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Preparation and characterization of epitaxial high temperature superconductor layers; Herstellung und Charakterisierung epitaktischer Hochtemperatursupraleiter-Schichten

Abstract

Two types of high temperature superconductor films have been prepared by diode sputtering in a high oxygen atmosphere and subsequent in situ annealing in oxygen. Both, the YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} and Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}}-films, showed an excellent c-axis orientation, as verified by X-ray diffraction and Rutherford backscattering spectrum measurements. The rocking curve of YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} showed a full width at half maximum value (FWHM) of 0.17 , and Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} showed 0.15 . The minimum yield of the channeling measurements is lower then 2% for YBa{sub 2}Cu{sub 3}O{sub 7-{delta}}, and 9% for Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}}. The minimum yield for the Bi-superconductor is higher because of its incommensurable structure in the BiO-plane. The magnetic properties of the films were measured with a SQUID-magnetometer. Both kinds of films have the same critical temperature of approximately 91 Kelvin. However, the zero-field-cooled suscebilities for both cases were quite different: for fields of about B = 0.1 mT the transition curve is broaden for Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} in contrast to the curves of the YBa{sub 2}Cu{sub 3}O{sub 7-{delta}}-films. Critical current estimations done with a SQUID-magnetometer yielded for YBa{sub 2}Cu{sub 3}O{sub 7-{delta}}-films at 5  More>>
Authors:
Publication Date:
Aug 01, 1994
Product Type:
Thesis/Dissertation
Report Number:
Juel-2953
Reference Number:
SCA: 665412; 360204; PA: DEN-95:0F5629; EDB-95:054688; SN: 95001361432
Resource Relation:
Other Information: TH: Diss.; PBD: Aug 1994
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; 36 MATERIALS SCIENCE; HIGH-TC SUPERCONDUCTORS; CATHODE SPUTTERING; MAGNETIC PROPERTIES; SUPERCONDUCTING FILMS; YTTRIUM OXIDES; BARIUM OXIDES; COPPER OXIDES; BISMUTH OXIDES; STRONTIUM OXIDES; CALCIUM OXIDES; EPITAXY; CRITICAL CURRENT; MAGNETIC FLUX; X-RAY DIFFRACTION; BACKSCATTERING; ELECTRIC CONDUCTIVITY; 665412; 360204; SUPERCONDUCTING DEVICES; PHYSICAL PROPERTIES
OSTI ID:
10128411
Research Organizations:
Forschungszentrum Juelich GmbH (Germany). Inst. fuer Festkoerperforschung; Koeln Univ. (Germany)
Country of Origin:
Germany
Language:
German
Other Identifying Numbers:
Journal ID: ISSN 0944-2952; Other: ON: DE95756101; TRN: DE95F5629
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
DEN
Size:
82 p.
Announcement Date:
Jul 04, 2005

Citation Formats

Osthoever, C. Preparation and characterization of epitaxial high temperature superconductor layers; Herstellung und Charakterisierung epitaktischer Hochtemperatursupraleiter-Schichten. Germany: N. p., 1994. Web.
Osthoever, C. Preparation and characterization of epitaxial high temperature superconductor layers; Herstellung und Charakterisierung epitaktischer Hochtemperatursupraleiter-Schichten. Germany.
Osthoever, C. 1994. "Preparation and characterization of epitaxial high temperature superconductor layers; Herstellung und Charakterisierung epitaktischer Hochtemperatursupraleiter-Schichten." Germany.
@misc{etde_10128411,
title = {Preparation and characterization of epitaxial high temperature superconductor layers; Herstellung und Charakterisierung epitaktischer Hochtemperatursupraleiter-Schichten}
author = {Osthoever, C}
abstractNote = {Two types of high temperature superconductor films have been prepared by diode sputtering in a high oxygen atmosphere and subsequent in situ annealing in oxygen. Both, the YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} and Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}}-films, showed an excellent c-axis orientation, as verified by X-ray diffraction and Rutherford backscattering spectrum measurements. The rocking curve of YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} showed a full width at half maximum value (FWHM) of 0.17 , and Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} showed 0.15 . The minimum yield of the channeling measurements is lower then 2% for YBa{sub 2}Cu{sub 3}O{sub 7-{delta}}, and 9% for Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}}. The minimum yield for the Bi-superconductor is higher because of its incommensurable structure in the BiO-plane. The magnetic properties of the films were measured with a SQUID-magnetometer. Both kinds of films have the same critical temperature of approximately 91 Kelvin. However, the zero-field-cooled suscebilities for both cases were quite different: for fields of about B = 0.1 mT the transition curve is broaden for Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} in contrast to the curves of the YBa{sub 2}Cu{sub 3}O{sub 7-{delta}}-films. Critical current estimations done with a SQUID-magnetometer yielded for YBa{sub 2}Cu{sub 3}O{sub 7-{delta}}-films at 5 K J{sub C}(5K) = 6.0 10{sup 7} A/cm{sup 2}, and at 77 Kelvin J{sub C}(77K) = 3.7 10{sup 6} A/cm{sup 2}, for Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} at 5 K J{sub C}(5K) = 1.0 10{sup 7} A/cm{sup 2}, at 77 K J{sub C}(77K) = 1.0 10{sup 4} A/cm{sup 2}. The different behaviour of both samples in an external magnetic field can be explained by a strong different anisotropy of the superconducting properties. (orig.)}
place = {Germany}
year = {1994}
month = {Aug}
}