You need JavaScript to view this

Spectrophotometric determination of vanadium after extraction of V(IV)-8-hydroxyquinoline complex into methyl isobutyl ketone

Abstract

A simple, rapid and cheap method for the determination of vanadium on trace amounts has been worked out. Employing sodium sulphide as reductant, pentavalent vanadium is reduced to tetravalent which forms reddish brown complex with oxine in hydrochloric acid solution in the presence of sodium acetate. The coloured species is quantitatively extracted into methyl isobutyl ketone and absorbance is measured at 430 nm. The method is free from the interference of Mo, Mn, Cr, Ni, Ag, W, U, Zn, Re, Os, Pt, Pd, Ru and Rh. (author). 16 refs, 1 fig., 2 tabs.
Authors:
Chauhan, A R.S.; Kakkar, L R [1] 
  1. Kurukshetra Univ. (India). Dept. of Chemistry
Publication Date:
Dec 31, 1994
Product Type:
Journal Article
Reference Number:
SCA: 400105; PA: AIX-26:058514; EDB-95:131000; SN: 95001461671
Resource Relation:
Journal Name: Chemia Analityczna; Journal Volume: 39; Journal Issue: 5; Other Information: PBD: 1994
Subject:
40 CHEMISTRY; VANADIUM IONS; COMPLEXES; SOLVENT EXTRACTION; VISIBLE SPECTRA; METHYL ISOBUTYL KETONE; QUINOLINES; SPECTROPHOTOMETRY
OSTI ID:
101519
Country of Origin:
Poland
Language:
English
Other Identifying Numbers:
Journal ID: CANWAJ; ISSN 0009-2223; TRN: PL9500291058514
Submitting Site:
PLN
Size:
pp. 585-589
Announcement Date:
Oct 06, 1995

Citation Formats

Chauhan, A R.S., and Kakkar, L R. Spectrophotometric determination of vanadium after extraction of V(IV)-8-hydroxyquinoline complex into methyl isobutyl ketone. Poland: N. p., 1994. Web.
Chauhan, A R.S., & Kakkar, L R. Spectrophotometric determination of vanadium after extraction of V(IV)-8-hydroxyquinoline complex into methyl isobutyl ketone. Poland.
Chauhan, A R.S., and Kakkar, L R. 1994. "Spectrophotometric determination of vanadium after extraction of V(IV)-8-hydroxyquinoline complex into methyl isobutyl ketone." Poland.
@misc{etde_101519,
title = {Spectrophotometric determination of vanadium after extraction of V(IV)-8-hydroxyquinoline complex into methyl isobutyl ketone}
author = {Chauhan, A R.S., and Kakkar, L R}
abstractNote = {A simple, rapid and cheap method for the determination of vanadium on trace amounts has been worked out. Employing sodium sulphide as reductant, pentavalent vanadium is reduced to tetravalent which forms reddish brown complex with oxine in hydrochloric acid solution in the presence of sodium acetate. The coloured species is quantitatively extracted into methyl isobutyl ketone and absorbance is measured at 430 nm. The method is free from the interference of Mo, Mn, Cr, Ni, Ag, W, U, Zn, Re, Os, Pt, Pd, Ru and Rh. (author). 16 refs, 1 fig., 2 tabs.}
journal = []
issue = {5}
volume = {39}
journal type = {AC}
place = {Poland}
year = {1994}
month = {Dec}
}