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High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear

Thesis/Dissertation:

Abstract

The nuclear magnetic resonance (NMR) techniques for High Resolution Spectroscopy in Solids are described. Also the construction project of a partially home made spectrometer and its applications in the characterization of solid samples are shown in detail. The high resolution spectrometer used is implemented with the double resonance multiple pulses sequences and magic angle spinning (MAS) and can be used with solid and liquid samples. The maximum spinning frequency for the MAS experiment is in excess of 5 Khz, the double resonance sequences can be performed with any type of nucleus, in the variable temperature operating range with nitrogen gas: -120{sup 0} C to +160{sup 0} C, and is fully controlled by a Macintosh IIci microcomputer. (author).
Authors:
Publication Date:
Jul 01, 1991
Product Type:
Thesis/Dissertation
Report Number:
INIS-BR-3354
Reference Number:
SCA: 665100; PA: AIX-25:050849; EDB-94:113355; ERA-19:026707; NTS-95:002868; SN: 94001055333
Resource Relation:
Other Information: TH: Tese (Ph.D.).; PBD: Jul 1991
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; SOLIDS; SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE; MEASURING METHODS; SPECTROMETERS; STRUCTURAL CHEMICAL ANALYSIS; 665100; NUCLEAR TECHNIQUES IN CONDENSED MATTER PHYSICS
OSTI ID:
10168611
Research Organizations:
Sao Paulo Univ., Sao Carlos, SP (Brazil). Inst. de Fisica e Quimica
Country of Origin:
Brazil
Language:
Portuguese
Other Identifying Numbers:
Other: ON: DE94631464; TRN: BR9432102050849
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
INIS
Size:
149 p.
Announcement Date:

Thesis/Dissertation:

Citation Formats

Bonagamba, T J. High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear. Brazil: N. p., 1991. Web.
Bonagamba, T J. High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear. Brazil.
Bonagamba, T J. 1991. "High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear." Brazil.
@misc{etde_10168611,
title = {High resolution spectroscopy in solids by nuclear magnetic resonance; Espectroscopia de alta resolucao em solidos por ressonancia magnetica nuclear}
author = {Bonagamba, T J}
abstractNote = {The nuclear magnetic resonance (NMR) techniques for High Resolution Spectroscopy in Solids are described. Also the construction project of a partially home made spectrometer and its applications in the characterization of solid samples are shown in detail. The high resolution spectrometer used is implemented with the double resonance multiple pulses sequences and magic angle spinning (MAS) and can be used with solid and liquid samples. The maximum spinning frequency for the MAS experiment is in excess of 5 Khz, the double resonance sequences can be performed with any type of nucleus, in the variable temperature operating range with nitrogen gas: -120{sup 0} C to +160{sup 0} C, and is fully controlled by a Macintosh IIci microcomputer. (author).}
place = {Brazil}
year = {1991}
month = {Jul}
}