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Errors of absolute methods of reactor neutron activation analysis caused by non-1/E epithermal neutron spectra. The influence of the errors of the activities of the flux monitors when using the bare triple monitor method with {sup 94}Zr, {sup 96}Zr and {sup 197}Au

Abstract

A sufficiently accurate characterization of the neutron flux and spectrum, i.e. the determination of the thermal flux, the flux ratio and the epithermal flux spectrum shape factor, {alpha}, is a prerequisite for all types of absolute and monostandard methods of reactor neutron activation analysis. A convenient method for these measurements is the bare triple monitor method. However, the results of this method, are very imprecise, because there are high error propagation factors form the counting errors of the monitor activities. Procedures are described to calculate the errors of the flux parameters, the {alpha}-dependent cross-section ratios, and of the analytical results from the errors of the activities of the monitor isotopes. They are included in FORTRAN programs which also allow a graphical representation of the results. A great number of examples were calculated for ten different irradiation facilities in four reactors and for 28 elements. Plots of the results are presented and discussed. (orig./HP) [Deutsch] Eine Voraussetzung fuer die Anwendung von Absolut- und Monostandardmethoden der Reaktorneutronenaktivierungsanalyse ist eine hinreichend genaue Charakterisierung der Neutronenflussdichte und des Neutronenspektrums, d.h. der thermischen Flussdichte, des Flussverhaeltnisses und des Formfaktors fuer das epithermische Neutronenspektrum, {alpha}. Diese Messungen koennen einfach und direkt mit der `Bare-Triple-Monitor-Methode` ausgefuehrt werden.  More>>
Authors:
Publication Date:
Aug 01, 1993
Product Type:
Technical Report
Report Number:
Juel-2808
Reference Number:
SCA: 400101; PA: DEN-94:0F4415; EDB-94:064496; NTS-94:020574; SN: 94001185735
Resource Relation:
Other Information: PBD: Aug 1993
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; NEUTRON ACTIVATION ANALYSIS; ACCURACY; ERRORS; CORRECTIONS; EPITHERMAL NEUTRONS; NEUTRON FLUX; ACTIVATION DETECTORS; RESEARCH REACTORS; 400101; ACTIVATION, NUCLEAR REACTION, RADIOMETRIC, AND RADIOCHEMICAL PROCEDURES
OSTI ID:
10141578
Research Organizations:
Forschungszentrum Juelich GmbH (Germany). Zentralabteilung fuer Chemische Analysen
Country of Origin:
Germany
Language:
English
Other Identifying Numbers:
Journal ID: ISSN 0944-2952; Other: ON: DE94758738; TRN: DE94F4415
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
DEN
Size:
88 p.
Announcement Date:
Jul 05, 2005

Citation Formats

Erdtmann, G. Errors of absolute methods of reactor neutron activation analysis caused by non-1/E epithermal neutron spectra. The influence of the errors of the activities of the flux monitors when using the bare triple monitor method with {sup 94}Zr, {sup 96}Zr and {sup 197}Au. Germany: N. p., 1993. Web.
Erdtmann, G. Errors of absolute methods of reactor neutron activation analysis caused by non-1/E epithermal neutron spectra. The influence of the errors of the activities of the flux monitors when using the bare triple monitor method with {sup 94}Zr, {sup 96}Zr and {sup 197}Au. Germany.
Erdtmann, G. 1993. "Errors of absolute methods of reactor neutron activation analysis caused by non-1/E epithermal neutron spectra. The influence of the errors of the activities of the flux monitors when using the bare triple monitor method with {sup 94}Zr, {sup 96}Zr and {sup 197}Au." Germany.
@misc{etde_10141578,
title = {Errors of absolute methods of reactor neutron activation analysis caused by non-1/E epithermal neutron spectra. The influence of the errors of the activities of the flux monitors when using the bare triple monitor method with {sup 94}Zr, {sup 96}Zr and {sup 197}Au}
author = {Erdtmann, G}
abstractNote = {A sufficiently accurate characterization of the neutron flux and spectrum, i.e. the determination of the thermal flux, the flux ratio and the epithermal flux spectrum shape factor, {alpha}, is a prerequisite for all types of absolute and monostandard methods of reactor neutron activation analysis. A convenient method for these measurements is the bare triple monitor method. However, the results of this method, are very imprecise, because there are high error propagation factors form the counting errors of the monitor activities. Procedures are described to calculate the errors of the flux parameters, the {alpha}-dependent cross-section ratios, and of the analytical results from the errors of the activities of the monitor isotopes. They are included in FORTRAN programs which also allow a graphical representation of the results. A great number of examples were calculated for ten different irradiation facilities in four reactors and for 28 elements. Plots of the results are presented and discussed. (orig./HP) [Deutsch] Eine Voraussetzung fuer die Anwendung von Absolut- und Monostandardmethoden der Reaktorneutronenaktivierungsanalyse ist eine hinreichend genaue Charakterisierung der Neutronenflussdichte und des Neutronenspektrums, d.h. der thermischen Flussdichte, des Flussverhaeltnisses und des Formfaktors fuer das epithermische Neutronenspektrum, {alpha}. Diese Messungen koennen einfach und direkt mit der `Bare-Triple-Monitor-Methode` ausgefuehrt werden. Die Ergebnisse sind jedoch ungenau, denn Fehler bei der Bestimmung der Aktivitaeten der Flussmonitore, z.B. statistische Zaehlfehler oder Ungenauigkeiten in der Eichkurve fuer die {gamma}-Zaehlausbeuten, werden mit hohen Fehlerfortpflanzungsfaktoren auf die Ergebnisse uebertragen. Es werden Verfahren beschrieben, um die Fehler der Flussparameter, der {alpha}-abhaengigen Aktivierungsquerschnittsverhaeltnisse, und der Analysenergebnisse aus den Fehlern der Aktivitaeten der Flussmonitore abzuschaetzen. Dafuer wurden FORTRAN-Programme geschrieben, die auch eine graphische Darstellung der Ergebnisse erlauben. Eine grosse Anzahl von Beispielen wurde durchgerechnet, wobei zehn verschiedene Bestrahlungseinrichtungen an vier Reaktoren, und 28 Elemente, bzw. (n, {gamma})-Reaktionen, beruecksichtigt worden sind. Die Ergebnisse sind graphisch dargestellt und sie werden diskutiert. (orig./HP)}
place = {Germany}
year = {1993}
month = {Aug}
}