You need JavaScript to view this

The development of {sup 99m}Tc-d, 1-HM-PAO. A new radiopharmaceutical for regional cerebral blood perfusion imaging

Abstract

The {sup 99m}Tc-d,1-HM-PAO is an ideal radiopharmaceutical for regional cerebral blood perfusion imaging. The improvement of synthesis and separation of diastereoisomers leads to obtain high purity (>99%) of d, 1-HM-PAO and meso-HM-PAO. During separation H NMR spectroscopy was used to monitor the relative composition of these two diastereoisomers that can ensure the purity of pligand of d,1-HM-PAO. The intravenous injection of {sup 99m}Tc-d,1-HM-PAO was formed by adding fresh {sup 99m}Tc washing liquor into a sterile. Pyrogen-free and freeze-dried vial. The radiochemical purity (RCP) of {sup 99m}Tc-d,1-HM-PAO was greater than 80%. From the experiments of {sup 99m}Tc-d,1-HM-PAO in mice, after two minutes of intravenously (I>V>) administration about 2.24% of injected dose (I.D.)appeared in the brain, and after 24 hours about 72% of radioactivity of injected dose still left in the brain. But for the {sup 99m}Tc-meso-HM-PAO after two minutes of i.v. administration, about 1.93% of I.D. appeared in the brain, and 24 hours later, 25% of radioactivity of I.D. was in the brain. This result shows that in the brain the radioactivity of {sup 99m}Tc-meso-HM-PAO declines faster than that of {sup 99m}Td-d,1-HM-PAO.
Authors:
Lanqin, Bai; Jinjie, Huang; Li, Fan; Suzhen, Bai; Guoli, Li; Hui, Jing; Lun, Xiao [1] 
  1. China Inst. of Atomic Energy, Beijing (China)
Publication Date:
Dec 01, 1991
Product Type:
Technical Report
Report Number:
CNIC-00547; IAE-0100.
Reference Number:
SCA: 400703; PA: AIX-24:004993; SN: 93000930232
Resource Relation:
Other Information: PBD: Dec 1991
Subject:
38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEAR CHEMISTRY; CONTRAST MEDIA; BRAIN; CHEMICAL PREPARATION; LABELLED COMPOUNDS; TISSUE DISTRIBUTION; BLOOD FLOW; CLEARANCE; LABELLING; NMR SPECTRA; NUCLEAR MAGNETIC RESONANCE; RADIOPHARMACEUTICALS; TECHNETIUM 99; UPTAKE; 400703; RADIOISOTOPE PRODUCTION
OSTI ID:
10118665
Research Organizations:
China Nuclear Information Centre, Beijing, BJ (China)
Country of Origin:
China
Language:
Chinese
Other Identifying Numbers:
Other: ON: DE93610800; ISBN 7-5022-0562-4; TRN: CN9201657004993
Availability:
OSTI; NTIS (US Sales Only); INIS
Submitting Site:
INIS
Size:
[14] p.
Announcement Date:
Jun 30, 2005

Citation Formats

Lanqin, Bai, Jinjie, Huang, Li, Fan, Suzhen, Bai, Guoli, Li, Hui, Jing, and Lun, Xiao. The development of {sup 99m}Tc-d, 1-HM-PAO. A new radiopharmaceutical for regional cerebral blood perfusion imaging. China: N. p., 1991. Web.
Lanqin, Bai, Jinjie, Huang, Li, Fan, Suzhen, Bai, Guoli, Li, Hui, Jing, & Lun, Xiao. The development of {sup 99m}Tc-d, 1-HM-PAO. A new radiopharmaceutical for regional cerebral blood perfusion imaging. China.
Lanqin, Bai, Jinjie, Huang, Li, Fan, Suzhen, Bai, Guoli, Li, Hui, Jing, and Lun, Xiao. 1991. "The development of {sup 99m}Tc-d, 1-HM-PAO. A new radiopharmaceutical for regional cerebral blood perfusion imaging." China.
@misc{etde_10118665,
title = {The development of {sup 99m}Tc-d, 1-HM-PAO. A new radiopharmaceutical for regional cerebral blood perfusion imaging}
author = {Lanqin, Bai, Jinjie, Huang, Li, Fan, Suzhen, Bai, Guoli, Li, Hui, Jing, and Lun, Xiao}
abstractNote = {The {sup 99m}Tc-d,1-HM-PAO is an ideal radiopharmaceutical for regional cerebral blood perfusion imaging. The improvement of synthesis and separation of diastereoisomers leads to obtain high purity (>99%) of d, 1-HM-PAO and meso-HM-PAO. During separation H NMR spectroscopy was used to monitor the relative composition of these two diastereoisomers that can ensure the purity of pligand of d,1-HM-PAO. The intravenous injection of {sup 99m}Tc-d,1-HM-PAO was formed by adding fresh {sup 99m}Tc washing liquor into a sterile. Pyrogen-free and freeze-dried vial. The radiochemical purity (RCP) of {sup 99m}Tc-d,1-HM-PAO was greater than 80%. From the experiments of {sup 99m}Tc-d,1-HM-PAO in mice, after two minutes of intravenously (I>V>) administration about 2.24% of injected dose (I.D.)appeared in the brain, and after 24 hours about 72% of radioactivity of injected dose still left in the brain. But for the {sup 99m}Tc-meso-HM-PAO after two minutes of i.v. administration, about 1.93% of I.D. appeared in the brain, and 24 hours later, 25% of radioactivity of I.D. was in the brain. This result shows that in the brain the radioactivity of {sup 99m}Tc-meso-HM-PAO declines faster than that of {sup 99m}Td-d,1-HM-PAO.}
place = {China}
year = {1991}
month = {Dec}
}