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Determination of 7 trace elements in nuclear pure uranium dioxide by ICP-AES

Abstract

The 237 quaternary ammonium extraction resin and extraction chromatography technique were used to separate 7 trace elements in nuclear pure uranium dioxide. The sample was separated at a flow rate of 0.7 ml/min with 6.5 mol/L HNO{sub 3} as medium. A model of 975 ICP direct reading spectrometer was used to determine trace elements of Ba, Be, Nb, Ru, Sb, Sn and Ta in nuclear pure uranium dioxide. The determination limits are 0.013 {mu}g/g {approx} 0.50 {mu}g/g. The recovery rates are 98% {approx} 103% and the relative standard deviation is less than 5%.
Authors:
Husheng, Liu [1] 
  1. Beijing Research Inst. of Chemical Engineering and Metallurgy (China)
Publication Date:
May 01, 1993
Product Type:
Technical Report
Report Number:
CNIC-00747; BICM-0010.
Reference Number:
SCA: 400102; 400105; 050700; PA: AIX-25:027404; EDB-94:054703; NTS-94:018422; SN: 94001177185
Resource Relation:
Other Information: PBD: May 1993
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; 11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS; QUATERNARY COMPOUNDS; EXTRACTION CHROMATOGRAPHY; URANIUM DIOXIDE; EMISSION SPECTROSCOPY; MULTI-ELEMENT ANALYSIS; IMPURITIES; ACCURACY; ELEMENTS; NITRIC ACID; PLASMA HEATING; SENSITIVITY; 400102; 400105; 050700; CHEMICAL AND SPECTRAL PROCEDURES; SEPARATION PROCEDURES; FUELS PRODUCTION AND PROPERTIES
OSTI ID:
10139688
Research Organizations:
China Nuclear Information Centre, Beijing, BJ (China)
Country of Origin:
China
Language:
Chinese
Other Identifying Numbers:
Other: ON: DE94620277; ISBN 7-5022-0935-2; TRN: CN9400200027404
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
INIS
Size:
7 p.
Announcement Date:
Jul 05, 2005

Citation Formats

Husheng, Liu. Determination of 7 trace elements in nuclear pure uranium dioxide by ICP-AES. China: N. p., 1993. Web.
Husheng, Liu. Determination of 7 trace elements in nuclear pure uranium dioxide by ICP-AES. China.
Husheng, Liu. 1993. "Determination of 7 trace elements in nuclear pure uranium dioxide by ICP-AES." China.
@misc{etde_10139688,
title = {Determination of 7 trace elements in nuclear pure uranium dioxide by ICP-AES}
author = {Husheng, Liu}
abstractNote = {The 237 quaternary ammonium extraction resin and extraction chromatography technique were used to separate 7 trace elements in nuclear pure uranium dioxide. The sample was separated at a flow rate of 0.7 ml/min with 6.5 mol/L HNO{sub 3} as medium. A model of 975 ICP direct reading spectrometer was used to determine trace elements of Ba, Be, Nb, Ru, Sb, Sn and Ta in nuclear pure uranium dioxide. The determination limits are 0.013 {mu}g/g {approx} 0.50 {mu}g/g. The recovery rates are 98% {approx} 103% and the relative standard deviation is less than 5%.}
place = {China}
year = {1993}
month = {May}
}