You need JavaScript to view this

Aqueous chemistry and thermodynamic modelling of CaO-SiO{sub 2}-H{sub 2}O gels at 80{sup o}C

Abstract

The dissolution of hydrated cement compounds controls the near-field chemistry in radwaste repositories containing cementitious materials. The dominant system in this respect is CaO-SiO{sub 2}-H{sub 2}O. Estimates of repository temperature indicate that this could be as high as 80{sup o}C in places. Therefore, in this work the thermodynamic properties and aqueous solubilities of compounds in the CaO-SiO{sub 2}-H{sub 2}O system have been determined at 80{sup o}C. The Gibbs energies of the solid phases have been expressed using a solid solution model, similar to that previously developed to describe data at 25{sup o}C, for the poorly crystalline gels that form in this system. The main effect of the higher temperature was found to be a reduction in pH. This is principally due to the different dissociation constant for water, with a smaller contribution from generally lower calcium solubilities at the higher temperature. Crystalline solid phases were observed to form, but these were not in equilibrium with the aqueous phase. (author).
Authors:
Atkinson, A; Hearne, J A; [1]  Knights, C F [2] 
  1. AEA Industrial Technology, Harwell (United Kingdom)
  2. AEA Technology, Harwell (United Kingdom)
Publication Date:
Dec 31, 1991
Product Type:
Technical Report
Report Number:
DOE-HMIP-RR-91.045; AEA-D and R-0153.
Reference Number:
SCA: 052002; 400201; PA: AIX-23:019708; SN: 92000664858
Resource Relation:
Other Information: PBD: 1991
Subject:
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE WASTES FROM NUCLEAR FACILITIES; 37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; CEMENTS; FREE ENTHALPY; RADIOACTIVE WASTE DISPOSAL; RADIOCHEMISTRY; THERMODYNAMIC MODEL; AQUEOUS SOLUTIONS; EXPERIMENTAL DATA; HYDRATION; PH VALUE; TEMPERATURE RANGE 0273-0400 K; 052002; 400201; WASTE DISPOSAL AND STORAGE; CHEMICAL AND PHYSICOCHEMICAL PROPERTIES
OSTI ID:
10120675
Research Organizations:
Department of the Environment, London (United Kingdom). Her Majesty`s Inspectorate of Pollution
Country of Origin:
United Kingdom
Language:
English
Other Identifying Numbers:
Other: ON: DE92618063; CNN: Contract PECD-7/9/504; TRN: GB9105511019708
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
GBN
Size:
33 p.
Announcement Date:
Jun 30, 2005

Citation Formats

Atkinson, A, Hearne, J A, and Knights, C F. Aqueous chemistry and thermodynamic modelling of CaO-SiO{sub 2}-H{sub 2}O gels at 80{sup o}C. United Kingdom: N. p., 1991. Web.
Atkinson, A, Hearne, J A, & Knights, C F. Aqueous chemistry and thermodynamic modelling of CaO-SiO{sub 2}-H{sub 2}O gels at 80{sup o}C. United Kingdom.
Atkinson, A, Hearne, J A, and Knights, C F. 1991. "Aqueous chemistry and thermodynamic modelling of CaO-SiO{sub 2}-H{sub 2}O gels at 80{sup o}C." United Kingdom.
@misc{etde_10120675,
title = {Aqueous chemistry and thermodynamic modelling of CaO-SiO{sub 2}-H{sub 2}O gels at 80{sup o}C}
author = {Atkinson, A, Hearne, J A, and Knights, C F}
abstractNote = {The dissolution of hydrated cement compounds controls the near-field chemistry in radwaste repositories containing cementitious materials. The dominant system in this respect is CaO-SiO{sub 2}-H{sub 2}O. Estimates of repository temperature indicate that this could be as high as 80{sup o}C in places. Therefore, in this work the thermodynamic properties and aqueous solubilities of compounds in the CaO-SiO{sub 2}-H{sub 2}O system have been determined at 80{sup o}C. The Gibbs energies of the solid phases have been expressed using a solid solution model, similar to that previously developed to describe data at 25{sup o}C, for the poorly crystalline gels that form in this system. The main effect of the higher temperature was found to be a reduction in pH. This is principally due to the different dissociation constant for water, with a smaller contribution from generally lower calcium solubilities at the higher temperature. Crystalline solid phases were observed to form, but these were not in equilibrium with the aqueous phase. (author).}
place = {United Kingdom}
year = {1991}
month = {Dec}
}