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Raman spectroscopic investigation of lanthanides and actinides complexation by pyridine-2-carboxamide

Abstract

Pyridine 2 - carboxamides - more commonly named picolinamides - are studied in CEA Fontenay-aux-Roses. Their possible ability to separate Actinides from Lanthanides could make them interesting in nuclear wastes processing. We have undertaken a Raman spectroscopic investigation of the reactions of unsubstituted picolinamides with the proton and 4f and 5f metallic cations in aqueous solution because pyridine 2 - carboxamide: - is fairly soluble in water, where Raman Spectroscopy is a good investigation method for studying complexation reactions, - possess strong characteristic vibrations: (a) pyridine cycle vibrations at 1000 and 1046 cm{sup -1}. (b) C = O bond vibration around 1675 cm{sup -1}, sensitive to complexation with proton and metallic ions. For more convenience we have worked in chloride media instead of the more frequent nitrate medium to prevent the strong disturbing nitrate vibration at 1047 cm{sup -1}. (author).
Publication Date:
Dec 31, 1993
Product Type:
Conference
Report Number:
CEA-CONF-11687; CONF-9304213-
Reference Number:
SCA: 400105; PA: AIX-25:020933; EDB-94:054735; ERA-19:012635; NTS-94:017821; SN: 94001170848
Resource Relation:
Conference: Actinides meeting,Buehl (Germany),20-23 Apr 1993; Other Information: PBD: 1993
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; RADIOACTIVE WASTE PROCESSING; ACTINIDES; PYRIDINE; RAMAN SPECTROSCOPY; RARE EARTHS; 400105; SEPARATION PROCEDURES
OSTI ID:
10138051
Research Organizations:
CEA Centre d`Etudes de la Vallee du Rhone, 30 - Marcoule (France). Dept. des Procedes de Retraitement
Country of Origin:
France
Language:
English
Other Identifying Numbers:
Other: ON: DE94617429; TRN: FR9401772020933
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
FRN
Size:
10 p.
Announcement Date:
Jul 05, 2005

Citation Formats

Livet, J, Cordier, P Y, and Condamines, N. Raman spectroscopic investigation of lanthanides and actinides complexation by pyridine-2-carboxamide. France: N. p., 1993. Web.
Livet, J, Cordier, P Y, & Condamines, N. Raman spectroscopic investigation of lanthanides and actinides complexation by pyridine-2-carboxamide. France.
Livet, J, Cordier, P Y, and Condamines, N. 1993. "Raman spectroscopic investigation of lanthanides and actinides complexation by pyridine-2-carboxamide." France.
@misc{etde_10138051,
title = {Raman spectroscopic investigation of lanthanides and actinides complexation by pyridine-2-carboxamide}
author = {Livet, J, Cordier, P Y, and Condamines, N}
abstractNote = {Pyridine 2 - carboxamides - more commonly named picolinamides - are studied in CEA Fontenay-aux-Roses. Their possible ability to separate Actinides from Lanthanides could make them interesting in nuclear wastes processing. We have undertaken a Raman spectroscopic investigation of the reactions of unsubstituted picolinamides with the proton and 4f and 5f metallic cations in aqueous solution because pyridine 2 - carboxamide: - is fairly soluble in water, where Raman Spectroscopy is a good investigation method for studying complexation reactions, - possess strong characteristic vibrations: (a) pyridine cycle vibrations at 1000 and 1046 cm{sup -1}. (b) C = O bond vibration around 1675 cm{sup -1}, sensitive to complexation with proton and metallic ions. For more convenience we have worked in chloride media instead of the more frequent nitrate medium to prevent the strong disturbing nitrate vibration at 1047 cm{sup -1}. (author).}
place = {France}
year = {1993}
month = {Dec}
}