Abstract
The nuclear magnetic resonance (NMR) techniques for High Resolution Spectroscopy in Solids are described. Also the construction project of a partially home made spectrometer and its applications in the characterization of solid samples are shown in detail. The high resolution spectrometer used is implemented with the double resonance multiple pulses sequences and magic angle spinning (MAS) and can be used with solid and liquid samples. The maximum spinning frequency for the MAS experiment is in excess of 5 Khz, the double resonance sequences can be performed with any type of nucleus, in the variable temperature operating range with nitrogen gas: -120{sup 0} C to +160{sup 0} C, and is fully controlled by a Macintosh IIci microcomputer. (author).
Citation Formats
Bonagamba, T J.
High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear.
Brazil: N. p.,
1991.
Web.
Bonagamba, T J.
High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear.
Brazil.
Bonagamba, T J.
1991.
"High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear."
Brazil.
@misc{etde_10168611,
title = {High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear}
author = {Bonagamba, T J}
abstractNote = {The nuclear magnetic resonance (NMR) techniques for High Resolution Spectroscopy in Solids are described. Also the construction project of a partially home made spectrometer and its applications in the characterization of solid samples are shown in detail. The high resolution spectrometer used is implemented with the double resonance multiple pulses sequences and magic angle spinning (MAS) and can be used with solid and liquid samples. The maximum spinning frequency for the MAS experiment is in excess of 5 Khz, the double resonance sequences can be performed with any type of nucleus, in the variable temperature operating range with nitrogen gas: -120{sup 0} C to +160{sup 0} C, and is fully controlled by a Macintosh IIci microcomputer. (author).}
place = {Brazil}
year = {1991}
month = {Jul}
}
title = {High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear}
author = {Bonagamba, T J}
abstractNote = {The nuclear magnetic resonance (NMR) techniques for High Resolution Spectroscopy in Solids are described. Also the construction project of a partially home made spectrometer and its applications in the characterization of solid samples are shown in detail. The high resolution spectrometer used is implemented with the double resonance multiple pulses sequences and magic angle spinning (MAS) and can be used with solid and liquid samples. The maximum spinning frequency for the MAS experiment is in excess of 5 Khz, the double resonance sequences can be performed with any type of nucleus, in the variable temperature operating range with nitrogen gas: -120{sup 0} C to +160{sup 0} C, and is fully controlled by a Macintosh IIci microcomputer. (author).}
place = {Brazil}
year = {1991}
month = {Jul}
}