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The dissolution properties of LiCoO{sub 2} in molten 62:38 mole% Li:K carbonate

Abstract

The lifetime of a Molten Carbonate Fuel Cell (MCFC) is reduced by the slow dissolution of the state-of-the-art lithiated nickel oxide cathode material. LiCoO{sub 2} is considered to be an alternative cathode material by its good performance in MCFC tests. However, its dissolution rate was not known. In this letter the dissolution properties of LiCoO{sub 2} in 62:38 (Li:K){sub 2}CO{sub 3} at 923K are reported. The concentration of the dissolved Co{sup 2+} ions in the molten carbonate was determined electrochemically and by the spectrometrical method ICP-AES. The solubility depends on [pCO{sub 2}]{sup 0.5} and on [pO{sub 2}]{sup 0.25}. Under cathode-gas conditions the solubilities ranged from 2 to 13 wt ppm, whereas the corresponding values for lithiated nickel oxide ranged from 7 to 20 wt ppm. The dissolution rate was determined from post-test analyses of small scale MCFC tests to be less than 0.5 {mu}g Co/cm{sup 2}h, which is an order of magnitude lower than that for nickel oxide. 3 figs., 11 refs.
Publication Date:
Jul 01, 1991
Product Type:
Technical Report
Report Number:
ECN-RX-91-062
Reference Number:
SCA: 300505; PA: ECN92:000217; SN: 92000695098
Resource Relation:
Other Information: DN: Submitted to the Journal of the Electrochemical Society; PBD: Jul 1991
Subject:
30 DIRECT ENERGY CONVERSION; MOLTEN CARBONATE FUEL CELLS; CATHODES; LIFETIME; COBALT OXIDES; NICKEL OXIDES; DISSOLUTION; SOLUBILITY; LITHIUM; BENCH-SCALE EXPERIMENTS; NUMERICAL DATA; 300505; ELECTROCHEMISTRY, MASS TRANSFER, AND THERMODYNAMICS
OSTI ID:
10132278
Research Organizations:
Netherlands Energy Research Foundation (ECN), Petten (Netherlands)
Country of Origin:
Netherlands
Language:
English
Other Identifying Numbers:
Other: ON: DE92790175; TRN: NL9200217
Availability:
OSTI; NTIS (US Sales Only)
Submitting Site:
ECN
Size:
12 p.
Announcement Date:
Jul 04, 2005

Citation Formats

Veldhuis, J B.J., Eckes, F C, and Plomp, L. The dissolution properties of LiCoO{sub 2} in molten 62:38 mole% Li:K carbonate. Netherlands: N. p., 1991. Web.
Veldhuis, J B.J., Eckes, F C, & Plomp, L. The dissolution properties of LiCoO{sub 2} in molten 62:38 mole% Li:K carbonate. Netherlands.
Veldhuis, J B.J., Eckes, F C, and Plomp, L. 1991. "The dissolution properties of LiCoO{sub 2} in molten 62:38 mole% Li:K carbonate." Netherlands.
@misc{etde_10132278,
title = {The dissolution properties of LiCoO{sub 2} in molten 62:38 mole% Li:K carbonate}
author = {Veldhuis, J B.J., Eckes, F C, and Plomp, L}
abstractNote = {The lifetime of a Molten Carbonate Fuel Cell (MCFC) is reduced by the slow dissolution of the state-of-the-art lithiated nickel oxide cathode material. LiCoO{sub 2} is considered to be an alternative cathode material by its good performance in MCFC tests. However, its dissolution rate was not known. In this letter the dissolution properties of LiCoO{sub 2} in 62:38 (Li:K){sub 2}CO{sub 3} at 923K are reported. The concentration of the dissolved Co{sup 2+} ions in the molten carbonate was determined electrochemically and by the spectrometrical method ICP-AES. The solubility depends on [pCO{sub 2}]{sup 0.5} and on [pO{sub 2}]{sup 0.25}. Under cathode-gas conditions the solubilities ranged from 2 to 13 wt ppm, whereas the corresponding values for lithiated nickel oxide ranged from 7 to 20 wt ppm. The dissolution rate was determined from post-test analyses of small scale MCFC tests to be less than 0.5 {mu}g Co/cm{sup 2}h, which is an order of magnitude lower than that for nickel oxide. 3 figs., 11 refs.}
place = {Netherlands}
year = {1991}
month = {Jul}
}