trace elements and radionuclides may 'disappear' from aqueous solutions due to adsorption on container walls and some of them due to volatilization, bacterial action, etc. Preconcentration techniques such as evaporation and freeze-drying may also lead to considerable losses of some elements. On the other hand, when the vessels employed for storing the water samples have not been adequately cleaned, some trace elements may be 'added' to the solution. The above mentioned difficulties can probably, at least in part, account for the fact that only a small part of the participating laboratories sent in their results before the original deadline. Even after setting the new deadline (30 January 1976) the results were flowing in very sluggishly over a period of a few months what obviously delayed the preparation of this report. Altogether 46 laboratories participated in the W-1 and W-2 runs and 35 in the W-3 run but only a few determined all or most of radionuclides or trace elements, respectively. The present intercomparisons  More>>
Publication Date:
Dec 01, 1976
Product Type:
Technical Report
Report Number:
IAEA-RL-40
Resource Relation:
Other Information: 13 refs, 28 figs, 32 tabs; PBD: Dec 1976
Subject:
54 ENVIRONMENTAL SCIENCES; AQUATIC ECOSYSTEMS; CONCENTRATION RATIO; CONTAMINATION; INTERLABORATORY COMPARISONS; MARINE SURVEYS; QUALITY CONTROL; RADIOCHEMICAL ANALYSIS; RADIOECOLOGICAL CONCENTRATION; RADIOISOTOPES; SEDIMENTS; TRACE AMOUNTS; WATER; WATER POLLUTION
OSTI ID:
20493896
Research Organizations:
International Atomic Energy Agency, Agency's Laboratories, Analytical Quality Control Services, Seibersdorf (Austria)
Country of Origin:
IAEA
Language:
English
Other Identifying Numbers:
TRN: XA0402432066073
Availability:
Available from INIS in electronic form; Also available on-line: http://www.iaea.org/programmes/aqcs/pdf/a_rl_040.pdf
Submitting Site:
INIS
Size:
65 pages
Announcement Date:
Aug 21, 2004

Citation Formats

None. Report on the intercomparison of determination of selected radionuclides and trace elements in water (W-1, W-2 and W-3, 1975-76). IAEA: N. p., 1976. Web.
None. Report on the intercomparison of determination of selected radionuclides and trace elements in water (W-1, W-2 and W-3, 1975-76). IAEA.
None. 1976. "Report on the intercomparison of determination of selected radionuclides and trace elements in water (W-1, W-2 and W-3, 1975-76)." IAEA.
@misc{etde_20493896,
title = {Report on the intercomparison of determination of selected radionuclides and trace elements in water (W-1, W-2 and W-3, 1975-76)}
author = {None}
abstractNote = {Water is one of the most common materials which are analyzed for the purpose of monitoring of environmental pollution. While being an apparently 'easy' matrix it can in fact pose serious problems even for an experienced analyst. Trace elements and radionuclides may 'disappear' from aqueous solutions due to adsorption on container walls and some of them due to volatilization, bacterial action, etc. Preconcentration techniques such as evaporation and freeze-drying may also lead to considerable losses of some elements. On the other hand, when the vessels employed for storing the water samples have not been adequately cleaned, some trace elements may be 'added' to the solution. The above mentioned difficulties can probably, at least in part, account for the fact that only a small part of the participating laboratories sent in their results before the original deadline. Even after setting the new deadline (30 January 1976) the results were flowing in very sluggishly over a period of a few months what obviously delayed the preparation of this report. Altogether 46 laboratories participated in the W-1 and W-2 runs and 35 in the W-3 run but only a few determined all or most of radionuclides or trace elements, respectively. The present intercomparisons were intended to provide the opportunity of checking up the analytical performance for the laboratories dealing with low level activity measurements in water as well as for those engaged in trace multielement analysis.}
place = {IAEA}
year = {1976}
month = {Dec}
}