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Determination of hafnium and zirconium in geological materials by neutron activation analysis; Determinacao de hafnio e zirconio em materiais geologicos por analise por ativacao com neutrons

Abstract

In this paper, neutron activation analysis was developed for determining hafnium and zirconium in geological materials. The USGS geological standard rocks GSP-1 (granodiorite) and W-1 (di abase). The Brazilian geological standards GB-1 (granite) and BB-1 (basalt) from Instituto de Geociencias da Universidade da Bahia and P-1 a uraniferous rock from Pocos de Caldas, MG, Brazil were analyzed. Hafnium present in these rocks was analyzed by purely instrumental method by irradiating with both thermal and epithermal neutrons from IEA-R1 nuclear research reactor. In the case of zirconium depending on the sample a radiochemical separation was required. {sup 154} Eu and {sup 152} Eu radioisotopes emit gamma rays with energies too close to those emitted by {sup 95} Zr and they cause interferences. (author).
Authors:
Publication Date:
Dec 31, 1992
Product Type:
Thesis/Dissertation
Report Number:
INIS-BR-3120
Reference Number:
SCA: 540211; 400101; PA: AIX-24:044629; SN: 93000988718
Resource Relation:
Other Information: TH: Tese (M.Sc.).; PBD: 1992
Subject:
54 ENVIRONMENTAL SCIENCES; 37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; HAFNIUM; NEUTRON ACTIVATION ANALYSIS; ZIRCONIUM; ION EXCHANGE; EXPERIMENTAL DATA; FISSION PRODUCTS; ROCKS; STANDARDIZATION; ZIRCONIUM 95; 540211; 400101; RADIOMETRIC TECHNIQUES; ACTIVATION, NUCLEAR REACTION, RADIOMETRIC, AND RADIOCHEMICAL PROCEDURES
OSTI ID:
10152208
Research Organizations:
Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil)
Country of Origin:
Brazil
Language:
Portuguese
Other Identifying Numbers:
Other: ON: DE93624521; TRN: BR9331134044629
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
INIS
Size:
[75] p.
Announcement Date:
Jul 05, 2005

Citation Formats

Lins, J P. Determination of hafnium and zirconium in geological materials by neutron activation analysis; Determinacao de hafnio e zirconio em materiais geologicos por analise por ativacao com neutrons. Brazil: N. p., 1992. Web.
Lins, J P. Determination of hafnium and zirconium in geological materials by neutron activation analysis; Determinacao de hafnio e zirconio em materiais geologicos por analise por ativacao com neutrons. Brazil.
Lins, J P. 1992. "Determination of hafnium and zirconium in geological materials by neutron activation analysis; Determinacao de hafnio e zirconio em materiais geologicos por analise por ativacao com neutrons." Brazil.
@misc{etde_10152208,
title = {Determination of hafnium and zirconium in geological materials by neutron activation analysis; Determinacao de hafnio e zirconio em materiais geologicos por analise por ativacao com neutrons}
author = {Lins, J P}
abstractNote = {In this paper, neutron activation analysis was developed for determining hafnium and zirconium in geological materials. The USGS geological standard rocks GSP-1 (granodiorite) and W-1 (di abase). The Brazilian geological standards GB-1 (granite) and BB-1 (basalt) from Instituto de Geociencias da Universidade da Bahia and P-1 a uraniferous rock from Pocos de Caldas, MG, Brazil were analyzed. Hafnium present in these rocks was analyzed by purely instrumental method by irradiating with both thermal and epithermal neutrons from IEA-R1 nuclear research reactor. In the case of zirconium depending on the sample a radiochemical separation was required. {sup 154} Eu and {sup 152} Eu radioisotopes emit gamma rays with energies too close to those emitted by {sup 95} Zr and they cause interferences. (author).}
place = {Brazil}
year = {1992}
month = {Dec}
}