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Development of high efficient process for simultaneous removal of SOx and NOx from flue gas (III)

Abstract

The object of this research is to develop the simultaneous SOx and NOx removal process from flue gases using limestone and P4 additive. The research results are as follows; 1. Phosphorus oxy acids produced by reaction of P4 and O2 were PO43-, PO33-, and PO23-, and ion concentration distribution in the reactor solution was more than 50% PO43-, less than 50% of PO33- and small amount of PO23-. Total ion concentration in both a reactor and washing column was PO43- of 77%, PO33- of 12.9% and PO23- of 10.1%. The byproduct produced from the oxidation of P4 was recovered as a phosphoric acid up to 98% using one washing column. 2. The effects of L/G, pH, inlet SO{sub 2} concentration were tested by long term experiments in the mini-pilot scale system. The measured change in SO{sub 2} pickup was a linear function of the inlet SO{sub 2} concentration over the range of SO{sub 2} concentrations tested. 3. The increase of P4 concentration from 0.1 to 0.5 w/w% increased the P/NO mole ratio from 2.0 to 4.2 and consumption rate of limestone increased linearly in the mini-pilot scale system. The increase of inlet NO concentration from 270 ppm to 750 ppm  More>>
Authors:
Lee, H K; Kim, C H; Choi, I S; Kim, Y I; Min, B M; Park, S D; Choi, W K; Bak, I H; Kim, J G; Cho, H D; Lee, J S; Kim, S U; Lee, W S [1] 
  1. Korea Institute of Energy Research, Taejon (Korea, Republic of)
Publication Date:
Oct 01, 1994
Product Type:
Technical Report
Report Number:
KE-93008S
Reference Number:
SCA: 320106; PA: KR-94:000151; EDB-95:028897; SN: 95001335467
Resource Relation:
Other Information: PBD: Oct 1994
Subject:
32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATION; NITROGEN OXIDES; REMOVAL; SULFUR OXIDES; FUEL GAS; PHOSPHOROUS ACID; LIME-LIMESTONE WET SCRUBBING PROCESSES; ADDITIVES; 320106; BUILDING EQUIPMENT
OSTI ID:
10115759
Research Organizations:
No corporate text available (Country unknown/Code not available)
Country of Origin:
Korea, Republic of
Language:
Korean
Other Identifying Numbers:
Other: ON: DE95744279; TRN: KR9400151
Availability:
OSTI; NTIS (US Sales Only)
Submitting Site:
KR
Size:
191 p.
Announcement Date:
Jun 30, 2005

Citation Formats

Lee, H K, Kim, C H, Choi, I S, Kim, Y I, Min, B M, Park, S D, Choi, W K, Bak, I H, Kim, J G, Cho, H D, Lee, J S, Kim, S U, and Lee, W S. Development of high efficient process for simultaneous removal of SOx and NOx from flue gas (III). Korea, Republic of: N. p., 1994. Web.
Lee, H K, Kim, C H, Choi, I S, Kim, Y I, Min, B M, Park, S D, Choi, W K, Bak, I H, Kim, J G, Cho, H D, Lee, J S, Kim, S U, & Lee, W S. Development of high efficient process for simultaneous removal of SOx and NOx from flue gas (III). Korea, Republic of.
Lee, H K, Kim, C H, Choi, I S, Kim, Y I, Min, B M, Park, S D, Choi, W K, Bak, I H, Kim, J G, Cho, H D, Lee, J S, Kim, S U, and Lee, W S. 1994. "Development of high efficient process for simultaneous removal of SOx and NOx from flue gas (III)." Korea, Republic of.
@misc{etde_10115759,
title = {Development of high efficient process for simultaneous removal of SOx and NOx from flue gas (III)}
author = {Lee, H K, Kim, C H, Choi, I S, Kim, Y I, Min, B M, Park, S D, Choi, W K, Bak, I H, Kim, J G, Cho, H D, Lee, J S, Kim, S U, and Lee, W S}
abstractNote = {The object of this research is to develop the simultaneous SOx and NOx removal process from flue gases using limestone and P4 additive. The research results are as follows; 1. Phosphorus oxy acids produced by reaction of P4 and O2 were PO43-, PO33-, and PO23-, and ion concentration distribution in the reactor solution was more than 50% PO43-, less than 50% of PO33- and small amount of PO23-. Total ion concentration in both a reactor and washing column was PO43- of 77%, PO33- of 12.9% and PO23- of 10.1%. The byproduct produced from the oxidation of P4 was recovered as a phosphoric acid up to 98% using one washing column. 2. The effects of L/G, pH, inlet SO{sub 2} concentration were tested by long term experiments in the mini-pilot scale system. The measured change in SO{sub 2} pickup was a linear function of the inlet SO{sub 2} concentration over the range of SO{sub 2} concentrations tested. 3. The increase of P4 concentration from 0.1 to 0.5 w/w% increased the P/NO mole ratio from 2.0 to 4.2 and consumption rate of limestone increased linearly in the mini-pilot scale system. The increase of inlet NO concentration from 270 ppm to 750 ppm decreased the P /NO ratio from 3.2 to 2.0. As the L/G ratio increased from 47.4 to 67.5, the maximum removal efficiency of NO was increased from 71.9 to 89.6%, and P/NO ratio was decreased from 3.2 to 2.2 in the mini-pilot scale system. 4. Sulfite oxidation reaction was investigated to use the byproduct in the lab-scale apparatus. When we keep the reaction order of 1.5, the rate constants were 3.19 x 10-4, and 8.95 x 10-4 when the pH were 4.5 and 9.5, respectively. The catalytic activity of Mn{sub 2}{sup +} was much higher than that of Mg{sub 2}{sup +} even though the concentration of Mn{sub 2}{sup +} was lower than Mg{sub 2}{sup +}. (author). refs., figs., tabs.}
place = {Korea, Republic of}
year = {1994}
month = {Oct}
}