You need JavaScript to view this

Studies of some reactions between uranyl halides and hydrocarbyl anions

Abstract

Reactions of uranyl halides (UO sub 2 X sub 2) with hydrocarbyl anions of the type (R=Ar sup - or Ar sub n H sub 3 sub - sub n C sup -), result in the formation of thermally unstable intermediates ([UO sub 2 R sub 2 X sub 2] sup - sup 2) which undergo thermolysis to give uranium dioxide and organic products. The type of organic product obtained depends on the thermolysis pathway of the intermediate. If the intermediate thermolysis occurs via H-abstraction, the monomer RH is formed, and if thermolysis occurs via reductive elimination (coupling) the dimer R-R is obtained. The thermolysis pathways, the yield of organic products, and the type of these products are discussed on the basis of electronic and steric factors. When the hydrocarbyl group used is benzilic, the main factor that controls reactivity is found to be electronic. On the other hand, the steric factor is the main factor that controls the reactivity in the case of phenolic type hydrocarbyls. Differences in reactivity between uranyl chloride and uranyl bromide towards hydrocarbyl anions are discussed. 25 refs., 2 figs., 3 tabs. (A.M.H.).
Authors:
Publication Date:
Apr 01, 1987
Product Type:
Thesis/Dissertation
Report Number:
INIS-mf-13488
Reference Number:
SCA: 400201; PA: AIX-24:028973; SN: 93000955368
Resource Relation:
Other Information: TH: Thesis (M.Sc.).; PBD: Apr 1987
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; URANYL COMPOUNDS; CHEMICAL REACTIONS; ANIONS; DIMERS; MONOMERS; ORGANIC COMPOUNDS; REACTION INTERMEDIATES; URANIUM; 400201; CHEMICAL AND PHYSICOCHEMICAL PROPERTIES
OSTI ID:
10133742
Research Organizations:
University of Jordan, Amman (Jordan)
Country of Origin:
Jordan
Language:
English
Other Identifying Numbers:
Other: ON: DE93618985; TRN: JO9300014028973
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
INIS
Size:
[55] p.
Announcement Date:
Jul 04, 2005

Citation Formats

Alarouri, A. Studies of some reactions between uranyl halides and hydrocarbyl anions. Jordan: N. p., 1987. Web.
Alarouri, A. Studies of some reactions between uranyl halides and hydrocarbyl anions. Jordan.
Alarouri, A. 1987. "Studies of some reactions between uranyl halides and hydrocarbyl anions." Jordan.
@misc{etde_10133742,
title = {Studies of some reactions between uranyl halides and hydrocarbyl anions}
author = {Alarouri, A}
abstractNote = {Reactions of uranyl halides (UO sub 2 X sub 2) with hydrocarbyl anions of the type (R=Ar sup - or Ar sub n H sub 3 sub - sub n C sup -), result in the formation of thermally unstable intermediates ([UO sub 2 R sub 2 X sub 2] sup - sup 2) which undergo thermolysis to give uranium dioxide and organic products. The type of organic product obtained depends on the thermolysis pathway of the intermediate. If the intermediate thermolysis occurs via H-abstraction, the monomer RH is formed, and if thermolysis occurs via reductive elimination (coupling) the dimer R-R is obtained. The thermolysis pathways, the yield of organic products, and the type of these products are discussed on the basis of electronic and steric factors. When the hydrocarbyl group used is benzilic, the main factor that controls reactivity is found to be electronic. On the other hand, the steric factor is the main factor that controls the reactivity in the case of phenolic type hydrocarbyls. Differences in reactivity between uranyl chloride and uranyl bromide towards hydrocarbyl anions are discussed. 25 refs., 2 figs., 3 tabs. (A.M.H.).}
place = {Jordan}
year = {1987}
month = {Apr}
}