You need JavaScript to view this
ETDEWEB   /       /    Comparison study Of H{sub 2}O determination in UO{sub 2} powder by using MEA (Moisture Evaluation Analysis) and KFT (Karl Fischer Titration); Studi banding penentuan kadar H{sub 2}O dalam serbuk UO{sub 2} menggunakan metoda MEA (Moisture Evaluation Analysis) dan KFT (Karl Fischer Titration)

Comparison study Of H{sub 2}O determination in UO{sub 2} powder by using MEA (Moisture Evaluation Analysis) and KFT (Karl Fischer Titration); Studi banding penentuan kadar H{sub 2}O dalam serbuk UO{sub 2} menggunakan metoda MEA (Moisture Evaluation Analysis) dan KFT (Karl Fischer Titration)

Conference:

SAVE / SHARE

XML RIS EndNote CSV/Excel JSON

Abstract

To find out an analytical method to determine H{sub 2}O content in UO{sub 2} powder as fuel elements of power reactors which is simple, economical, precise, and accurate, it is necessary to do comparison study of H{sub 2}O content determination using MEA method which is based on electrolysis process with two helically wound electrodes which contains P{sub 2} O{sub 5} that has function to absorb water steam. The platinum electrodes have a 67 Volt potential on them. The quantity of charge required to electrolyse 0.1 {mu}gr of H{sub 2}O is a constant which is the basic of the electronic measurement. In KFT method is based on volumetric titration using the one component reagent hydronol composite contain all reactants i.e. iodine, sulfur dioxide and imidazole as the base, dissolved in a suitable alcohol. The t- (student) test show that there is no different result significantly between those method. The H{sub 2}O contain obtained is 0.956{+-}0.0095 %, for MEA method and 0.953{+-}0.023 % for KFT method. (author)
Authors:
Farida,; Yudhi, N; Lilis, W; Putro, P K [1] 
  1. Center for Development of Nuclear Fuel and Recycling Technology, National Atomic Energy Agency, Serpong (Indonesia)
Publication Date:
Mar 08, 2000
Product Type:
Conference
Report Number:
INIS-ID-015
Resource Relation:
Conference: 5. Scientific Presentation on Nuclear Fuel Cycle: Development of Nuclear Fuel Cycle Technology in Third Millennium, Presentasi Ilmiah Daur Bahan Bakar Nuklir V: Pengembangan Teknologi Daur Bahan Bakar Nuklir Dalam Menyongsong Milenium Ketiga, Jakarta (Indonesia), 22 Feb 2000; Other Information: 4 refs; 8 figs; PBD: 8 Mar 2000; Related Information: In: Proceeding of the Fifth Scientific Presentation on Nuclear Fuel Cycle: Development of Nuclear Fuel Cycle Technology in Third Millennium, Presentasi Ilmiah Daur Bahan Bakar Nuklir V: Pengembangan Teknologi Daur Bahan Bakar Nuklir Dalam Menyongsong Milenium Ketiga, by Suripto, A.; Sastratenaya, A.S.; Sutarno, D. [National Atomic Energy Agency, Serpong (Indonesia)] [and others], 332 pages.
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; CALIBRATION; FUEL ELEMENTS; GRAVIMETRY; POWDERS; URANIUM; WATER
OSTI ID:
20253719
Research Organizations:
Nuclear Fuel Elements Development Centre, National Atomic Energy Agency, Serpong (Indonesia)
Country of Origin:
Indonesia
Language:
Indonesian
Other Identifying Numbers:
Other: ISSN 1410-1998; TRN: ID0200109023383
Availability:
Available from INIS in electronic form; Also available from Center for Development of Informatics and Computation Technology, National Nuclear Energy Agency, Puspiptek Area, Fax. 62-21-7560923, PO BOX 4274, Jakarta (ID)
Submitting Site:
INIS
Size:
page(s) 86-93
Announcement Date:
Jul 02, 2002

Conference:

SAVE / SHARE

XML RIS EndNote CSV/Excel JSON

Citation Formats

Farida,, Yudhi, N, Lilis, W, and Putro, P K. Comparison study Of H{sub 2}O determination in UO{sub 2} powder by using MEA (Moisture Evaluation Analysis) and KFT (Karl Fischer Titration); Studi banding penentuan kadar H{sub 2}O dalam serbuk UO{sub 2} menggunakan metoda MEA (Moisture Evaluation Analysis) dan KFT (Karl Fischer Titration). Indonesia: N. p., 2000. Web.
Farida,, Yudhi, N, Lilis, W, & Putro, P K. Comparison study Of H{sub 2}O determination in UO{sub 2} powder by using MEA (Moisture Evaluation Analysis) and KFT (Karl Fischer Titration); Studi banding penentuan kadar H{sub 2}O dalam serbuk UO{sub 2} menggunakan metoda MEA (Moisture Evaluation Analysis) dan KFT (Karl Fischer Titration). Indonesia.
Farida,, Yudhi, N, Lilis, W, and Putro, P K. 2000. "Comparison study Of H{sub 2}O determination in UO{sub 2} powder by using MEA (Moisture Evaluation Analysis) and KFT (Karl Fischer Titration); Studi banding penentuan kadar H{sub 2}O dalam serbuk UO{sub 2} menggunakan metoda MEA (Moisture Evaluation Analysis) dan KFT (Karl Fischer Titration)." Indonesia.
@misc{etde_20253719,
title = {Comparison study Of H{sub 2}O determination in UO{sub 2} powder by using MEA (Moisture Evaluation Analysis) and KFT (Karl Fischer Titration); Studi banding penentuan kadar H{sub 2}O dalam serbuk UO{sub 2} menggunakan metoda MEA (Moisture Evaluation Analysis) dan KFT (Karl Fischer Titration)}
 author = {Farida,, Yudhi, N, Lilis, W, and Putro, P K}
 abstractNote = {To find out an analytical method to determine H{sub 2}O content in UO{sub 2} powder as fuel elements of power reactors which is simple, economical, precise, and accurate, it is necessary to do comparison study of H{sub 2}O content determination using MEA method which is based on electrolysis process with two helically wound electrodes which contains P{sub 2} O{sub 5} that has function to absorb water steam. The platinum electrodes have a 67 Volt potential on them. The quantity of charge required to electrolyse 0.1 {mu}gr of H{sub 2}O is a constant which is the basic of the electronic measurement. In KFT method is based on volumetric titration using the one component reagent hydronol composite contain all reactants i.e. iodine, sulfur dioxide and imidazole as the base, dissolved in a suitable alcohol. The t- (student) test show that there is no different result significantly between those method. The H{sub 2}O contain obtained is 0.956{+-}0.0095 %, for MEA method and 0.953{+-}0.023 % for KFT method. (author)}
 place = {Indonesia}
 year = {2000}
 month = {Mar}
 }