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Thermal stability and ionic conductivity of polymeric complexes Pva-KHSO4; Estabilidad termica y conductividad ionica de los complejos polimericos PVA-KHSO4

Abstract

Its had synthesized highly conductive thin films of polymeric electrolytes, based on commercial glue (BASF's colbon) and KHSO4 salt, by means the solving casting method, using H3PO2 as common solvent. By high resolution thermal analysis and impedance spectroscopy we found that these complexes are highly amorphous and thermally stable in the 160 - 450 K temperature range. The glass transition temperature, Tg, varies with the salt concentration. The highest electrical conductivity at ambient temperature is obtained for x=0.16 salt concentration (on the higher concentrations range) and its value is around 10-2 (gamma cm)-1 , one of the highest reported in the literature for this type of compounds.
Publication Date:
Jul 01, 1996
Product Type:
Journal Article
Reference Number:
EDB-00:074754
Resource Relation:
Journal Name: Revista Colombiana de Fisica; Journal Volume: 28; Journal Issue: 2; Other Information: PBD: 1996
Subject:
36 MATERIALS SCIENCE; AMORPHOUS STATE; CHEMICAL PREPARATION; ELECTRIC IMPEDANCE; ELECTROLYTES; FILMS; IONIC CONDUCTIVITY; PVA; SENSITIVITY; THERMAL DEGRADATION
OSTI ID:
20031754
Country of Origin:
Colombia
Language:
Spanish
Other Identifying Numbers:
Journal ID: ISSN 0120-2650; TRN: CO9900033001682
Submitting Site:
INIS
Size:
page(s) 305-308
Announcement Date:
Sep 17, 2000

Citation Formats

Vargas, R A, Vargas, M A, and Garcia, A. Thermal stability and ionic conductivity of polymeric complexes Pva-KHSO4; Estabilidad termica y conductividad ionica de los complejos polimericos PVA-KHSO4. Colombia: N. p., 1996. Web.
Vargas, R A, Vargas, M A, & Garcia, A. Thermal stability and ionic conductivity of polymeric complexes Pva-KHSO4; Estabilidad termica y conductividad ionica de los complejos polimericos PVA-KHSO4. Colombia.
Vargas, R A, Vargas, M A, and Garcia, A. 1996. "Thermal stability and ionic conductivity of polymeric complexes Pva-KHSO4; Estabilidad termica y conductividad ionica de los complejos polimericos PVA-KHSO4." Colombia.
@misc{etde_20031754,
title = {Thermal stability and ionic conductivity of polymeric complexes Pva-KHSO4; Estabilidad termica y conductividad ionica de los complejos polimericos PVA-KHSO4}
author = {Vargas, R A, Vargas, M A, and Garcia, A}
abstractNote = {Its had synthesized highly conductive thin films of polymeric electrolytes, based on commercial glue (BASF's colbon) and KHSO4 salt, by means the solving casting method, using H3PO2 as common solvent. By high resolution thermal analysis and impedance spectroscopy we found that these complexes are highly amorphous and thermally stable in the 160 - 450 K temperature range. The glass transition temperature, Tg, varies with the salt concentration. The highest electrical conductivity at ambient temperature is obtained for x=0.16 salt concentration (on the higher concentrations range) and its value is around 10-2 (gamma cm)-1 , one of the highest reported in the literature for this type of compounds.}
journal = []
issue = {2}
volume = {28}
journal type = {AC}
place = {Colombia}
year = {1996}
month = {Jul}
}